Article(id=1322608999518819242, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190540, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1561996800000, receivedDateStr=2019-07-02, revisedDate=1569513600000, revisedDateStr=2019-09-27, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264158372, onlineDateStr=2026-10-29, pubDate=1582128000000, pubDateStr=2020-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264158372, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264158372, creator=13701087609, updateTime=1793264158372, updator=13701087609, issue=Issue{id=1322608967147172356, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='2', pageStart='147', pageEnd='324', issueExtLink='null', onlineDate='null', pubDate='1582128000000', pubDateStr='2020-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264150653, creator='13701087609', updateTime=1793276939599, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662607933255748, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662607933255749, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=204, endPage=210, ext={EN=ArticleExt(id=1322608999686591403, articleId=1322608999518819242, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Enhanced Photoluminescence of Ba₂SiO₄:Eu²⁺ Phosphor by Ca²⁺ or Mg²⁺ Substitution, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

(Ba_1-xMe_x)_1.95SiO₄:0.05Eu (Me=Ca, Mg) phosphor was synthesized in a reducing atmosphere by a high-temperature solid-phase method. Ca²⁺ and Mg²⁺ solubilities in Ba₂SiO₄-phase should be 10% (mole fraction, the same below) and 30%, and the solid solution induces an increase in green fluorescence brightness under ultraviolet excitation. The intensity of (Ba_0.9Ca_0.1)_1.95SiO₄:0.05Eu and (Ba_0.7Mg_0.3)_1.95SiO₄:0.05Eu phosphors is 110% and 140% greater than that of Ba₂SiO₄:Eu under 365 nm, and 105% and 125% greater than that of Ba₂SiO₄:Eu under 254 nm. Based on the analysis by X-ray diffraction, (Ba_1-xCa_x)_1.95SiO₄ (0.1<x≤0.3) is T-phase but not Ba₂SiO₄-phase. Ca²⁺ or Mg²⁺ substitution does not decrease in cell volume but causes the better crystallization (i.e., the diffraction peak is higher, and the half-width is more narrow). Further more, b decreases a little more quickly than c, indicating that Eu²⁺ ions prefer 9-coordinated Ba²⁺(II) sites more than 10-coordinated Ba²⁺(I) sites. According to the high-resolution photo luminescent spectra, Eu²⁺(I) contributes more than Eu²⁺(II) for the green luminescence intensity. Moreover, Eu²⁺(I)/Eu²⁺(II) ratio increases as Ca²⁺ or Mg²⁺ solubility increases. The high-resolution X-ray photoelectron spectra of Eu4d indicate that the valence of Eu is rarely changed after cation substitution. Ca²⁺ or Mg²⁺ substitution can improve the crystallinity, promote Eu²⁺ to enter Ba²⁺(I) site(which would has higher luminescent efficiency) and keep Eu ion valence stable due to the improvement of phosphor luminescent intensity by cation substitution.

, authors=Mingyuan GAO¹, Lan LUO^{1, 2}, Yu WANG¹, Rui GUO¹, authorsList=Mingyuan GAO, Lan LUO, Yu WANG, Rui GUO, authorCompany=null, correspAuthors=Lan LUO, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608999921472428, articleId=1322608999518819242, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Ca²⁺、Mg²⁺固溶Ba₂SiO₄：Eu²⁺荧光增强机理, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用高温固相法在还原气氛得到（Ba_1-xMe_x）_1.95SiO₄：0.05Eu（Me=Ca，Mg）荧光粉。采用X射线衍射仪、场发射扫描电镜、元素分析仪、荧光光谱仪对样品进行分析，结果表明：Ca²⁺、Mg²⁺在Ba₂SiO₄相的固溶度分别为10%（摩尔分数，下同）和30%，其对应荧光粉比Ba₂SiO₄：Eu在紫外激发绿色荧光亮度有明显提高（365 nm激发下亮度为Ba₂SiO₄：Eu的110%、140%，254 nm激发下则为105%、125%）。（Ba_1-xCa_x）_1.95SiO₄（0.1<x≤0.3）为T相而非Ba₂SiO₄相，故离子半径与Ba²⁺更接近的Ca²+反而比Mg²⁺在Ba₂SiO₄相的固溶度更低；Ca²⁺、Mg²⁺在Ba₂SiO₄中固溶，使得晶格参数略微减小，且b比c减小更快，即Ca²⁺、Mg²⁺更倾向取代9配位Ba²⁺（II）而非10配位Ba²⁺（I）；固溶有利于粉末结晶状况提高（衍射峰增强、半峰宽变窄）。Eu²⁺（I）比Eu²⁺（II）对绿光贡献更大，Ca²⁺、Mg²⁺可促进Eu²⁺（I）/Eu²⁺（II）比值提高。Eu4d高分辨光电子谱表明，Ca²⁺、Mg²⁺对Eu离子的价态无明显影响。由此可见，Ca²⁺、Mg²⁺固溶可提高Ba₂SiO₄相粉末结晶程度、促进Eu²⁺进入发光效率更高Ba²⁺（I）位置，同时不影响Eu²⁺的价态稳定性，是固溶提升Ba₂SiO₄：Eu荧光粉发光性能原因所在。

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GAO Mingyuan (1998-), male, Master candidate. E-mail: 1206861141@qq.com

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GAO Mingyuan (1998-), male, Master candidate. E-mail: 1206861141@qq.com

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高明远（1998—），男，硕士研究生。

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高明远（1998—），男，硕士研究生。

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