Article(id=1322608995647468334, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190457, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1561910400000, receivedDateStr=2019-07-01, revisedDate=1564588800000, revisedDateStr=2019-08-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264157448, onlineDateStr=2026-10-29, pubDate=1582128000000, pubDateStr=2020-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264157448, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264157448, creator=13701087609, updateTime=1793264157448, updator=13701087609, issue=Issue{id=1322608967147172356, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='2', pageStart='147', pageEnd='324', issueExtLink='null', onlineDate='null', pubDate='1582128000000', pubDateStr='2020-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264150653, creator='13701087609', updateTime=1793276939599, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662607933255748, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662607933255749, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=309, endPage=315, ext={EN=ArticleExt(id=1322608995878155055, articleId=1322608995647468334, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis and Characterization of Hierarchical Zeolite L Nanocrystals, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Zeolite L with a Si/Al moles ratio of 1.9 was synthesized from initial concentrated gel in the absence of organic templates. The crystallization behavior and the crystal microstructure during crystallization were analyzed by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption and energy dispersive X-ray spectroscopy. The effects of synthesis parameters such as synthesis time, aging time and molar compositions on the crystal growth were investigated. The results show that as-synthesized zeolite nanocrystals possess hierarchical structure. Pure zeolite L with a high crystallinity was obtained within a wide ratio range of gel SiO₂/Al₂O₃ of 20-100. Moreover, the adsorption performance of the samples under the optimized synthesis conditions were evaluated via the equilibrium adsorption of pure gases CO₂, CH₄ and N₂ at 25 ℃. Zeolite nanocrystals exhibit a high CO₂ adsorption capacity.

, authors=Na HU, Jiayou ZHANG, Huizhi ZHANG, Xiangshu CHEN, authorsList=Na HU, Jiayou ZHANG, Huizhi ZHANG, Xiangshu CHEN, authorCompany=null, correspAuthors=Xiangshu CHEN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608996113036080, articleId=1322608995647468334, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=多级孔道纳米L型分子筛的合成与表征, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

在非有机模板剂体系中、采用浓稠的初始合成溶胶高效合成Si/Al比为1.9的L型分子筛。借助X射线衍射、扫描电子显微镜、透射电子显微镜、氮气吸脱附测试和X射线能谱仪等手段表征晶体的晶化行为和微结构，并考察了合成条件如合成时间、老化时间和溶胶配比对晶体生长的影响。结果表明：合成的纳米L型分子筛具有多级孔道结构。高结晶度且纯相的L型分子筛可在较宽的n（SiO₂）/n（Al₂O₃）值（20~100）范围内得到。此外，优化条件下合成的纳米L型分子筛在25 ℃时对CO₂、CH₄和N₂进行等温吸附测试，结果表明此分子筛具有较高的CO₂吸附量。

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HU Na (1984−), female, Ph.D., Senior Experimentalist. E-mail: huna@jxnu.edu.cn

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HU Na (1984−), female, Ph.D., Senior Experimentalist. E-mail: huna@jxnu.edu.cn

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胡娜（1984—），女，博士，高级实验师。

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胡娜（1984—），女，博士，高级实验师。

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