Article(id=1322608993093145473, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190314, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1557676800000, receivedDateStr=2019-05-13, revisedDate=1562083200000, revisedDateStr=2019-07-03, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264156839, onlineDateStr=2026-10-29, pubDate=1579449600000, pubDateStr=2020-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264156839, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264156839, creator=13701087609, updateTime=1793264156839, updator=13701087609, issue=Issue{id=1322608929100649011, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='1', pageStart='1', pageEnd='146', issueExtLink='null', onlineDate='null', pubDate='1579449600000', pubDateStr='2020-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264141583, creator='13701087609', updateTime=1793276771816, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661904204542961, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661904208737266, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=86, endPage=93, ext={EN=ArticleExt(id=1322608994934444930, articleId=1322608993093145473, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Lime on Properties of Filling Cementitious Material Prepared by Hemihydrate Phosphogypsum, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The gelling activity of hemihydrate phosphogypsum (HPG) is poor and its setting process is slow due to the effect of soluble impurities such as P₂O₅ and F^-. Compared to cement clinker, the strength of HPG modified with lime as a hemihydrate phosphogypsum filling cementitious material (HCM) for goaf filling can be improved. The setting time and bleeding rate of HCM decrease rapidly and then increase slowly, and the compressive strength reverses with the increase of lime. Also, the concentration of total phosphorus and fluoride in the HCM leaching solution gradually decreases to below the standard values from the National Standard of Class I Solid Wastes. For the filling performance and environmental protection, the optimum mass fraction of lime in HCM is 2.0%. Lime can transform soluble P₂O₅ and F^- into insoluble precipitates such as Ca₃(PO₄)₂ and CaF₂ to accelerate HPG hydration, increase the number of dihydrate gypsum crystal contact points, and further improve the HCM filling performance. The experimental pH value of HCM leaching solution is lower than the theoretical value, indicating that P₂O₅ in crystal can dissolve into soluble P₂O₅ in the process of HPG hydration, thus leading to a decreased alkalinity of backfill.

, authors=Guanzhao JIANG¹, Aixiang WU¹, Yiming WANG¹, Jianqiu LI², authorsList=Guanzhao JIANG, Aixiang WU, Yiming WANG, Jianqiu LI, authorCompany=null, correspAuthors=Aixiang WU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608995219657603, articleId=1322608993093145473, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=生石灰对半水磷石膏充填胶凝材料性能影响, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

由于可溶性P₂O₅、F^-等杂质的影响，半水磷石膏（HPG）胶凝活性较差，凝结速率慢。与水泥熟料相比，生石灰改性后的HPG强度性能显著提高，可以作为半水磷石膏充填胶凝材料（HCM）应用于采空区充填。室内试验表明，随着生石灰添加量的增加，HCM凝结时间和泌水率呈先快速下降后缓慢上升规律，抗压强度变化则相反，同时浸出液中总磷和氟化物浓度逐渐降至Ⅰ类固体废弃物标准允许值以下。综合考虑充填性能和环保性，HCM最佳生石灰添加量为2.0%（质量分数）。生石灰使可溶性P₂O₅、F^-转化为Ca₃（PO₄）₂和CaF₂等难溶性沉淀，加速HPG水化，增加二水石膏晶体接触点数目，提高HCM充填性能。HCM浸出液pH实验值均低于理论值，说明HPG水化过程中共晶P₂O₅会溶为可溶性P₂O₅，降低充填体碱度。

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JIANG Guanzhao (1993-), male, Ph.D. candidate. E-mail: jgz_ustb@163.com

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姜关照（1993—），男，博士研究生。

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姜关照（1993—），男，博士研究生。

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