Article(id=1322608982942921429, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190584, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1564243200000, receivedDateStr=2019-07-28, revisedDate=1565798400000, revisedDateStr=2019-08-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264154420, onlineDateStr=2026-10-29, pubDate=1582128000000, pubDateStr=2020-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264154420, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264154420, creator=13701087609, updateTime=1793264154420, updator=13701087609, issue=Issue{id=1322608967147172356, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='2', pageStart='147', pageEnd='324', issueExtLink='null', onlineDate='null', pubDate='1582128000000', pubDateStr='2020-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264150653, creator='13701087609', updateTime=1793276939599, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662607933255748, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662607933255749, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=211, endPage=221, ext={EN=ArticleExt(id=1322608983127470806, articleId=1322608982942921429, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Early Hydration and Microstructure of Cement Pastes Mixed with Low-Temperature Early Strength Accelerator at 5 ℃, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A low-temperature early-strength accelerator was designed with three components, such as calcium bromide (CaBr₂), lithium bromide (LiBr) and triisopropanolamine (TIPA). Effect of early-strength accelerator on the strength, setting time and fluidity of cement paste at a low temperature was investigated, and its mechanism of action was discussed based on the perspectives of hydration heat and product microstructure. The results show that the incorporation of low-temperature early-strength accelerator shortens the initial and final setting time of cement pastes, and accelerates the strength development of specimens at a low temperature (i.e., 5 ℃). The 1-d, 3-d, 7-d and 28-d compressive strength of cement pastes mixed with the low-temperature early-strength accelerator can be increased by 291%, 78%, 62% and 40%, respectively, and the strengthat each age after 3 d already exceeds that of the contrast sample cured at 20 ℃. At a low temperature, the early-strength accelerator can shorten the hydration induction period of cement hydration and advance the acceleration period. Furthermore, the maximum heat release rate can be increased by 78%, compared to the contrast sample. The cumulative heat release is increased by 227% and 52% at 12 h and 7 d, respectively. The early-strength accelerator can also promote the hydration reaction at the initial stage of cement hydration, increase the content of Ca(OH)₂ in the sample and increase the hydration degree. Large amounts of Ca(OH)₂ are formed in the products at the age of only 12 h, and some products, such as bromine-containing C-S-H gels and hydrated calcium bromoaluminate (Ca₄Al₂O₆Br₂·10H₂O), are also generated. Large amounts of hydration products are accumulated, refining the pore diameter of the specimens at the initial stage of hydration (before 7 d) and decreasing the number of macropores. The total porosity of the cement pastes at 1 and 7 d is decreased by 16% and 31%, respectively, thus leading to the denser microstructure.

, authors=Feng ZHANG^{1, 2}, Yin BAI^{1, 2}, Yuebo CAI^{1, 2}, Bo CHEN^{1, 2}, Fengwei NING^{1, 2}, authorsList=Feng ZHANG, Yin BAI, Yuebo CAI, Bo CHEN, Fengwei NING, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608983345574615, articleId=1322608982942921429, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=5 ℃时掺低温早强剂水泥的早期水化及微观结构, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以溴化钙（CaBr₂）、溴化锂（LiBr）和三异丙醇胺（TIPA）三组分制备低温早强剂，研究低温下，早强剂对净浆强度、凝结时间、流动度的影响，并从水化热、产物微观结构等角度出发，探讨其作用机理。结果表明：5 ℃低温时，低温早强剂的掺入使净浆初、终凝时间均略有所缩短，可明显加快试件的强度发展，掺低温早强剂净浆1、3、7、28 d抗压强度较对比样分别提高291%、78%、62%和40%，3 d后各龄期强度已超对比样20 ℃时强度。低温下，低温早强剂使水泥水化诱导期缩短、加速期提前，最大放热速率较对比样增大78%，12 h、7 d累计放热量则分别增大227%和52%。低温早强剂可促进水泥初期水化反应，使试样中Ca（OH）₂含量增加、水化程度增大，水化12 h产物中即有大量Ca（OH）₂生成，且生成了含溴C-S-H凝胶和水化溴氧铝酸钙[Ca₄Al₂O₆Br₂·10H₂O]产物。水化产物相互堆积，细化了水化初期（7 d前）试件的孔径，大孔数量明显减少，净浆1、7 d总孔隙率较对比样分别减小16%、31%，试样微观结构更加致密。

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ZHANG Feng (1989-), male, Ph.D., Engineer. E-mail: fzhang@nhri.cn

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