Article(id=1322608970120942310, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190127, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1551283200000, receivedDateStr=2019-02-28, revisedDate=1553184000000, revisedDateStr=2019-03-22, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264151363, onlineDateStr=2026-10-29, pubDate=1579449600000, pubDateStr=2020-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264151363, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264151363, creator=13701087609, updateTime=1793264151363, updator=13701087609, issue=Issue{id=1322608929100649011, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='1', pageStart='1', pageEnd='146', issueExtLink='null', onlineDate='null', pubDate='1579449600000', pubDateStr='2020-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264141583, creator='13701087609', updateTime=1793276771816, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661904204542961, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661904208737266, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=65, endPage=72, ext={EN=ArticleExt(id=1322608970657813223, articleId=1322608970120942310, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Compressive Elastic Moduli of Dendritic Mesoporous Silica Particles and Their Composites, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Dendritic-like mesoporous silica particles (DMS) were prepared via a developed oil-water biphase stratification approach using cetyltrimethylammonium bromide, tetraethoxysilane, triethanolamine, and n-hexane as starting materials. The ceria nanoparticles were grafted onto the DMS surfaces using cerium nitrate as a cerium source and hexamethylene tetramine as a precipitant, and core/shell structured DMS/CeO₂ composites were obtained. The samples were characterized by scanning electron microscopy, transmission electron microscopy, low-angle X-ray diffraction, selected area electron diffraction, and nitrogen adsorption-desorption analysis. The elastic contact between an individual particle and a probe was evaluated by atomic force microscopy. The compressive elastic moduli of the DMS particles before and after ceria coating were calculated by fitting the force curves based on the Derjaguin-Müller-Toporov model. The results show that the DMS samples (ca. 92 nm in particle size) have central-radial three-dimensional mesopores with an average pore size of 6.9 nm. The average particle size of DMS/CeO₂ is about 106 nm, and the thin layer of ceria nanoparticles (i.e., 5-8 nm) is uniformly coated onto the cores. The compressive modulus of DMS particles is (3.7±1.2)GPa, further revealing that an enlarged pore size contributs to the elastic response enhancement for mesoporous silica materials. The compressive modulus of DMS/CeO₂ [i.e., (6.6±1.9)GPa] is much lower than that of bulk ceria materials, and much closed to that of DMS cores. The elastic response of DMS/CeO₂ derives from the cores, and the coated ceria nanoparticles contributed to the surface hardness enhancement.

, authors=Ailian CHEN^{1, 2}, Xiangyu MA³, Wanying WANG³, Wenjie CAI³, Yang CHEN³, authorsList=Ailian CHEN, Xiangyu MA, Wanying WANG, Wenjie CAI, Yang CHEN, authorCompany=null, correspAuthors=Yang CHEN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608971047883496, articleId=1322608970120942310, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=树枝状介孔氧化硅及其复合颗粒的制备和压缩弹性模量, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以正己烷、三乙醇胺、正硅酸乙酯和十六烷基三甲基溴化铵等为主要原料，采用改进的油水两相反应体系制备树枝状介孔氧化硅（DMS）颗粒；再以硝酸亚铈为铈源、六亚甲基四胺为缓释沉淀剂，在DMS表面均匀包覆CeO₂纳米粒子，得到核壳结构DMS/CeO₂复合颗粒。利用扫描电子显微镜、透射电子显微镜、小角度X射线衍射仪、选区电子衍射和氮气吸附-脱附等手段对样品进行结构表征。借助原子力显微镜力曲线技术，评价单个颗粒与探针之间的弹性接触，结合DMT模型拟合计算被测样品的压缩弹性模量。结果表明：DMS颗粒（约92 nm）内部存在中心三维树枝状介孔孔道，平均孔径约6.9 nm；复合颗粒的平均粒径约106 nm，CeO₂纳米粒子（5~8 nm）在内核表面均匀包覆形成薄层。DMS颗粒的弹性模量为（3.7±1.2）GPa，对比发现增大孔径有助于介孔氧化硅弹性响应的提高。复合颗粒的模量（6.6±1.9）GPa显著低于CeO₂块体材料，更接近于DMS内核，表明其弹性行为由内核所提供，壳层粒子可提高颗粒的整体表面硬度。

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CHEN Ailian (1975-), female, Ph.D., Associate Professor. E-mail: cy_cczu@126.com

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CHEN Ailian (1975-), female, Ph.D., Associate Professor. E-mail: cy_cczu@126.com

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