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Article(id=1322608941155070229, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190284, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1556467200000, receivedDateStr=2019-04-29, revisedDate=1562688000000, revisedDateStr=2019-07-10, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264144456, onlineDateStr=2026-10-29, pubDate=1579449600000, pubDateStr=2020-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264144456, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264144456, creator=13701087609, updateTime=1793264144456, updator=13701087609, issue=Issue{id=1322608929100649011, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='1', pageStart='1', pageEnd='146', issueExtLink='null', onlineDate='null', pubDate='1579449600000', pubDateStr='2020-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264141583, creator='13701087609', updateTime=1793276771816, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661904204542961, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661904208737266, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=53, endPage=60, ext={EN=ArticleExt(id=1322608941364785430, articleId=1322608941155070229, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Zirconia Nanopowder by Sol-gel Method, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A zirconia nanopowder was prepared by a sol-gel method using ZrOCl2·8H2O as zirconium source and polyethylene oxide-polypropylene oxide-polyethylene oxide (P123) as a dispersant. In the preparation, carbon nanoparticles generated via carbonization of P123 have an effect on the dispersion of zirconia particles, thus obtaining zirconia nanopowder without impurity ions via water washing/alcohol washing. The results show that zirconia nanopowder with a narrow particle size distribution and a median size (D50) of 158 nm can be obtained at a mass ratio of P123 to zirconia of 80% and calcination temperature of 1 100 ℃. This method could be used as an environmentally friendly and efficient approach for the preparation of the nanopowder

, authors=Yang WANG, Qikun WANG, Chao WANG, Yongqing WANG, Ke YANG, Qibing CHANG, authorsList=Yang WANG, Qikun WANG, Chao WANG, Yongqing WANG, Ke YANG, Qibing CHANG, authorCompany=null, correspAuthors=Qikun WANG, Qibing CHANG, authorNote=

WANG Yang (1995-), male, Master candidate. E-mail:

, correspAuthorsNote=
CHANG Qibing (1978-), male, Ph.D., Professor. E-mail:
WANG Qikun(1992-), male, Doctoral candidate.
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以八水氧氯化锆为锆源，聚环氧乙烷-聚环氧丙烷-聚环氧乙烷三嵌段共聚物（P123）为分散剂，采用P123辅助溶胶-凝胶法制备纳米氧化锆粉体。在制备过程中，P123经碳化生成的纳米碳颗粒起到了将氧化锆颗粒隔离分散的作用，因此在该方法中无需水洗/醇洗过程去除杂质离子即可获得纳米氧化锆粉体。结果表明：当P123与理论合成氧化锆的质量比为80%，煅烧温度为1100 ℃时，能够得到分散性好，粒径分布较窄，中位粒径（D50）仅为158 nm的纳米氧化锆粉体。该方法为环保、高效制备纳米粉体提供了一种新的思路。

, authors=王洋, 汪其堃, 汪超, 汪永清, 杨柯, 常启兵, authorsList=王洋, 汪其堃, 汪超, 汪永清, 杨柯, 常启兵, authorCompany=null, correspAuthors=汪其堃, 常启兵, authorNote=

王洋（1995—），男，硕士研究生。

, correspAuthorsNote=
常启兵（1978—），男，博士，教授。
汪其堃（1992—），男，博士研究生。
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WANG Yang (1995-), male, Master candidate. E-mail:

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WANG Yang (1995-), male, Master candidate. E-mail:

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王洋（1995—），男，硕士研究生。

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王洋（1995—），男，硕士研究生。

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辅助溶胶-凝胶法制备纳米氧化锆粉体
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王洋 , 汪其堃 , 汪超 , 汪永清 , 杨柯 , 常启兵
硅酸盐学报 | 2020,48(1): 53-60
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硅酸盐学报 | 2020 , 48 (1) : 53 -60
辅助溶胶-凝胶法制备纳米氧化锆粉体
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景德镇 333403)])])]
王洋 , 汪其堃 , 汪超, 汪永清, 杨柯, 常启兵
作者信息
  • 景德镇陶瓷大学材料科学与工程学院，江西 景德镇 333403
通讯作者:
常启兵（1978—），男，博士，教授。
汪其堃（1992—），男，博士研究生。
作者简介:

王洋（1995—），男，硕士研究生。

Preparation of Zirconia Nanopowder by Sol-gel Method
Yang WANG , Qikun WANG , Chao WANG, Yongqing WANG, Ke YANG, Qibing CHANG
Affiliations
  • School of Materials Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333403, Jiangxi, China
    • Corresponding Author:
    CHANG Qibing (1978-), male, Ph.D., Professor. E-mail:
    WANG Qikun(1992-), male, Doctoral candidate.

    WANG Yang (1995-), male, Master candidate. E-mail:

出版时间: 2020-01-20 doi: 10.14062/j.issn.0454-5648.20190284
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以八水氧氯化锆为锆源，聚环氧乙烷-聚环氧丙烷-聚环氧乙烷三嵌段共聚物（P123）为分散剂，采用P123辅助溶胶-凝胶法制备纳米氧化锆粉体。在制备过程中，P123经碳化生成的纳米碳颗粒起到了将氧化锆颗粒隔离分散的作用，因此在该方法中无需水洗/醇洗过程去除杂质离子即可获得纳米氧化锆粉体。结果表明：当P123与理论合成氧化锆的质量比为80%，煅烧温度为1100 ℃时，能够得到分散性好，粒径分布较窄，中位粒径（D50）仅为158 nm的纳米氧化锆粉体。该方法为环保、高效制备纳米粉体提供了一种新的思路。

氧化锆  /  聚环氧乙烷-聚环氧丙烷-聚环氧乙烷三嵌段共聚物  /  纳米粉体  /  分散  /  隔离

A zirconia nanopowder was prepared by a sol-gel method using ZrOCl2·8H2O as zirconium source and polyethylene oxide-polypropylene oxide-polyethylene oxide (P123) as a dispersant. In the preparation, carbon nanoparticles generated via carbonization of P123 have an effect on the dispersion of zirconia particles, thus obtaining zirconia nanopowder without impurity ions via water washing/alcohol washing. The results show that zirconia nanopowder with a narrow particle size distribution and a median size (D50) of 158 nm can be obtained at a mass ratio of P123 to zirconia of 80% and calcination temperature of 1 100 ℃. This method could be used as an environmentally friendly and efficient approach for the preparation of the nanopowder

zirconia  /  polyethylene oxide-polypropylene oxide-polyethylene oxide  /  nanopowder  /  disperse  /  isolate
王洋, 汪其堃, 汪超, 汪永清, 杨柯, 常启兵. 辅助溶胶-凝胶法制备纳米氧化锆粉体. 硅酸盐学报, 2020 , 48 (1) : 53 -60 . DOI: 10.14062/j.issn.0454-5648.20190284
Yang WANG, Qikun WANG, Chao WANG, Yongqing WANG, Ke YANG, Qibing CHANG. Preparation of Zirconia Nanopowder by Sol-gel Method[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (1) : 53 -60 . DOI: 10.14062/j.issn.0454-5648.20190284
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  • 国家自然科学基金(51262020; 51772136; 21761015)
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doi: 10.14062/j.issn.0454-5648.20190284
  • 接收时间：2019-04-29
  • 首发时间：2026-10-29
  • 出版时间：2020-01-20
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  • 收稿日期：2019-04-29
  • 修回日期：2019-07-10
基金
国家自然科学基金(51262020; 51772136; 21761015)
作者信息
    景德镇陶瓷大学材料科学与工程学院，江西 景德镇 333403

通讯作者:

常启兵（1978—），男，博士，教授。
汪其堃（1992—），男，博士研究生。
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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