Article(id=1320090126689095967, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20240635, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1727625600000, receivedDateStr=2024-09-30, revisedDate=1735056000000, revisedDateStr=2024-12-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1792663612290, onlineDateStr=2026-10-22, pubDate=1745078400000, pubDateStr=2025-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792663612290, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792663612290, creator=13701087609, updateTime=1792663612290, updator=13701087609, issue=Issue{id=1320090116236882876, tenantId=1146029695717560320, journalId=1263187385517883426, year='2025', volume='53', issue='4', pageStart='733', pageEnd='1030', issueExtLink='null', onlineDate='null', pubDate='1745078400000', pubDateStr='2025-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792663609799, creator='13701087609', updateTime=1792663788359, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1320090865276670951, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1320090865276670952, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=816, endPage=827, ext={EN=ArticleExt(id=1320090127146275104, articleId=1320090126689095967, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Impact of Calcination Condition on Phase Composition and Carbonation Reactivity of Wollastonite, columnId=1321897768591937660, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on the 14th Inorganic and Non-metallic Materials Conference—Research Article, runingTitle=null, highlight=null, articleAbstract=
Introduction Cement industry continues to face significant environmental challenges due to its substantial CO2 emissions, primarily stemming from carbonate decomposition in raw materials and fossil fuel combustion during production. Carbonatable binders and carbonation curing technologies have a promising potential for CO2 reduction in cement production, and the existing methods involve the calcination of calcareous and siliceous raw materials to produce low-lime silicates for their emission reduction limits. Natural wollastonite, primarily composed of calcium silicate (CS), has an attractive alternative due to its abundant reserves and ease of extraction. Utilizing natural wollastonite as a carbonatable binder can eliminate both fossil fuel combustion and the need for calcareous raw materials, thereby avoiding the carbonate decomposition entirely. However, its application is currently limited due to its low carbonation reactivity. This study was to investigate the enhancement of carbonation reactivity of natural wollastonite via optimizing calcination activation to develop a high-performance carbonatable binder.
Methods Natural wollastonite was calcinated under various calcination activation condictions (i.e., temperature, time, and cooling regimes). The activated wollastonite powder was mixed with water and compressed at 4 MPa to form the samples with different two dimensions (i.e., 20 mm × 20 mm × 20 mm and 20 mm × 80 mm × 20 mm). These samples underwent carbonation curing for 24 h before characterization. The mechanical properties were evaluated through compressive and flexural strength tests. The phase composition was characterized by X-ray diffraction (XRD) on both the wollastonite powder and carbonated samples before and after calcination activation. The structure of the samples was determined by Fourier-transform infrared spectroscopy (FT-IR) to analyze both the calcination activation effects and the resulting carbonation products. The microstructural evolution was determined by scanning electron microscopy (SEM). CO2 uptakes were analyzed by thermogravimetric analysis (TGA).
Results and discussion This study reveals that calcination activation significantly enhances the carbonation hardening performance of natural wollastonite via increasing carbonation reactivity. Optimal conditions are identified at a calcination temperature of 1200 ℃, effectively transforming Para-CS and β-CS into metastable α-CS. The effective calcination time for the complete transformation is 60 min, while preserving the material valuable fibrous structure. Water quenching is found to be the most effective cooling method, retaining higher concentrations of crystal defects in the metastable α-CS. The transformation from a chain structure to a ternary ring structure at 1200 ℃ results in an increased structural distortion, thus leading to an enhanced carbonation reactivity of α-CS. The carbonation analysis reveals the extensive formation of carbonation products, primarily calcium carbonate and highly polymerized silica gel, resulting in a dense microstructure. Note that the preservation of the fibrous structure through calcination activation allows unreacted wollastonite to serve as a fibrous reinforcement within the carbonation hardening system, contributing to enhanced mechanical properties.
Conclusions The results showed that calcination temperature exhibited a dominant effect, followed by calcination time and cooling regime. The optimal calcination temperature of 1200 ℃ led to the improvements in compressive strength, flexural strength, and CO2 uptakes of the carbonated samples. The calcination time was critical in ensuring a complete phase transformation, while maintaining structural integrity, and a rapid cooling could preserve crystal defects that enhanced carbonation reactivity. The resulting carbonatable binder developed a carbonation hardening system comprising calcium carbonate, highly polymerized silica gel, and unreacted wollastonite fibers that could serve as an effective reinforcement within the carbonation hardening system. These findings could provide a promising pathway for the large-scale utilization of natural wollastonite in sustainable construction materials, having a potential for reducing the environmental impact of cement industry.
, authors=Songhui LIU, Donglin LI, Xinyu ZHANG, Genshen LI, Jianping ZHU, Xuemao GUAN, authorsList=Songhui LIU, Donglin LI, Xinyu ZHANG, Genshen LI, Jianping ZHU, Xuemao GUAN, authorCompany=null, correspAuthors=Genshen LI, authorNote=
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水泥行业CO2排放量居高不下，开发低钙固碳胶凝材料已成为全球研究热点之一。以天然硅灰石（CS）为原材料，通过煅烧活化制备了一种以纤维状介稳态硅灰石（α-CS）为主的高碳化活性固碳胶凝材料。系统研究了煅烧温度、煅烧时间、冷却制度对该材料的物相组成、微观结构、碳化硬化性能、CO2封存能力等的影响。研究发现，1200 ℃的煅烧温度能够使得天然硅灰石中的Para-CS和β-CS转变为具有更高碳化活性的α-CS，α-CS的含量可达68.58%，60 min的煅烧时间确保了天然硅灰石发生充分转变且保留其独特的纤维状结构特征，而淬水冷却则保留了更多的晶体缺陷，进一步提升碳化活性。煅烧活化后，固碳胶凝材料的抗压强度、抗折强度以及CO2吸收量分别提升1333%、680%和92%，达到80.11、9.13 MPa和14.15%。通过优化煅烧活化工艺可显著提升天然硅灰石的碳化活性，为开发高性能固碳胶凝材料提供了新思路，对降低水泥行业CO2排放具有重要意义。
, authors=刘松辉, 李东林, 张欣雨, 李根深, 朱建平, 管学茂, authorsList=刘松辉, 李东林, 张欣雨, 李根深, 朱建平, 管学茂, authorCompany=null, correspAuthors=李根深, authorNote=
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李根深（1993—），男，博士，副教授。
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刘松辉（1991—），男，博士，副教授。
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