Article(id=1320090120900948967, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20240695, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1730390400000, receivedDateStr=2024-11-01, revisedDate=1731859200000, revisedDateStr=2024-11-18, acceptedDate=null, acceptedDateStr=null, onlineDate=1792663610911, onlineDateStr=2026-10-22, pubDate=1745078400000, pubDateStr=2025-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792663610911, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792663610911, creator=13701087609, updateTime=1792663610911, updator=13701087609, issue=Issue{id=1320090116236882876, tenantId=1146029695717560320, journalId=1263187385517883426, year='2025', volume='53', issue='4', pageStart='733', pageEnd='1030', issueExtLink='null', onlineDate='null', pubDate='1745078400000', pubDateStr='2025-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792663609799, creator='13701087609', updateTime=1792663788359, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1320090865276670951, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1320090865276670952, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320090116236882876, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=769, endPage=777, ext={EN=ArticleExt(id=1320090121102275560, articleId=1320090120900948967, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of SrO(SrTiO
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2 Thermoelectric Ceramics and Their Infrared Emission Properties, columnId=1321897768591937660, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on the 14th Inorganic and Non-metallic Materials Conference—Research Article, runingTitle=null, highlight=null, articleAbstract=
Introduction SrO(SrTiO3)2 (Hereinafter referred to as Sr3Ti2O7) is a layered perovskite-like structural material, which can be considered as a SrTiO3 superlattice interspersed with SrO layers. Compared to SrTiO3, Sr3Ti2O7 exhibits higher asymmetry and more significant dipole moment changes, thus providing a broader space for infrared radiation performance regulation. Also, the interface between SrO layer and SrTiO3 layer enhances phonon scattering, significantly reducing the thermal conductivity of electron-doped Sr3Ti2O7, compared to cubic SrTiO3. For the high-temperature stability and environmental friendliness of Sr3Ti2O7, there is a motivation to explore the relationship between its thermoelectric transport properties and infrared radiation properties to develop novel multifunctional materials. However, little researches on the intrinsic relationship between these two properties in Sr3Ti2O7 have been reported. Exploring the relationship between thermoelectric and infrared radiation properties and further studying the combination of thermoelectric materials with infrared materials can enhance the conversion efficiency and functional applications of thermoelectric materials, driving technological development and innovation, and open new avenues for applications in environmental monitoring, energy management, and efficient detection across multiple fields.
Methods SrCO3, TiO2, Nb2O3, and Gd2O3 were mixed as raw materials with an appropriate amount of alcohol according to a specific molar ratio. The mixed powder was ground in a ball mill for 1.5 h. Afterwards, the prepared raw powder in a mold was pressed by an electric press at 3.0 MPa for 2.0 min, and then demold. The pressed pellets were tightly wrapped with a plastic wrap and pressed by cold isostatic pressing at 39.5-44.5 MPa for 8.0 min. Afterwards, the sample wrapped in carbon paper was placed in an alumina crucible. The sample in carbon powder was heated in a muffle furnace at 1200 ℃ for 5.0 h. The sintered pellets were ground into a powder. The powder was pressed in an electric press at 5.0 MPa for 1.5 min, and then by cold isostatic pressing again at 39.5-44.5 MPa for 8.0 min. The pellets wrapped in carbon paper were buried in carbon powder and heated in the muffle furnace at 1500 ℃ for 10.0 h to obtain the final sample.
Results and discussion The XRD patterns of (Sr0.8Gd0.2)3(Ti1-xNbx)2O7 (0.01≤x≤0.05) show that the samples are similar to the standard material of Sr3Ti2O7, with a small amount of Gd2O3 phase. The most intense peak shifts between the planes (105) and (110), indicating that Nb doping affects the phase composition. As Nb doping increases, the XRD peak positions between 31° and 33° shift to lower angles due to the lattice distortion caused by Nb5+ with the radius of 0.690 Å substituting for Ti4+ with the radius of 0.605 Å. The SEM image reveals that a small amount of Nb doping (1%, in mole) improves the density, but higher doping levels increase the porosity and reduce the density.
The electrical conductivity of the sample decreases with increasing temperature. The maximum electrical conductivity for the sample doped with 1% (in mole) Nb can be obtained, which can be enhanced by 503% at 340 K and 95% at 973 K, compared to undoped samples. The Seebeck coefficient of Gd20Nb1 significantly reduces, while the power factors of Gd20Nb1 and Gd20Nb2 are similar at high temperatures. The thermal diffusivity, lattice thermal conductivity, and total thermal conductivity all decrease with increasing temperature. The sample Gd20Nb1 exhibits the maximum thermal conductivity, while the sample Gd20Nb5 reaches the minimum value of 1.4 W·m-1·K-1 at 973 K. The zT value is maximum at 0.19 for the sample doped with 2% (in mole) Nb, which is primarily affected by the power factor. A lower thermal diffusivity of the sample Gd20Nb2 resulted in a lower thermal conductivity, compared to the sample Gd20Nb1, achieving the maximum zT value.
The Nb-doped samples show an intense infrared absorption in the range of 8-14 μm, as the infrared emissivity increases with temperature due to the enhanced carrier scattering. At 973 K, the infrared emissivity of the sample Gd20Nb1 reaches 95% in the range of 8-14 μm, indicating potential applications in high-temperature protective coatings. This demonstrates a promising potential for simultaneous tuning of thermoelectric and infrared properties, thus offering some possibilities for Sr3Ti2O7-based materials in radiation heat shielding and other fields.
Conclusions Gd/Nb co-doped Sr3Ti2O7 ceramics were synthesized by a solid-state method. The influence of Nb doping concentration on the thermoelectric transport and infrared radiation properties as well as the interrelationship between these properties were analyzed. The results showed that a small amount of Nb doping significantly enhanced the electrical conductivity of the material, and the zT value reached an optimal 0.19 at 973 K when the Nb doping concentration reached 2% (in mole). Furthermore, the Nb-doped samples exhibited an intense absorption in the 8-14 μm range, and their infrared emissivity increased with the increase of the power factor and zT value. At 973 K, the sample Gd20Nb1 achieved the maximum average infrared emissivity of ~95% in the 8-14 μm atmospheric window. The sample Gd20Nb5 had the minimum thermal conductivity of ~1.4 W·m-1·K-1. The results revealed the the synergistic effects of Sr3Ti2O7-based ceramics on the thermoelectric and infrared radiation properties, demonstrating their application potential in radiant heat protection and high infrared emissivity materials. This study could provide important references for the further optimization and design of novel thermoelectric and infrared materials.
, authors=Yaqian DU, Haodong LIU, Meina MENG, Jianbo LI, Jun WANG, authorsList=Yaqian DU, Haodong LIU, Meina MENG, Jianbo LI, Jun WANG, authorCompany=null, correspAuthors=Jun WANG, authorNote=
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2热电陶瓷的制备及其红外发射性能, columnId=1321897768759709821, journalTitle=硅酸盐学报, columnName=第14届无机非金属材料专题研讨会专题—研究论文, runingTitle=null, highlight=null, articleAbstract=
相较于经典钙钛矿材料SrTiO3，层状钙钛矿结构SrO（SrTiO3）2表现出较低的热导率和较高的热膨胀系数，在辐射热防护等军事领域具有更大的应用潜力。前期工作证明热电效应和辐射性能具有一定的联系，然而目前关于SrO（SrTiO3）2两种性能内在联系的报道较少。采用固相法合成了Gd/Nb共掺杂的SrO（SrTiO3）2陶瓷，分析了Nb掺杂浓度对其热电输运性能和红外发射率的影响，以及这些性能之间的相互关系。研究发现，少量Nb元素的掺杂显著提高材料的电导率，其中2%（摩尔分数）Nb掺杂样品的zT值在973 K时可达0.19。Nb掺杂的SrO（SrTiO3）2样品在8~14 μm波段表现出强吸收，其红外发射率随功率因子和zT值的增大而增大。973 K时，8~14 μm大气窗口内1%Nb掺杂样品的平均红外发射率达到最高~95%。5%Nb掺杂样品热导率达到最低~1.4 W·m-1·K-1。该研究为进一步优化设计兼具热电和红外性能的新型材料提供了可能性。
, authors=杜雅倩, 刘昊东, 孟美娜, 李建波, 王俊, authorsList=杜雅倩, 刘昊东, 孟美娜, 李建波, 王俊, authorCompany=null, correspAuthors=王俊, authorNote=
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王俊（1982—），男，博士，教授。
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