Article(id=1320089977522868779, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320089968630944199, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20240837, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1735315200000, receivedDateStr=2024-12-28, revisedDate=1736524800000, revisedDateStr=2025-01-11, acceptedDate=null, acceptedDateStr=null, onlineDate=1792663576726, onlineDateStr=2026-10-22, pubDate=1750348800000, pubDateStr=2025-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792663576726, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792663576726, creator=13701087609, updateTime=1792663576726, updator=13701087609, issue=Issue{id=1320089968630944199, tenantId=1146029695717560320, journalId=1263187385517883426, year='2025', volume='53', issue='6', pageStart='1403', pageEnd='1776', issueExtLink='null', onlineDate='null', pubDate='1750348800000', pubDateStr='2025-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792663574607, creator='13701087609', updateTime=1792663739055, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1320090658786881616, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320089968630944199, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1320090658786881617, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320089968630944199, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1469, endPage=1477, ext={EN=ArticleExt(id=1320089977791304236, articleId=1320089977522868779, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Application and Prospects of Synchrotron X-Ray Technology for All-Solid-State Batteries, columnId=1321945714683392392, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Development of All-Solid-State Batteries—Review, runingTitle=null, highlight=null, articleAbstract=
All-solid-state batteries (ASSBs) emerge as a current research hotspot due to their high safety, extended cycle life, and elevated energy density. Understanding the intrinsic relationship between the structure and performance of solid electrolytes (SEs), along with interfacial charge transport properties, is crucial for the stable operation of ASSBs. Synchrotron radiation (SR) technology provides a significant support for analyzing the composition-structure-performance relationship in ASSBs due to its high brightness and adjustable energy. It is especially applicable to investigate the dynamic evolution of materials and interfaces, charge migration, and failure mechanisms during battery cycling.
The review outlines the classification, principles, and applications of synchrotron radiation X-ray (SR-X) technologies, i.e., synchrotron X-ray diffraction (SXRD), X-ray absorption spectroscopy (XAS), synchrotron X-ray photoelectron spectroscopy (SXPS), and synchrotron X-ray microscopy (SXM). The focus is on the advantages of SR in elucidating local structures, chemical states, and microstructures.
The review also represents the applications and progress of SR-X in ASSBs. Initially, it highlights progress on using SR-X to explore the composition-structure-property relationships in SEs and monitor structural evolution and charge mobility during ASSB operation. The review represents the use of SR-X in detecting SEs/interfaces, examining changes in interface structure, composition, and morphology during battery cycling, with a focus on SEs/cathode and SEs/anode interfaces.
Summary and prospects This review represents recent advancements in the application of SR-X techniques for studying SEs and their interfaces, emphasizing their unique capabilities in resolving local structures, chemical states, coordination environments, and interfacial heterogeneities, while elucidating the failure mechanisms of ASSBs. To advance the practical implementation of ASSBs, the future development on SR-X technology should focus on three key areas, i.e., 1) Advancing in-situ SR-X techniques with higher temporal and spatial resolution. Real-time monitoring of the dynamic evolution of solid-solid interfaces during battery operation is essential for capturing transient phenomena in chemical and electrochemical reactions. An atomic-scale resolution will enable a detailed investigation of microstructural and chemical properties, particularly for sensitive elements like Li and Na. 2) Integrating SR-X with complementary techniques for multiscale analysis. Combining methods such as SXM and XAFS can provide synergistic insights into the microstructure and chemical composition of materials, offering a comprehensive understanding of both heterogeneous and average properties in ASSB components. 3) Developing in-situ electrochemical cell designs compatible with SR-X techniques. These configurations should ensure sufficient signal strength for characterizing material components and interfaces, while maintaining a typical electrochemical behavior under synchrotron beamline conditions. Advancing these aspects will unlock the full potential of SR-X techniques, driving the commercial viability of ASSBs.
, authors=Meng WU
1, Yang LI
1, Hong LIU
2, Xun WANG
1, Lizhen FAN
1, authorsList=Meng WU, Yang LI, Hong LIU, Xun WANG, Lizhen FAN, authorCompany=null, correspAuthors=Lizhen FAN, authorNote=
, correspAuthorsNote=
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1320089978051351085, articleId=1320089977522868779, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=同步辐射X射线技术在全固态电池中的应用与展望, columnId=1321945714859553161, journalTitle=硅酸盐学报, columnName=全固态电池发展专刊—综合评述, runingTitle=null, highlight=null, articleAbstract=
同步辐射（SR）技术因其高亮度、高时空分辨率及能量可调等优势，为解析全固态电池（ASSBs）内在材料组成-结构-性能间构效关系提供了强有力的技术支撑，尤其涉及电池充放电循环过程中材料及界面结构的动态演化、电荷迁移特性及电池失效机制等。本文首先介绍了SR的基本原理、技术分类及其功能应用。其次，系统综述了近年来SR技术在ASSBs领域的应用和研究进展。重点总结和评述了同步辐射X射线（SR-X）技术在解析无机固体电解质材料结构、离子传输机制及固-固界面失效分析等方面的研究应用。最后展望了SR技术在促进ASSBs实用化进程中的研究重点和发展方向。
, authors=武猛
1, 李洋
1, 刘洪
2, 王寻
1, 范丽珍
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范丽珍（1975—），女，博士，教授。
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