Article(id=1319987077320655316, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210626, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1627574400000, receivedDateStr=2021-07-30, revisedDate=1629820800000, revisedDateStr=2021-08-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639043407, onlineDateStr=2026-10-22, pubDate=1647705600000, pubDateStr=2022-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639043407, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639043407, creator=13701087609, updateTime=1792639043407, updator=13701087609, issue=Issue{id=1319986978137944236, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='3', pageStart='555', pageEnd='876', issueExtLink='null', onlineDate='null', pubDate='1647705600000', pubDateStr='2022-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792639019760, creator='13701087609', updateTime=1792639223744, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319987833767575858, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319987833767575859, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=735, endPage=741, ext={EN=ArticleExt(id=1319987077542953429, articleId=1319987077320655316, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Reactive Flash Sintering of BiFeO3-BaTiO3 Ceramics, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Rapid preparation of dense BiFeO3-BaTiO3 lead-free piezoelectric ceramics at low temperatures is beneficial to preventing the Bi volatilization, reducing the energy consumption and developing novel materials with some unique properties. In this paper, dense BiFeO3-BaTiO3 ceramics with good ferroelectric and piezoelectric properties were prepared in an electric field of 200 V/cm with a current limit of 280 mA via reactive flash sintering of multiphase precursor powders (i.e., Bi2O3, Fe2O3, TiO2 and BaCO3) at 415 ℃ for 30 s. The solid-state reaction in sintering occurs during the flash event. The current limit has an effect on the phase transformation and densification. It is indicated that the reactive flash sintering technology could prepare the single-phase and dense ceramic material through flash sintering of starting precursors in one step, thus providing an effective approach for the rapid production of ceramic materials.

, authors=Gai AN, Zhihua JIAO, Mengying FU, Xinghua SU, authorsList=Gai AN, Zhihua JIAO, Mengying FU, Xinghua SU, authorCompany=null, correspAuthors=Xinghua SU, authorNote=

AN Gai (1996-), male, Master candidate.

, correspAuthorsNote=
SU Xinghua (1981-), male, Ph.D., Professor. E-mail:
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BiFeO3-BaTiO3陶瓷的低温快速烧结致密化有助于抑制Bi元素的挥发,降低能耗以及快速筛选出具有优异电学性能的BiFeO3-BaTiO3基陶瓷材料。在200 V/cm的直流电场和280 mA的限制电流作用下,通过反应闪烧Bi2O3、Fe2O3、TiO2和BaCO3混合粉体,能够在415 ℃的炉温下,30 s内获得具有良好铁电及压电性能的致密BiFeO3-BaTiO3陶瓷。反应闪烧过程中,固相化学反应和烧结致密化同时发生;限制电流值的大小对样品的相变和致密化程度有重要影响。反应闪烧技术可通过一步闪烧陶瓷材料的前驱体混合粉末而获得单相且致密的陶瓷材料,为陶瓷材料的快速制备提供了一个新的途径。

, authors=安盖, 焦智华, 付梦莹, 苏兴华, authorsList=安盖, 焦智华, 付梦莹, 苏兴华, authorCompany=null, correspAuthors=苏兴华, authorNote=

安盖(1996—),男,硕士研究生。

, correspAuthorsNote=
苏兴华(1981—),男,博士,教授。
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安盖(1996—),男,硕士研究生。

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反应闪烧技术制备BiFeO3-BaTiO3陶瓷
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安盖 , 焦智华 , 付梦莹 , 苏兴华
硅酸盐学报 | 研究论文 2022,50(3): 735-741
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反应闪烧技术制备BiFeO3-BaTiO3陶瓷
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安盖, 焦智华, 付梦莹, 苏兴华
作者信息
  • 长安大学材料科学与工程学院,西安 710061
通讯作者:
苏兴华(1981—),男,博士,教授。
作者简介:

安盖(1996—),男,硕士研究生。

Reactive Flash Sintering of BiFeO3-BaTiO3 Ceramics
Gai AN, Zhihua JIAO, Mengying FU, Xinghua SU
Affiliations
  • School of Materials Science and Engineering, Chang'an University, Xi'an 710061, China
  • Corresponding Author:
    SU Xinghua (1981-), male, Ph.D., Professor. E-mail:

    AN Gai (1996-), male, Master candidate.

出版时间: 2022-03-20 doi: 10.14062/j.issn.0454-5648.20210626
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BiFeO3-BaTiO3陶瓷的低温快速烧结致密化有助于抑制Bi元素的挥发,降低能耗以及快速筛选出具有优异电学性能的BiFeO3-BaTiO3基陶瓷材料。在200 V/cm的直流电场和280 mA的限制电流作用下,通过反应闪烧Bi2O3、Fe2O3、TiO2和BaCO3混合粉体,能够在415 ℃的炉温下,30 s内获得具有良好铁电及压电性能的致密BiFeO3-BaTiO3陶瓷。反应闪烧过程中,固相化学反应和烧结致密化同时发生;限制电流值的大小对样品的相变和致密化程度有重要影响。反应闪烧技术可通过一步闪烧陶瓷材料的前驱体混合粉末而获得单相且致密的陶瓷材料,为陶瓷材料的快速制备提供了一个新的途径。

铁酸铋-钛酸钡  /  无铅压电陶瓷  /  反应闪烧  /  相变  /  致密化

Rapid preparation of dense BiFeO3-BaTiO3 lead-free piezoelectric ceramics at low temperatures is beneficial to preventing the Bi volatilization, reducing the energy consumption and developing novel materials with some unique properties. In this paper, dense BiFeO3-BaTiO3 ceramics with good ferroelectric and piezoelectric properties were prepared in an electric field of 200 V/cm with a current limit of 280 mA via reactive flash sintering of multiphase precursor powders (i.e., Bi2O3, Fe2O3, TiO2 and BaCO3) at 415 ℃ for 30 s. The solid-state reaction in sintering occurs during the flash event. The current limit has an effect on the phase transformation and densification. It is indicated that the reactive flash sintering technology could prepare the single-phase and dense ceramic material through flash sintering of starting precursors in one step, thus providing an effective approach for the rapid production of ceramic materials.

bismuth ferrite-Barium titanate  /  lead-free piezoelectric ceramics  /  reactive flash sintering  /  phase transformation  /  densification
安盖, 焦智华, 付梦莹, 苏兴华. 反应闪烧技术制备BiFeO3-BaTiO3陶瓷. 硅酸盐学报, 2022 , 50 (3) : 735 -741 . DOI: 10.14062/j.issn.0454-5648.20210626
Gai AN, Zhihua JIAO, Mengying FU, Xinghua SU. Reactive Flash Sintering of BiFeO3-BaTiO3 Ceramics[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (3) : 735 -741 . DOI: 10.14062/j.issn.0454-5648.20210626
  • 陕西省重点研发计划项目(2021GY-250)
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doi: 10.14062/j.issn.0454-5648.20210626
  • 接收时间:2021-07-30
  • 首发时间:2026-10-22
  • 出版时间:2022-03-20
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  • 收稿日期:2021-07-30
  • 修回日期:2021-08-25
基金
陕西省重点研发计划项目(2021GY-250)
作者信息
    长安大学材料科学与工程学院,西安 710061

通讯作者:

苏兴华(1981—),男,博士,教授。
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种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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