Article(id=1319987019720274400, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210478, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1623340800000, receivedDateStr=2021-06-11, revisedDate=1627401600000, revisedDateStr=2021-07-28, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639029673, onlineDateStr=2026-10-22, pubDate=1647705600000, pubDateStr=2022-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639029673, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639029673, creator=13701087609, updateTime=1792639029673, updator=13701087609, issue=Issue{id=1319986978137944236, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='3', pageStart='555', pageEnd='876', issueExtLink='null', onlineDate='null', pubDate='1647705600000', pubDateStr='2022-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792639019760, creator='13701087609', updateTime=1792639223744, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319987833767575858, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319987833767575859, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=782, endPage=790, ext={EN=ArticleExt(id=1319987019896435169, articleId=1319987019720274400, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Optimisation of Ammonium Sulphate Crystallization Based on Response Surface Methodology, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The influences of pH value, Fe³⁺ mass concentration, and stirring rate and their interactions on the ammonium sulfate crystallization were investigated via cooling crystallization and sieving based on a response surface methodology. An average particle size quadratic orthogonal model and a variation coefficient 2FI orthogonal model were proposed. The interactions among the various factors were analyzed. The results show that pH value (A) > stirring rate (C) > Fe³⁺ ions concentration (B) is a decreased order for the parameter effects on the average particle size and variation coefficient. Their interactions have a decreased effect order (i.e., AC >BC > AB) on the average particle size and variation coefficient. When pH value is 5.5, stirring rate is 150 r/min, and Fe³⁺ ions concentration is 0.3 g/L, the average particle size and variation coefficient of the ideal crystals is 0.985 mm and 793.719, respectively.

, authors=Rui LI¹, Yonghua JIANG¹, Yanling ZHANG¹, Kunqing CHEN¹, Bangfu HUANG², Lu LI², authorsList=Rui LI, Yonghua JIANG, Yanling ZHANG, Kunqing CHEN, Bangfu HUANG, Lu LI, authorCompany=null, correspAuthors=Bangfu HUANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319987020164870626, articleId=1319987019720274400, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=基于响应曲面法优化硫酸铵结晶, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

采用冷却结晶和筛分法研究了响应曲面法设计下pH值、Fe³⁺浓度、搅拌速率各因素不同水平对平均粒径和变异系数影响程度，构建了平均粒径2次回归模型和C·V·值2FI回归模型，深入探究了各影响因素之间交互作用，研究表明：各因素对平均粒径和C·V·值影响程度为母液pH>搅拌速率>Fe³⁺质量浓度；各因素之间交互作用对晶体平均粒径和C·V·值影响程度为AC >BC >AB；当母液pH为5.5、搅拌速率为150 r/min、Fe³⁺质量浓度为0.3 g/L时，可得到平均粒径为0.985 mm、C·V·为793.719的晶体；经验证模型值与实验值误差较小，回归模型具有良好拟合度和可靠性。

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LI Rui (1973-), male, Undergraduate, Senior Engineer. E-mail: snjc-lr@ynkg.com

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LI Rui (1973-), male, Undergraduate, Senior Engineer. E-mail: snjc-lr@ynkg.com

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李锐（1973—），男，本科，高级工程师。

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李锐（1973—），男，本科，高级工程师。

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