Article(id=1319987001244365108, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210500, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1624291200000, receivedDateStr=2021-06-22, revisedDate=1625587200000, revisedDateStr=2021-07-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639025268, onlineDateStr=2026-10-22, pubDate=1647705600000, pubDateStr=2022-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639025268, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639025268, creator=13701087609, updateTime=1792639025268, updator=13701087609, issue=Issue{id=1319986978137944236, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='3', pageStart='555', pageEnd='876', issueExtLink='null', onlineDate='null', pubDate='1647705600000', pubDateStr='2022-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792639019760, creator='13701087609', updateTime=1792639223744, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319987833767575858, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319987833767575859, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986978137944236, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=704, endPage=712, ext={EN=ArticleExt(id=1319987001466663221, articleId=1319987001244365108, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Mechanism of Alumina Ceramics with Ag-CuO-B₂O₃ Filler via Reactiver Air Brazing, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Alumina ceramics were joined with Ag-10CuO-10B₂O₃ filler via reactiver air brazing for the formation of whiskers (Cu₂Al₆B₄O₁₇) in the joints. The effects of brazing temperature and holding time on the microstructure, properties of the joints and the whisker structure were investigated. The results show that Al₂O₃ reacts with CuO and B₂O₃ to form Cu₂Al₆B₄O₁₇ whiskers in the brazing process, thus obtaining a reliable joint with the superior performance. At the holding time of 60 min and the brazing temperature of > 950 ℃, an effective connection of Al₂O₃ ceramic joint can be realized. The center area of the brazing joint is mainly Ag, while the interface at the both sides of the joint is composed of CuO、Cu₃B₂O₆ phase and Cu₂Al₆B₄O₁₇ whiskers. The shear strength of the joint increases with the increase of the brazing temperature. The whiskers become thick and the adhesion occurs when the brazing temperature is > 1 050 ℃, thus reducing the strengthening effect on the joint and the shear strength of the joint. The whiskers decompose into some lamellar products, and the shear strength of the joint decreases when the brazing temperature is >1 100 ℃. The shear strength of the joint prepared under optimum process parameters (i.e., at 1 000 ℃ for 60 min) can reach 86.7 MPa, and the fracture occurs in the weld nearby alumina ceramic base material.

, authors=Xinyue LI¹, Jian LI^{1, 2}, Jiankang ZHANG³, Panpan LIN¹, Tiesong LIN¹, Peng HE¹, authorsList=Xinyue LI, Jian LI, Jiankang ZHANG, Panpan LIN, Tiesong LIN, Peng HE, authorCompany=null, correspAuthors=Panpan LIN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319987001684767030, articleId=1319987001244365108, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Ag-CuO-B₂O₃钎料空气反应钎焊连接Al₂O₃陶瓷机理, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以Ag-CuO-B₂O₃为钎料，采用空气反应钎焊法连接了Al₂O₃陶瓷，在接头中合成了新型Cu₂Al₆B₄O₁₇晶须。研究了连接温度与保温时间对接头显微结构、性能以及生成的晶须结构的影响。结果表明：钎焊过程中，Al₂O₃与钎料中的CuO、B₂O₃发生反应生成Cu₂Al₆B₄O₁₇晶须，获得性能优异的可靠接头。保温时间为60 min、连接温度高于950 ℃时，可以实现Al₂O₃陶瓷接头的有效连接，钎缝中心区主要为Ag，靠近连接界面处为CuO、Cu₃B₂O₆相及Cu₂Al₆B₄O₁₇晶须。随着连接温度的升高，接头的抗剪强度升高。连接温度高于1 050 ℃后，晶须变得粗大，出现黏接，对接头的强化效果减弱，接头的抗剪强度降低。连接温度高于1 100 ℃后，晶须分解为片层状产物，接头的抗剪强度大幅降低。最佳工艺参数为在1 000 ℃条件下保温60 min，接头的抗剪强度可达86.7 MPa，断裂发生在焊缝中靠近母材处。

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LI Xinyue(1998-), female, Master candidate. E-mail: lxy13604066725@163.com

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李昕悦（1998—），女，硕士研究生。

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李昕悦（1998—），女，硕士研究生。

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