Article(id=1319986893069070969, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210624, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1627660800000, receivedDateStr=2021-07-31, revisedDate=1635696000000, revisedDateStr=2021-11-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1792638999477, onlineDateStr=2026-10-22, pubDate=1652976000000, pubDateStr=2022-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792638999477, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792638999477, creator=13701087609, updateTime=1792638999477, updator=13701087609, issue=Issue{id=1319986871980118160, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='5', pageStart='1201', pageEnd='1454', issueExtLink='null', onlineDate='null', pubDate='1652976000000', pubDateStr='2022-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792638994450, creator='13701087609', updateTime=1792639285419, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988092451275233, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988092451275234, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1325, endPage=1334, ext={EN=ArticleExt(id=1319986893278786170, articleId=1319986893069070969, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Hydrophobic Silica Aerogel with High Thermal Stability by Argon Atmosphere Heat Treatment, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Improving the thermal stability of silica (SiO₂) aerogel plays a crucial role in expanding its heat insulation application. In this work, heat treatment in argon atmosphere was adopted to avoid the thermal oxidative decomposition of hydrophobic groups, which inevitably occurred in the heat treatment in air atmosphere. Also, the physicochemical properties were analyzed. The results show that the hydrophobicity of SiO₂ aerogels still maintains at a contact angle of 140° after heat treatment in argon atmosphere at 700 ℃. In the differential scanning calorimetry test in air atmosphere, the peak temperature in exothermic reaction (T_peak) of heat treated SiO₂ aerogels reaches 584 ℃, which is approximately 300 ℃ higher than that of untreated SiO₂ aerogels, thus improving the thermal stability. The results obtained also indicate that hydrophobic SiO₂ aerogels could be used at high temperatures due to the improved thermal stability and safety.

, authors=Zhi LI¹, Yunmeng DENG¹, Yang WANG¹, Bing DU¹, Ming LI¹, Qiong LIU¹, Xudong CHENG², authorsList=Zhi LI, Yunmeng DENG, Yang WANG, Bing DU, Ming LI, Qiong LIU, Xudong CHENG, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986893643690619, articleId=1319986893069070969, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=氩气热处理制备高热稳定性疏水SiO₂气凝胶, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

提高疏水SiO₂气凝胶的热稳定性对拓展其保温隔热应用具有重大意义。为了避免空气氛围下热处理对疏水基团造成的热氧化分解，采用氩气氛围对疏水SiO₂气凝胶进行热处理，达到调控其热稳定性的目的。结果表明：经氩气氛围700 ℃热处理后，SiO₂气凝胶仍维持着良好疏水性，接触角约140°。在空气氛围下的差式扫描量热测试中，热流峰值达到584 ℃，与未热处理的疏水SiO₂气凝胶相比提高约300 ℃，热稳定性显著提高。这为提高疏水SiO₂气凝胶的热稳定性和安全性提供了新思路，奠定了疏水SiO₂气凝胶高温应用的新基础。

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LI Zhi (1989-), male, Ph.D., Associate Professor. E-mail: lizhi89@csu.edu.cn

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LI Zhi (1989-), male, Ph.D., Associate Professor. E-mail: lizhi89@csu.edu.cn

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李治（1989—），博士，副教授。

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李治（1989—），博士，副教授。

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