Article(id=1319237199506297754, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220614, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1659024000000, receivedDateStr=2022-07-29, revisedDate=1661097600000, revisedDateStr=2022-08-22, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460258603, onlineDateStr=2026-10-20, pubDate=1671465600000, pubDateStr=2022-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460258603, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460258603, creator=13701087609, updateTime=1792460258603, updator=13701087609, issue=Issue{id=1319237171312177253, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='12', pageStart='3091', pageEnd='3336', issueExtLink='null', onlineDate='null', pubDate='1671465600000', pubDateStr='2022-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460251882, creator='13701087609', updateTime=1792460721974, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319239143067071226, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319239143067071227, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3276, endPage=3283, ext={EN=ArticleExt(id=1319237199741178779, articleId=1319237199506297754, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Tailoring Inclusions and Improvement of ZnTe Crystal Quality by Annealing, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The temperature gradient solution method can effectively reduce the growth temperature of zinc telluride (ZnTe) crystal. However, it is inevitable to introduce Te inclusions in the as-grown ZnTe crystals, leading to degrading the crystal quality. In this paper, the Te inclusions under saturated Zn vapor were eliminated via both isothermal annealing and gradient annealing. The removal efficiency of Te inclusions was evaluated, which was determined by the annealing temperature and gradient. A removal efficiency of 83% is achieved via gradient annealing at 650 ℃ for 100 h. In addition, V_Te-Te_i complex defects caused by Te atoms diffusion appear in the crystal after annealing, thus affecting the crystal quality and photoelectric properties of the ZnTe crystal. Based on the X-ray double-crystal rocking curves of the ZnTe crystal, the crystal quality is generally improved when the Te inclusions are removed, indicating that the Te inclusions are a dominated factor affecting the quality of ZnTe crystal.

, authors=Han SUN¹, Zixuan JIA¹, Wenjun LI¹, Yan WANG², Yadong XU¹, authorsList=Han SUN, Zixuan JIA, Wenjun LI, Yan WANG, Yadong XU, authorCompany=null, correspAuthors=Yadong XU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319237200001225628, articleId=1319237199506297754, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=ZnTe晶体中夹杂相的退火调控与结晶质量提升, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

太赫兹技术的不断发展和在各个领域的进一步应用，对碲化锌（ZnTe）电光晶体提出越来越高的要求。采用Te溶剂法生长碲化锌晶体，可以有效降低晶体的生长温度，但不可避免的会引入Te夹杂相，进而影响其结晶质量。本工作提出利用Zn气氛等温退火和梯度退火2种方法，在不同退火温度下成功消除了ZnTe晶体内部尺寸小于10 μm的Te夹杂相，发现夹杂相去除效率与退火温度和梯度密切相关。经过650 ℃，100 h的梯度退火后，Te夹杂相去除效率可达83%。Zn气氛退火后，晶体内部出现V_Te-Te_i复合缺陷，表明退火中存在扩散导致的缺陷反应，对晶体的结晶质量和光学性能产生影响。通过对退火前后晶体的X射线摇摆曲线衍射峰的研究，发现去除Te夹杂后晶体结晶质量总体提高，证明Te夹杂相是左右ZnTe晶体结晶质量的主要结构缺陷。

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SUN Han (1996-), male, Doctoral candidate. E-mail: sunh@mail.nwpu.edu.cn

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SUN Han (1996-), male, Doctoral candidate. E-mail: sunh@mail.nwpu.edu.cn

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孙晗（1996—），男，博士研究生。

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孙晗（1996—），男，博士研究生。

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