Article(id=1319237187036631865, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220387, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1652371200000, receivedDateStr=2022-05-13, revisedDate=1653494400000, revisedDateStr=2022-05-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460255630, onlineDateStr=2026-10-20, pubDate=1671465600000, pubDateStr=2022-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460255630, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460255630, creator=13701087609, updateTime=1792460255630, updator=13701087609, issue=Issue{id=1319237171312177253, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='12', pageStart='3091', pageEnd='3336', issueExtLink='null', onlineDate='null', pubDate='1671465600000', pubDateStr='2022-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460251882, creator='13701087609', updateTime=1792460721974, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319239143067071226, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319239143067071227, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3222, endPage=3229, ext={EN=ArticleExt(id=1319237188756296506, articleId=1319237187036631865, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Sintering Process Optimization and Grain Growth Mechanism of BaBiO
3 Ceramic Targets, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=
High quality ceramic targets is crucial to produce BaBiO3-based negative temperature coefficient (NTC) thermosensitive films via RF magnetron sputtering. In this paper, the shrinkage, flatness and volume density of pure BaBiO3 target were measured, and the orthogonal experiment was designed via changing the major factors (i.e., compressive time, sintering temperature, holding time and heating rate), and the structure-activity relationship between each factor and the target material quality index was analyzed. Also, based on the influence of sintering behaviors on the grain growth of BaBiO3 ceramic targets, the key sintering process factors such as sintering temperature, holding time and heating rate were regulated by the phenomenological equation and intercept method to discuss the intrinsic relationship among the grain growth mechanism, growth index n and key influencing factors. According to the results by X-ray diffraction, Raman spectroscopy and scanning electron microscopy-enery dispersive spectroscopy, the phase structure and elemental composition of the target samples obtained at the given process factors were analyzed. The results show that BaBiO3 ceramic targets with slight deformation, high density and good apparent quality can be obtained under the optimum conditions (i.e., compressive time of 12 min, sintering temperature of 750 ℃, holding time of 120 min and heating rate of 2 ℃/min).
, authors=Jingjing QU
1, 3, Qi SU
2, Fei LIU
2, Nairui SHEN
2, Changlai YUAN
4, Xiao LIU
4, Liufang MENG
4, authorsList=Jingjing QU, Qi SU, Fei LIU, Nairui SHEN, Changlai YUAN, Xiao LIU, Liufang MENG, authorCompany=null, correspAuthors=Fei LIU, authorNote=
, correspAuthorsNote=
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3陶瓷靶材的烧制工艺优化及其晶粒生长机制, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=
高质量的陶瓷靶材对于射频磁控溅射法可镀制出综合性能优异的BaBiO3基负温度系数热敏薄膜至关重要。基于此,本工作以纯BaBiO3靶材样品的收缩率、平整度和体积密度为主要质量特性衡量指标,通过改变保压时间、烧结温度、保温时间和升温速率等4个因素,设计了正交实验并加以分析各因素与靶材质量指标的构效关系。同时,基于烧结行为对BaBiO3靶材晶粒生长的影响关系,包括调控烧结温度、保温时间和升温速率等关键烧结工艺参数,结合唯象方程和截距法,探讨了晶粒生长机制、生长指数n与关键影响因素间的内在关联性。基于此,进一步联合X射线衍射、Raman光谱、扫描电子显微镜和能谱等表征方法分析了不同工艺参数条件下靶材样品的相结构和元素构成,从而验证了正交化实验的有效性。结果表明,获得综合质量较优(变形程度小、致密度高和表观质量良好)的BaBiO3陶瓷靶材的烧制工艺为:保压时间12 min、烧结温度750 ℃、保温时间120 min和升温速率2 ℃/min。
, authors=屈婧婧
1, 3, 苏琪
2, 刘飞
2, 沈乃瑞
2, 袁昌来
4, 刘笑
4, 蒙柳方
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, correspAuthorsNote=
刘飞(1985—),男,博士,副教授。
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1, 3, address=
1.School of Electronic Engineering and Automation, Guilin University of Electronic Technology, Guilin 541004, Guangxi, China
3.Technology Department, Guilin University of Aerospace Technology, Guilin 541004, Guangxi, China, bio={"content":"
QU Jingjing (1988-), female, Ph.D., associate Professor. E-mail: qujingjing@guat.edu.cn
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QU Jingjing (1988-), female, Ph.D., associate Professor. E-mail: qujingjing@guat.edu.cn
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屈婧婧(1988—),女,博士,副教授。
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屈婧婧(1988—),女,博士,副教授。
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