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Article(id=1319236721070424312, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220172, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1646582400000, receivedDateStr=2022-03-07, revisedDate=1648224000000, revisedDateStr=2022-03-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460144535, onlineDateStr=2026-10-20, pubDate=1666195200000, pubDateStr=2022-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460144535, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460144535, creator=13701087609, updateTime=1792460144535, updator=13701087609, issue=Issue{id=1319236705027207343, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='10', pageStart='2579', pageEnd='2808', issueExtLink='null', onlineDate='null', pubDate='1666195200000', pubDateStr='2022-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460140711, creator='13701087609', updateTime=1792460672919, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319238937323884737, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319238937323884738, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2684, endPage=2691, ext={EN=ArticleExt(id=1319236721330471161, articleId=1319236721070424312, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Acetaldehyde Sensing Properties of Ti3C2Tx-WO3 Composites Synthesized by Hydrothermal Method, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The acetaldehyde vapor produced in industrial production and life needs to be monitored in real time and efficiently, WO3 nanoplates and a series of Ti3C2Tx-WO3 composite materials were synthesized by a hydrothermal method. The structure and morphology of the as-prepared materials were investigated by X-ray diffraction, scanning electron microscopy, and X-ray photoelectron spectroscopy. The gas sensing properties of materials were analyzed. The results show that the addition of Ti3C2Tx can enhance the gas sensing performance of WO3 nanoplates. The optimized gas sensing operation temperature is 80 ℃ for 7%(mass fraction) Ti3C2Tx-WO3 composite material. The sensitivity of 7% Ti3C2Tx-WO3 composite material to 100 μL/L acetaldehyde vapor at 80 ℃ is 32.9 within a low detection limit of 0.1 μL/L.

, authors=Sijie BAO1, Xin BU1, Yuying BAI1, Chunshui WANG1, Xiangfeng Chu1, Shiming LIANG2, authorsList=Sijie BAO, Xin BU, Yuying BAI, Chunshui WANG, Xiangfeng Chu, Shiming LIANG, authorCompany=null, correspAuthors=Xiangfeng Chu, Shiming LIANG, authorNote=

BAO Sijie (1997-), female, Master candidate. E-mail:

, correspAuthorsNote=
CHU Xiangfeng (1962-), male, Ph.D., Professor; E-mail:
LIANG Shiming (1983-), male, Ph.D., Lecturer.
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工业生产生活中产生的乙醛气体需要实时高效监测，利用水热法制备了WO3纳米片和一系列Ti3C2Tx-WO3复合材料。采用X射线衍射法、扫描电子显微镜、Fourier红外光谱、X射线能谱等对制备出的Ti3C2Tx-WO3复合材料进行了结构和形貌表征。对Ti3C2Tx-WO3复合材料进行了气敏性能研究，并且探究了碳化钛加入量对Ti3C2Tx-WO3复合材料气敏性能的影响。结果表明：Ti3C2Tx的加入能够有效提高WO3纳米片的气敏性能。当Ti3C2Tx的加入量在7%（质量分数）时，Ti3C2Tx-WO3复合材料的最佳工作温度优化为80 ℃。7% Ti3C2Tx-WO3材料在80 ℃时对100 μL/L的乙醛气体的灵敏度达到了32.9，最低检测限为0.1 μL/L。

, authors=鲍思洁1, 卜鑫1, 白玉莹1, 王春水1, 储向峰1, 梁士明2, authorsList=鲍思洁, 卜鑫, 白玉莹, 王春水, 储向峰, 梁士明, authorCompany=null, correspAuthors=储向峰, 梁士明, authorNote=

鲍思洁（1997—），女，硕士研究生。

, correspAuthorsNote=
储向峰（1966—），男，博士，教授；
梁士明（1983—），男，博士，讲师。
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BAO Sijie (1997-), female, Master candidate. E-mail:

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鲍思洁（1997—），女，硕士研究生。

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鲍思洁（1997—），女，硕士研究生。

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水热法制备Ti3C2Tx-WO3复合材料及其对乙醛气体的传感性能
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鲍思洁 1 , 卜鑫 1 , 白玉莹 1 , 王春水 1 , 储向峰 1 , 梁士明 2
硅酸盐学报 | 研究论文 2022,50(10): 2684-2691
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硅酸盐学报 |研究论文 2022 , 50 (10) : 2684 -2691
水热法制备Ti3C2Tx-WO3复合材料及其对乙醛气体的传感性能
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鲍思洁1 , 卜鑫1, 白玉莹1, 王春水1, 储向峰1 , 梁士明2
作者信息
  • 1．安徽工业大学化学与化工学院，安徽 马鞍山 243002
  • 2．临沂大学材料科学与工程学院，山东 临沂 276005
通讯作者:
储向峰（1966—），男，博士，教授；
梁士明（1983—），男，博士，讲师。
作者简介:

鲍思洁（1997—），女，硕士研究生。

Acetaldehyde Sensing Properties of Ti3C2Tx-WO3 Composites Synthesized by Hydrothermal Method
Sijie BAO1 , Xin BU1, Yuying BAI1, Chunshui WANG1, Xiangfeng Chu1 , Shiming LIANG2
Affiliations
  • 1.School of Chemistry and Chemical Engineering, Anhui University of Technology, Maanshan 243002, Anhui, China
  • 2.School of Materials Science and Engineering, Linyi University, Linyi 276005, Shandong, China
    • Corresponding Author:
    CHU Xiangfeng (1962-), male, Ph.D., Professor; E-mail:
    LIANG Shiming (1983-), male, Ph.D., Lecturer.

    BAO Sijie (1997-), female, Master candidate. E-mail:

出版时间: 2022-10-20 doi: 10.14062/j.issn.0454-5648.20220172
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工业生产生活中产生的乙醛气体需要实时高效监测，利用水热法制备了WO3纳米片和一系列Ti3C2Tx-WO3复合材料。采用X射线衍射法、扫描电子显微镜、Fourier红外光谱、X射线能谱等对制备出的Ti3C2Tx-WO3复合材料进行了结构和形貌表征。对Ti3C2Tx-WO3复合材料进行了气敏性能研究，并且探究了碳化钛加入量对Ti3C2Tx-WO3复合材料气敏性能的影响。结果表明：Ti3C2Tx的加入能够有效提高WO3纳米片的气敏性能。当Ti3C2Tx的加入量在7%（质量分数）时，Ti3C2Tx-WO3复合材料的最佳工作温度优化为80 ℃。7% Ti3C2Tx-WO3材料在80 ℃时对100 μL/L的乙醛气体的灵敏度达到了32.9，最低检测限为0.1 μL/L。

复合材料  /  碳化钛  /  乙醛  /  气敏性能

The acetaldehyde vapor produced in industrial production and life needs to be monitored in real time and efficiently, WO3 nanoplates and a series of Ti3C2Tx-WO3 composite materials were synthesized by a hydrothermal method. The structure and morphology of the as-prepared materials were investigated by X-ray diffraction, scanning electron microscopy, and X-ray photoelectron spectroscopy. The gas sensing properties of materials were analyzed. The results show that the addition of Ti3C2Tx can enhance the gas sensing performance of WO3 nanoplates. The optimized gas sensing operation temperature is 80 ℃ for 7%(mass fraction) Ti3C2Tx-WO3 composite material. The sensitivity of 7% Ti3C2Tx-WO3 composite material to 100 μL/L acetaldehyde vapor at 80 ℃ is 32.9 within a low detection limit of 0.1 μL/L.

composite material  /  titanium carbide  /  acetaldehyde  /  gas sensing properties
鲍思洁, 卜鑫, 白玉莹, 王春水, 储向峰, 梁士明. 水热法制备Ti3C2Tx-WO3复合材料及其对乙醛气体的传感性能. 硅酸盐学报, 2022 , 50 (10) : 2684 -2691 . DOI: 10.14062/j.issn.0454-5648.20220172
Sijie BAO, Xin BU, Yuying BAI, Chunshui WANG, Xiangfeng Chu, Shiming LIANG. Acetaldehyde Sensing Properties of Ti3C2Tx-WO3 Composites Synthesized by Hydrothermal Method[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (10) : 2684 -2691 . DOI: 10.14062/j.issn.0454-5648.20220172
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  • 国家自然科学基金项目(61971003)
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2022年第50卷第10期
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doi: 10.14062/j.issn.0454-5648.20220172
  • 接收时间：2022-03-07
  • 首发时间：2026-10-20
  • 出版时间：2022-10-20
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  • 收稿日期：2022-03-07
  • 修回日期：2022-03-26
基金
国家自然科学基金项目(61971003)
作者信息
    1．安徽工业大学化学与化工学院，安徽 马鞍山 243002
    2．临沂大学材料科学与工程学院，山东 临沂 276005

通讯作者:

储向峰（1966—），男，博士，教授；
梁士明（1983—），男，博士，讲师。
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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