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Article(id=1319236607471899536, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236561179366013, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220184, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1646928000000, receivedDateStr=2022-03-11, revisedDate=1650038400000, revisedDateStr=2022-04-16, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460117451, onlineDateStr=2026-10-20, pubDate=1663603200000, pubDateStr=2022-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460117451, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460117451, creator=13701087609, updateTime=1792460117451, updator=13701087609, issue=Issue{id=1319236561179366013, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='9', pageStart='2351', pageEnd='2578', issueExtLink='null', onlineDate='null', pubDate='1663603200000', pubDateStr='2022-09-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460106415, creator='13701087609', updateTime=1792460650608, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319238843744764843, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236561179366013, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319238843744764844, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236561179366013, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2483, endPage=2492, ext={EN=ArticleExt(id=1319236607727752081, articleId=1319236607471899536, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Low-Temperature Synthesis and Photoluminescence Properties of 3C-SiC Nanowires via Co Nanoparticle Catalytic Reaction, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

3C-SiC nanowires were synthesized in Ar atomosphere via Co nanoparticle catalytic reaction with expanded graphite and silicon powders as raw materials and Co(NO3)2·6H2O as a catalyst precursor. The effects of reaction temperature and catalyst addition on the formation of SiC nanowires were investigated. The phase composition and microstructure of the as-prepared products were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The optoelectronic property of as-prepared 3C-SiC nanowires was analyzed. The results show that Co catalyst promotes the growth of 3C-SiC nanowires and decreases the complete reaction temperature and the formation temperature. 3C-SiC nanowires could be synthesized at 1 573 K for 3 h using 3.0% Co as catalysts at C/Si molar ratio of 1∶1. The formed 3C-SiC nanowires are approximately 50-60 nm in diameter and tens micrometers in length. According to the results by the first-principles calculation, the activities of the reactants are increased via dwindling the bonding strength of C=C, Si—O and C—O bonds. The room-temperature PL spectra indicate that the as-synthesized 3C-SiC nanowires have a special emission at 307 nm (4.04 eV), which could be used as a potential material for optoelectronic nanodevices.

, authors=Huifang WANG1, Haijun ZHANG2, Shiming HAO3, Haisheng LI3, Yubao BI4, Wei JIANG1, Juhui LIU1, authorsList=Huifang WANG, Haijun ZHANG, Shiming HAO, Haisheng LI, Yubao BI, Wei JIANG, Juhui LIU, authorCompany=null, correspAuthors=Shiming HAO, authorNote=

WANG Huifang (1975-), female, Ph.D., Associate Professor. E-mail:

, correspAuthorsNote=
HAO Shiming (1975-), male, Ph.D., Associate Professor. E-mail:
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以膨胀石墨和硅粉为原料、Co（NO3）3·6H2O为催化剂前驱体，在流动Ar气中合成了3C-SiC纳米线。研究了反应温度、催化剂用量对合成3C-SiC粉体反应的影响。用第一性原理计算分析了Co纳米颗粒的催化机理，研究了3C-SiC纳米线的光致发光性能。结果表明：催化剂Co的引入降低了硅粉碳化反应生成SiC的开始反应温度和完全反应温度。催化剂Co的加入量为3%（质量分数）时，1 573 K保温3 h反应后合成的3C-SiC纳米线的直径为50~60 nm，长度约几十微米，其生长机理主要为气-固反应。Co纳米颗粒与反应物之间的吸附作用降低了C=C键、C—O键和Si—O键的结合，从而促进了SiC的成核与生长。激发波长为254 nm时，3C-SiC纳米线的室温光致发光谱的特征峰在307 nm，该纳米线在光电子纳米材料领域有良好的应用前景。

, authors=王慧芳1, 张海军2, 郝世明3, 李海生3, 毕玉保4, 姜威1, 柳菊荟1, authorsList=王慧芳, 张海军, 郝世明, 李海生, 毕玉保, 姜威, 柳菊荟, authorCompany=null, correspAuthors=郝世明, authorNote=

王慧芳（1975—），女，博士，副教授。

, correspAuthorsNote=
郝世明（1975—），男，博士，副教授。
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Co纳米颗粒低温催化合成3C-SiC纳米线及其光致发光性能
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王慧芳 1 , 张海军 2 , 郝世明 3 , 李海生 3 , 毕玉保 4 , 姜威 1 , 柳菊荟 1
硅酸盐学报 | 研究论文 2022,50(9): 2483-2492
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硅酸盐学报 |研究论文 2022 , 50 (9) : 2483 -2492
Co纳米颗粒低温催化合成3C-SiC纳米线及其光致发光性能
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王慧芳1 , 张海军2, 郝世明3 , 李海生3, 毕玉保4, 姜威1, 柳菊荟1
作者信息
  • 1．山西工程技术学院-矿区生态修复与固废资源化省市共建山西省重点实验室培育基地，山西 阳泉 045000
  • 2．武汉科技大学省部共建耐火材料与冶金国家重点实验室，武汉 430081
  • 3．河南科技大学物理工程学院，河南 洛阳 471003
  • 4．河南科技大学高温材料研究院，河南 洛阳 471003
通讯作者:
郝世明（1975—），男，博士，副教授。
作者简介:

王慧芳（1975—），女，博士，副教授。

Low-Temperature Synthesis and Photoluminescence Properties of 3C-SiC Nanowires via Co Nanoparticle Catalytic Reaction
Huifang WANG1 , Haijun ZHANG2, Shiming HAO3 , Haisheng LI3, Yubao BI4, Wei JIANG1, Juhui LIU1
Affiliations
  • 1.The Cultivation Base of Shanxi Key Laboratory of Mining Area Ecological Restoration and Solid Wastes Utilization, Shanxi Institute of Technology, Yangquan 045000, Shanxi, China
  • 2.The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China
  • 3.School of Physics and Engineering, Henan University of Science and Technology, Luoyang 471003, Henan, China
  • 4.High Temperature Materials Institute, Henan University of Science and Technology, Luoyang 471003, Henan, China
    • Corresponding Author:
    HAO Shiming (1975-), male, Ph.D., Associate Professor. E-mail:

    WANG Huifang (1975-), female, Ph.D., Associate Professor. E-mail:

出版时间: 2022-09-20 doi: 10.14062/j.issn.0454-5648.20220184
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摘要
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以膨胀石墨和硅粉为原料、Co（NO3）3·6H2O为催化剂前驱体，在流动Ar气中合成了3C-SiC纳米线。研究了反应温度、催化剂用量对合成3C-SiC粉体反应的影响。用第一性原理计算分析了Co纳米颗粒的催化机理，研究了3C-SiC纳米线的光致发光性能。结果表明：催化剂Co的引入降低了硅粉碳化反应生成SiC的开始反应温度和完全反应温度。催化剂Co的加入量为3%（质量分数）时，1 573 K保温3 h反应后合成的3C-SiC纳米线的直径为50~60 nm，长度约几十微米，其生长机理主要为气-固反应。Co纳米颗粒与反应物之间的吸附作用降低了C=C键、C—O键和Si—O键的结合，从而促进了SiC的成核与生长。激发波长为254 nm时，3C-SiC纳米线的室温光致发光谱的特征峰在307 nm，该纳米线在光电子纳米材料领域有良好的应用前景。

3C-碳化硅纳米线  /  光致发光  /  第一性原理计算  /  钴纳米颗粒催化剂  /  膨胀石墨

3C-SiC nanowires were synthesized in Ar atomosphere via Co nanoparticle catalytic reaction with expanded graphite and silicon powders as raw materials and Co(NO3)2·6H2O as a catalyst precursor. The effects of reaction temperature and catalyst addition on the formation of SiC nanowires were investigated. The phase composition and microstructure of the as-prepared products were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The optoelectronic property of as-prepared 3C-SiC nanowires was analyzed. The results show that Co catalyst promotes the growth of 3C-SiC nanowires and decreases the complete reaction temperature and the formation temperature. 3C-SiC nanowires could be synthesized at 1 573 K for 3 h using 3.0% Co as catalysts at C/Si molar ratio of 1∶1. The formed 3C-SiC nanowires are approximately 50-60 nm in diameter and tens micrometers in length. According to the results by the first-principles calculation, the activities of the reactants are increased via dwindling the bonding strength of C=C, Si—O and C—O bonds. The room-temperature PL spectra indicate that the as-synthesized 3C-SiC nanowires have a special emission at 307 nm (4.04 eV), which could be used as a potential material for optoelectronic nanodevices.

3C-silicon carbide nanowires  /  optoelectronic property  /  first-principles calculations  /  cobalt-nanoparticle catalysts  /  expanded graphite
王慧芳, 张海军, 郝世明, 李海生, 毕玉保, 姜威, 柳菊荟. Co纳米颗粒低温催化合成3C-SiC纳米线及其光致发光性能. 硅酸盐学报, 2022 , 50 (9) : 2483 -2492 . DOI: 10.14062/j.issn.0454-5648.20220184
Huifang WANG, Haijun ZHANG, Shiming HAO, Haisheng LI, Yubao BI, Wei JIANG, Juhui LIU. Low-Temperature Synthesis and Photoluminescence Properties of 3C-SiC Nanowires via Co Nanoparticle Catalytic Reaction[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (9) : 2483 -2492 . DOI: 10.14062/j.issn.0454-5648.20220184
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  • 国家自然科学基金(11404098)
  • 山西省基础研究计划自由探索类面上项目(20210302123427)
  • 山西省留学回国人员科技活动择优资助项目(20220038)
  • 山西省回国留学人员科研资助(2020-151)
  • 省部共建耐火材料与冶金国家重点实验室开放基金(G202006; G202008)
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doi: 10.14062/j.issn.0454-5648.20220184
  • 接收时间：2022-03-11
  • 首发时间：2026-10-20
  • 出版时间：2022-09-20
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  • 收稿日期：2022-03-11
  • 修回日期：2022-04-16
基金
国家自然科学基金(11404098)
山西省基础研究计划自由探索类面上项目(20210302123427)
山西省留学回国人员科技活动择优资助项目(20220038)
山西省回国留学人员科研资助(2020-151)
省部共建耐火材料与冶金国家重点实验室开放基金(G202006; G202008)
作者信息
    1．山西工程技术学院-矿区生态修复与固废资源化省市共建山西省重点实验室培育基地，山西 阳泉 045000
    2．武汉科技大学省部共建耐火材料与冶金国家重点实验室，武汉 430081
    3．河南科技大学物理工程学院，河南 洛阳 471003
    4．河南科技大学高温材料研究院，河南 洛阳 471003

通讯作者:

郝世明（1975—），男，博士，副教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20220184
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
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