Article(id=1319232626372755717, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20211011, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1637769600000, receivedDateStr=2021-11-25, revisedDate=1640188800000, revisedDateStr=2021-12-23, acceptedDate=null, acceptedDateStr=null, onlineDate=1792459168284, onlineDateStr=2026-10-20, pubDate=1658246400000, pubDateStr=2022-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792459168284, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792459168284, creator=13701087609, updateTime=1792459168284, updator=13701087609, issue=Issue{id=1319232566922695375, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='7', pageStart='1775', pageEnd='2066', issueExtLink='null', onlineDate='null', pubDate='1658246400000', pubDateStr='2022-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792459154109, creator='13701087609', updateTime=1792460038980, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319236278420357264, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319236278420357265, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1945, endPage=1954, ext={EN=ArticleExt(id=1319232627870122246, articleId=1319232626372755717, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Performance of Passive NO_x Adsorbent Pd/ZSM-5, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The existing NO_x post-treatment techniques of diesel vehicle exhaust have a poor performance during the cold start, passive NO_x adsorbent (PNA) is thus proposed. In this paper, Pd/ZSM-5 PNA was obtained by loading 1% Pd onto ZSM-5 zeolite in Si/Al ratio of 11.5 via incipient wetness impregnation and ion exchange, respectively. The effect of reaction atmosphere (with or without O₂ and H₂O) on the adsorbed-released NO_x performance of PNA with two Pd loading methods was investigated. The mechanism of the factors affecting the structure properties, Pd species state and acid properties of Pd/ZSM-5 was analyzed by X-ray diffraction, N₂ adsorption-desorption isotherm, transmission tlectron microscopy, in-situ diffuse reflectance infrared Fourier transform spectroscopy and NH₃-temperature programmed desorption, respectively. The O₂ effect in the pretreatment atmosphere was further evaluated. The results show that there are more NO active adsorption sites with O₂ in pretreatment and reaction atmosphere during incipient wetness impregnation, thus improving the NO adsorption capacity of Pd/ZSM-5. In addition, O₂ promotes the release of NO_x at a lower temperature (~200 ℃), and an incipient wetness impregnation method reduces the release temperature to 430 ℃, which is conducive to the material regeneration. H₂O inhibits NO adsorption, but promotes NO_x release capacity at a higher temperature. This work can provide a reference for the design of high-performance Pd/zeolites. High adsorption-release capacity is the important prerequisite for the development of high-performance PNA.

, authors=Rouxing PAN¹, Qingjun YU^{1, 2}, Honghong YI^{1, 2}, Fengyu GAO^{1, 2}, Xianzheng MENG¹, Yuanyuan LIU¹, Xiaolong TANG^{1, 2}, authorsList=Rouxing PAN, Qingjun YU, Honghong YI, Fengyu GAO, Xianzheng MENG, Yuanyuan LIU, Xiaolong TANG, authorCompany=null, correspAuthors=Xiaolong TANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319232628214055175, articleId=1319232626372755717, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=被动式NO_x吸附剂Pd/ZSM-5的性能影响因素, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

柴油车尾气NO_x后处理技术对冷启动阶段NO_x净化效果较差，被动NO_x吸附剂（PNA）应运而生。分别采用等体积浸渍法和离子交换法将1% Pd负载于m（Si）/m（Al）为11.5的ZSM-5分子筛，获得Pd/ZSM-5 PNA材料。考察反应气氛（有无O₂和H₂O）对2种不同Pd负载方式PNA吸附-释放NO_x性能的影响。采用X射线衍射、N₂吸附-脱附曲线测定、透射电子显微镜、原位漫反射Fourier变换红外光谱和NH₃程序升温脱附手段，从Pd/ZSM-5结构性质，Pd物种形态和酸性质分析以上因素的影响作用机制，并进一步评价预处理气氛中O₂作用。结果表明：反应气和预处理气氛存在O₂及等体积浸渍法中存在更多NO活性吸附位点从而提高Pd/ZSM-5的NO吸附能力。此外，O₂促进NO_x低温（~200 ℃）释放，等体积浸渍法使释放温度降至430 ℃，有利于材料再生。H₂O抑制了NO吸附，但可提高NO_x高温释放能力。为设计高性能Pd/分子筛提供建议，具备高吸附-释放能力是开发高性能PNA的重要前提。

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PAN Rouxing (1996-), female, Master candidate. E-mail: 1159385056@qq.com

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PAN Rouxing (1996-), female, Master candidate. E-mail: 1159385056@qq.com

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潘柔杏（1996—），女，硕士研究生。

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潘柔杏（1996—），女，硕士研究生。

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