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Article(id=1319232598119919955, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210955, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1636473600000, receivedDateStr=2021-11-10, revisedDate=1641571200000, revisedDateStr=2022-01-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1792459161547, onlineDateStr=2026-10-20, pubDate=1658246400000, pubDateStr=2022-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792459161547, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792459161547, creator=13701087609, updateTime=1792459161547, updator=13701087609, issue=Issue{id=1319232566922695375, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='7', pageStart='1775', pageEnd='2066', issueExtLink='null', onlineDate='null', pubDate='1658246400000', pubDateStr='2022-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792459154109, creator='13701087609', updateTime=1792460038980, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319236278420357264, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319236278420357265, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1929, endPage=1935, ext={EN=ArticleExt(id=1319232598556127572, articleId=1319232598119919955, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Properties of Yttria Stabilized Zirconia Electrolyte for Solid Oxide Fuel Cell by Plasma Spraying, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Metal-supported solid oxide fuel cells have promising applications. However, there is no the corresponding cost-effective preparation technology. Yttria stabilized zirconia (YSZ) electrolyte of solid oxide fuel cell was fabricated on a meatal substrate via high-efficiency and low-cost atmospheric plasma spraying (APS). The relationship between depositional particle morphology and coating structure under heating matrix conditions was investigated. The mechanical properties of electrolyte and cell out performance were evaluated. The results indicate that YSZ deposition particles on the heated substrate are fully spread. However, some microcracks appear in the splats, leading to some vertical cracks and interlamellar unbonded-interfaces inside the coating, the porosity is 7.16%, and nanoindentation hardness and elastic modulus of YSZ electrolyte are (13±1.04) GPa and (188.5±2.59) GPa, respectively. The maximum open voltage of cell with YSZ electrolyte deposited by APS is 0.97 V, thus improving the density. Nevertheless, the cell out performance is quite considerable with a peak power density of 850 mW/cm2 at 900 ℃. After the optimization of equipment iteration or combined with the post-treatment process, APS can be used to obtain alarge-scale and low-cost preparation of dense YSZ electrolytes.

, authors=Ke DU1, 2, Chen SONG1, Min YU2, Dan CHEN1, Yu GUO1, Taikai LIU1, Chenghao YANG3, Min LIU1, authorsList=Ke DU, Chen SONG, Min YU, Dan CHEN, Yu GUO, Taikai LIU, Chenghao YANG, Min LIU, authorCompany=null, correspAuthors=Chen SONG, authorNote=

DU Ke (1996-), male, Master candidate. E-mail:

, correspAuthorsNote=
SONG Chen (1990-), male, Ph.D.. E-mail:
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金属支撑型固体氧化物燃料电池极具应用前景，但缺少高性价比制备技术。采用高效率、低成本大气等离子喷涂（APS）在金属基体上制备了氧化钇稳定氧化锆（YSZ）电解质，研究加热基体条件下沉积粒子形貌与涂层结构间的联系，并评估电解质的力学性能和电池性能。结果表明：加热后的基体上，YSZ沉积粒子铺展充分，片层内存在微裂纹，导致结构中除未结合区域外还存在垂直裂纹，涂层孔隙率为7.16%，YSZ纳米压痕硬度和弹性模量分别为（13.0±1.0） GPa和（188.5±2.6） GPa。受电解质不致密的影响，APS沉积的YSZ单电池最高开路电压为0.97 V，致密度还需进一步提高，但电池输出性能可观，900 ℃峰功率密度为850 mW/cm2。随着设备迭代优化或结合后处理工艺，APS有望实现致密YSZ电解质的大规模低成本制备。

, authors=杜柯1, 2, 宋琛1, 余敏2, 陈丹1, 郭宇1, 刘太楷1, 杨成浩3, 刘敏1, authorsList=杜柯, 宋琛, 余敏, 陈丹, 郭宇, 刘太楷, 杨成浩, 刘敏, authorCompany=null, correspAuthors=宋琛, authorNote=

杜柯（1996—），男，硕士研究生

, correspAuthorsNote=
宋琛（1990—），男，博士
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DU Ke (1996-), male, Master candidate. E-mail:

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DU Ke (1996-), male, Master candidate. E-mail:

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固体氧化物燃料电池氧化钇稳定氧化锆电解质的等离子喷涂制备及性能
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杜柯 1, 2 , 宋琛 1 , 余敏 2 , 陈丹 1 , 郭宇 1 , 刘太楷 1 , 杨成浩 3 , 刘敏 1
硅酸盐学报 | 研究论文 2022,50(7): 1929-1935
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硅酸盐学报 |研究论文 2022 , 50 (7) : 1929 -1935
固体氧化物燃料电池氧化钇稳定氧化锆电解质的等离子喷涂制备及性能
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杜柯1, 2 , 宋琛1 , 余敏2, 陈丹1, 郭宇1, 刘太楷1, 杨成浩3, 刘敏1
作者信息
  • 1．广东省科学院新材料研究所，现代材料表面工程技术国家工程实验室，广东省现代表面工程技术重点实验室，广州 510650
  • 2．西南交通大学材料科学与工程学院，成都 610031
  • 3．华南理工大学环境与能源学院，广州 510006
通讯作者:
宋琛（1990—），男，博士
作者简介:

杜柯（1996—），男，硕士研究生

Preparation and Properties of Yttria Stabilized Zirconia Electrolyte for Solid Oxide Fuel Cell by Plasma Spraying
Ke DU1, 2 , Chen SONG1 , Min YU2, Dan CHEN1, Yu GUO1, Taikai LIU1, Chenghao YANG3, Min LIU1
Affiliations
  • 1.Institute of New Materials, Guangdong Academy of Sciences, National Engineering Laboratory for Modern Materials Surface Engineering Technology, The Key Lab of Guangdong for Modern Surface Engineering Technology, Guangzhou 510650, China
  • 2.School of Materials Science and Engineering, Southwest Jiaotong University, Chengdu 610031, China
  • 3.School of Environment and Energy, South China University of Technology, Guangzhou 510006, China
    • Corresponding Author:
    SONG Chen (1990-), male, Ph.D.. E-mail:

    DU Ke (1996-), male, Master candidate. E-mail:

出版时间: 2022-07-20 doi: 10.14062/j.issn.0454-5648.20210955
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金属支撑型固体氧化物燃料电池极具应用前景，但缺少高性价比制备技术。采用高效率、低成本大气等离子喷涂（APS）在金属基体上制备了氧化钇稳定氧化锆（YSZ）电解质，研究加热基体条件下沉积粒子形貌与涂层结构间的联系，并评估电解质的力学性能和电池性能。结果表明：加热后的基体上，YSZ沉积粒子铺展充分，片层内存在微裂纹，导致结构中除未结合区域外还存在垂直裂纹，涂层孔隙率为7.16%，YSZ纳米压痕硬度和弹性模量分别为（13.0±1.0） GPa和（188.5±2.6） GPa。受电解质不致密的影响，APS沉积的YSZ单电池最高开路电压为0.97 V，致密度还需进一步提高，但电池输出性能可观，900 ℃峰功率密度为850 mW/cm2。随着设备迭代优化或结合后处理工艺，APS有望实现致密YSZ电解质的大规模低成本制备。

固体氧化物燃料电池  /  氧化钇稳定氧化锆  /  大气等离子喷涂  /  电解质

Metal-supported solid oxide fuel cells have promising applications. However, there is no the corresponding cost-effective preparation technology. Yttria stabilized zirconia (YSZ) electrolyte of solid oxide fuel cell was fabricated on a meatal substrate via high-efficiency and low-cost atmospheric plasma spraying (APS). The relationship between depositional particle morphology and coating structure under heating matrix conditions was investigated. The mechanical properties of electrolyte and cell out performance were evaluated. The results indicate that YSZ deposition particles on the heated substrate are fully spread. However, some microcracks appear in the splats, leading to some vertical cracks and interlamellar unbonded-interfaces inside the coating, the porosity is 7.16%, and nanoindentation hardness and elastic modulus of YSZ electrolyte are (13±1.04) GPa and (188.5±2.59) GPa, respectively. The maximum open voltage of cell with YSZ electrolyte deposited by APS is 0.97 V, thus improving the density. Nevertheless, the cell out performance is quite considerable with a peak power density of 850 mW/cm2 at 900 ℃. After the optimization of equipment iteration or combined with the post-treatment process, APS can be used to obtain alarge-scale and low-cost preparation of dense YSZ electrolytes.

solid oxide fuel cell  /  yttria stabilized zirconia  /  atmospheric plasma spraying  /  electrolyte
杜柯, 宋琛, 余敏, 陈丹, 郭宇, 刘太楷, 杨成浩, 刘敏. 固体氧化物燃料电池氧化钇稳定氧化锆电解质的等离子喷涂制备及性能. 硅酸盐学报, 2022 , 50 (7) : 1929 -1935 . DOI: 10.14062/j.issn.0454-5648.20210955
Ke DU, Chen SONG, Min YU, Dan CHEN, Yu GUO, Taikai LIU, Chenghao YANG, Min LIU. Preparation and Properties of Yttria Stabilized Zirconia Electrolyte for Solid Oxide Fuel Cell by Plasma Spraying[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (7) : 1929 -1935 . DOI: 10.14062/j.issn.0454-5648.20210955
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  • 广东省基础与应用基础研究基金(2022A1515010682; 2021A1515110260)
  • 广东省软科学研究计划项目(2019B101001011)
  • 广州市科技计划项目(202007020008)
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doi: 10.14062/j.issn.0454-5648.20210955
  • 接收时间：2021-11-10
  • 首发时间：2026-10-20
  • 出版时间：2022-07-20
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  • 收稿日期：2021-11-10
  • 修回日期：2022-01-08
基金
广东省基础与应用基础研究基金(2022A1515010682; 2021A1515110260)
广东省软科学研究计划项目(2019B101001011)
广州市科技计划项目(202007020008)
作者信息
    1．广东省科学院新材料研究所，现代材料表面工程技术国家工程实验室，广东省现代表面工程技术重点实验室，广州 510650
    2．西南交通大学材料科学与工程学院，成都 610031
    3．华南理工大学环境与能源学院，广州 510006

通讯作者:

宋琛（1990—），男，博士
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20210955
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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