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Article(id=1319232592709267745, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20211097, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1640016000000, receivedDateStr=2021-12-21, revisedDate=1641225600000, revisedDateStr=2022-01-04, acceptedDate=null, acceptedDateStr=null, onlineDate=1792459160257, onlineDateStr=2026-10-20, pubDate=1658246400000, pubDateStr=2022-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792459160257, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792459160257, creator=13701087609, updateTime=1792459160257, updator=13701087609, issue=Issue{id=1319232566922695375, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='7', pageStart='1775', pageEnd='2066', issueExtLink='null', onlineDate='null', pubDate='1658246400000', pubDateStr='2022-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792459154109, creator='13701087609', updateTime=1792460038980, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319236278420357264, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319236278420357265, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1899, endPage=1908, ext={EN=ArticleExt(id=1319232592910594338, articleId=1319232592709267745, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Fabrication and Electrochemical Performance of Flexible Interdigital Supercapacitor Based on NiCo2S4/g-C3N4 Hybrid, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The manufacture of flexible, miniature, large-area and low-cost energy storge units has attracted much attention with a rapid development of flexible electronic devices. In this paper, NiCo2S4/g-C3N4 nanocomposite material was prepared via a one-step solvothermal process with nickel and cobalt nitrate hexahydrate as raw materials, thiourea as a vulcanizing agent and pyrolysis g-C3N4. The interdigital electrode of NiCo2S4/g-C3N4 was created via mask printing on a polyethylene glycol terephthalate flexible substrate with the well-prepared ink. The flexible interdigital supercapacitor was obtained by coating a layer of gel electrolyte. Based on the structure and electrochemical performance characterizations, NiCo2S4 nanoparticles dispersedly grow on g-C3N4 nanoplates, thus improving the charge transfer and accommodating the volume expansion of NiCo2S4 during charge-discharge cycles. The area specific capacitance of the nanocomposite electrode is 9.1 F/cm2 at a current density of 10 mA/cm2. The assembled supercapacitor can operate at -0.2-0.6 V and remainsstable at a scanning rate of 500 mV/s, revealing a good rate performance. The area specific capacitance of the device is 5.7 mF/cm2 at a scanning rate of 20 mV/s, and the energy density is 0.56 mW·h/cm3 at a power density of 17.5 mW/cm3.

, authors=Zhongqing TIAN1, Dandan WANG1, Fancheng MENG1, Chunyan ZHANG1, Liangliang CAO1, Huixing LIN2, authorsList=Zhongqing TIAN, Dandan WANG, Fancheng MENG, Chunyan ZHANG, Liangliang CAO, Huixing LIN, authorCompany=null, correspAuthors=Liangliang CAO, Huixing LIN, authorNote=

TIAN Zhongqing (1973-), male, Professor. E-mail:

, correspAuthorsNote=
CAO Liangliang (1987-), male, Ph.D; E-mail:
LIN Huixing (1979-), male, Ph.D., Professor.
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近年来，随着柔性电子的快速发展，制造柔性、微型、大面积和低成本的储能器件得到了极大的关注。以六水硝酸镍/钴为原料、硫脲为硫化剂、引入热解g-C3N4，通过一步溶剂热制备NiCo2S4/g-C3N4纳米复合材料。采用掩膜版将调配的NiCo2S4/g-C3N4油墨印刷在柔性聚对苯二甲酸乙二醇酯基底形成叉指结构电极，继而涂覆凝胶电解质组装成柔性叉指型超级电容器。结构和电化学性能研究表明：NiCo2S4纳米晶分布生长在g-C3N4纳米片层表面，引入的g-C3N4起到增强NiCo2S4充放电过程中的电荷传输及容纳其体积膨胀的作用，复合材料电极在10 mA/cm2的电流密度下面积比电容为9.1 F/cm2。组装的叉指电容器可在-0.2~0.6 V的电压下工作，并且在高至500 mV/s的扫描速率下保持稳定，表明器件良好的倍率性能。在20 mV/s的扫描速率下，器件的面积比电容可达5.7 mF/cm2，当功率密度为17.5 mW/cm3时，器件的能量密度为0.56 mW·h/cm3。

, authors=田中青1, 王丹丹1, 孟范成1, 张春艳1, 曹亮亮1, 林慧兴2, authorsList=田中青, 王丹丹, 孟范成, 张春艳, 曹亮亮, 林慧兴, authorCompany=null, correspAuthors=曹亮亮, 林慧兴, authorNote=

田中青（1973—），男，教授。

, correspAuthorsNote=
曹亮亮（1987—），男，博士；
林慧兴（1979—），男，博士，研究员。
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TIAN Zhongqing (1973-), male, Professor. E-mail:

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TIAN Zhongqing (1973-), male, Professor. E-mail:

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田中青（1973—），男，教授。

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田中青（1973—），男，教授。

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NiCo2S4/g-C3N4柔性叉指型超级电容制备与电化学性能
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田中青 1 , 王丹丹 1 , 孟范成 1 , 张春艳 1 , 曹亮亮 1 , 林慧兴 2
硅酸盐学报 | 研究论文 2022,50(7): 1899-1908
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硅酸盐学报 |研究论文 2022 , 50 (7) : 1899 -1908
NiCo2S4/g-C3N4柔性叉指型超级电容制备与电化学性能
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田中青1 , 王丹丹1, 孟范成1, 张春艳1, 曹亮亮1 , 林慧兴2
作者信息
  • 1．重庆理工大学材料科学与工程学院，重庆 400054
  • 2．中科院上海硅酸盐研究所，无机功能材料与器件重点实验室，上海 201800
通讯作者:
曹亮亮（1987—），男，博士；
林慧兴（1979—），男，博士，研究员。
作者简介:

田中青（1973—），男，教授。

Fabrication and Electrochemical Performance of Flexible Interdigital Supercapacitor Based on NiCo2S4/g-C3N4 Hybrid
Zhongqing TIAN1 , Dandan WANG1, Fancheng MENG1, Chunyan ZHANG1, Liangliang CAO1 , Huixing LIN2
Affiliations
  • 1.College of Materials Science and Engineering, Chongqing University of Technology, Chongqing 400054, China
  • 2.Key Laboratory of Inorganic Functional Materials and Devices, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 201800, China
    • Corresponding Author:
    CAO Liangliang (1987-), male, Ph.D; E-mail:
    LIN Huixing (1979-), male, Ph.D., Professor.

    TIAN Zhongqing (1973-), male, Professor. E-mail:

出版时间: 2022-07-20 doi: 10.14062/j.issn.0454-5648.20211097
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近年来，随着柔性电子的快速发展，制造柔性、微型、大面积和低成本的储能器件得到了极大的关注。以六水硝酸镍/钴为原料、硫脲为硫化剂、引入热解g-C3N4，通过一步溶剂热制备NiCo2S4/g-C3N4纳米复合材料。采用掩膜版将调配的NiCo2S4/g-C3N4油墨印刷在柔性聚对苯二甲酸乙二醇酯基底形成叉指结构电极，继而涂覆凝胶电解质组装成柔性叉指型超级电容器。结构和电化学性能研究表明：NiCo2S4纳米晶分布生长在g-C3N4纳米片层表面，引入的g-C3N4起到增强NiCo2S4充放电过程中的电荷传输及容纳其体积膨胀的作用，复合材料电极在10 mA/cm2的电流密度下面积比电容为9.1 F/cm2。组装的叉指电容器可在-0.2~0.6 V的电压下工作，并且在高至500 mV/s的扫描速率下保持稳定，表明器件良好的倍率性能。在20 mV/s的扫描速率下，器件的面积比电容可达5.7 mF/cm2，当功率密度为17.5 mW/cm3时，器件的能量密度为0.56 mW·h/cm3。

双金属硫化物  /  叉指超级电容  /  掩膜印刷  /  电化学性能

The manufacture of flexible, miniature, large-area and low-cost energy storge units has attracted much attention with a rapid development of flexible electronic devices. In this paper, NiCo2S4/g-C3N4 nanocomposite material was prepared via a one-step solvothermal process with nickel and cobalt nitrate hexahydrate as raw materials, thiourea as a vulcanizing agent and pyrolysis g-C3N4. The interdigital electrode of NiCo2S4/g-C3N4 was created via mask printing on a polyethylene glycol terephthalate flexible substrate with the well-prepared ink. The flexible interdigital supercapacitor was obtained by coating a layer of gel electrolyte. Based on the structure and electrochemical performance characterizations, NiCo2S4 nanoparticles dispersedly grow on g-C3N4 nanoplates, thus improving the charge transfer and accommodating the volume expansion of NiCo2S4 during charge-discharge cycles. The area specific capacitance of the nanocomposite electrode is 9.1 F/cm2 at a current density of 10 mA/cm2. The assembled supercapacitor can operate at -0.2-0.6 V and remainsstable at a scanning rate of 500 mV/s, revealing a good rate performance. The area specific capacitance of the device is 5.7 mF/cm2 at a scanning rate of 20 mV/s, and the energy density is 0.56 mW·h/cm3 at a power density of 17.5 mW/cm3.

bimetallic sulfide  /  interdigital supercapacitor  /  mask printing  /  electrochemical performance
田中青, 王丹丹, 孟范成, 张春艳, 曹亮亮, 林慧兴. NiCo2S4/g-C3N4柔性叉指型超级电容制备与电化学性能. 硅酸盐学报, 2022 , 50 (7) : 1899 -1908 . DOI: 10.14062/j.issn.0454-5648.20211097
Zhongqing TIAN, Dandan WANG, Fancheng MENG, Chunyan ZHANG, Liangliang CAO, Huixing LIN. Fabrication and Electrochemical Performance of Flexible Interdigital Supercapacitor Based on NiCo2S4/g-C3N4 Hybrid[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (7) : 1899 -1908 . DOI: 10.14062/j.issn.0454-5648.20211097
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  • 重庆市教育委员会科学技术研究计划项目(KJQN201901140)
  • 中科院无机功能材料与器件重点实验室开放课题项目(KLIFMD202106)
  • 重庆理工大学科研启动项目(2019ZD39)
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doi: 10.14062/j.issn.0454-5648.20211097
  • 接收时间：2021-12-21
  • 首发时间：2026-10-20
  • 出版时间：2022-07-20
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  • 收稿日期：2021-12-21
  • 修回日期：2022-01-04
基金
重庆市教育委员会科学技术研究计划项目(KJQN201901140)
中科院无机功能材料与器件重点实验室开放课题项目(KLIFMD202106)
重庆理工大学科研启动项目(2019ZD39)
作者信息
    1．重庆理工大学材料科学与工程学院，重庆 400054
    2．中科院上海硅酸盐研究所，无机功能材料与器件重点实验室，上海 201800

通讯作者:

曹亮亮（1987—），男，博士；
林慧兴（1979—），男，博士，研究员。
参考文献
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20211097
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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