Article(id=1319222740809269317, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222716851405704, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230070, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1676304000000, receivedDateStr=2023-02-14, revisedDate=1677340800000, revisedDateStr=2023-02-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456811381, onlineDateStr=2026-10-20, pubDate=1687190400000, pubDateStr=2023-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456811381, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456811381, creator=13701087609, updateTime=1792456811381, updator=13701087609, issue=Issue{id=1319222716851405704, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='6', pageStart='1373', pageEnd='1648', issueExtLink='null', onlineDate='null', pubDate='1687190400000', pubDateStr='2023-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456805669, creator='13701087609', updateTime=1792456995739, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223514108903801, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222716851405704, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223514108903802, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222716851405704, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1572, endPage=1582, ext={EN=ArticleExt(id=1319222740998012998, articleId=1319222740809269317, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Microscopic Characteristics and Activity of Light-Burned Magnesia, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Activity is a main application characteristic that is closely related to the microstructure of light-burned magnesia. The light-burned magnesia was obtained via calcining macrocrystalline magnesite powder at 700-1 100 ℃. The cell parameter, grain size, crystallinity, specific surface area, pore diameter distribution, specific pore volume, average pore diameter, activity and microstructure of light-burned magnesia at different temperatures were characterized. The particulate structure of light-burned magnesia was investigated by thermogravimetry based on the non-isothermal reaction kinetics theory, and the mechanism of the particulate structure evolution with temperature and its influence on the activity of light-burned magnesia were further analyzed. The results show that the cell parameter a₀ of light-burned magnesia firstly reduces and then becomes stable, and the grain size increases while the specific surface area decreases gradually when the calcination temperature increases from 700 ℃ to 1 100 ℃. However, the activity of light-burned magnesia does not comply with this rule, and reaches the maximum value at 800 ℃. The thermal decomposition of macrocrystalline magnesite powder is controlled via the chemical reaction at the phase interface. The decomposition product, i.e., the light-burned magnesia 'pseudo' particles, is composed of magnesia microcrystals and connected a pore network structure. The sintering of magnesia microcrystals affect the "pseudo" particle structure of light-burned magnesia as the calcination temperature increases, thus affectingits activity. The sample light-burned at 800 ℃ has a smaller grain size, a lower crystallinity, a larger specific pore volume, and a largest average pore size due to the lattice adjustment, which is conducive to the penetration of the reactant solution into the particles and accelerates the reaction progression, leading to the maximum activity.

, authors=Yunqin GAO¹, Jiawei WANG¹, Xiaoli TIAN², Yanlong YANG¹, Xing HOU¹, authorsList=Yunqin GAO, Jiawei WANG, Xiaoli TIAN, Yanlong YANG, Xing HOU, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222741203533895, articleId=1319222740809269317, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=轻烧氧化镁的微观特征及其活性, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

活性是轻烧氧化镁的主要应用特性，它与轻烧氧化镁的微观结构密切相关。将新疆某粗晶菱镁矿粉在700~1 100 ℃煅烧制得轻烧氧化镁，对不同温度轻烧氧化镁的晶胞参数、晶粒尺寸、结晶度、比表面积、孔径分布、比孔容、平均孔径、活性和显微结构等进行表征，利用TG结合非等温反应动力学理论研究轻烧氧化镁的微粒结构，分析该微粒结构随温度变化的机理及其对轻烧氧化镁活性的影响。结果表明：从700 ℃至1 100 ℃，轻烧氧化镁晶胞参数a₀缩小并趋于稳定，晶粒尺寸逐渐增大，比表面积逐渐减小，但其活性变化并不遵从这一规律，在800 ℃时活性最高；粗晶菱镁矿粉的热分解受相界面上的化学反应所控制，分解产物—轻烧氧化镁“假象”微粒由氧化镁微晶和贯通的气孔网络结构组成；随煅烧温度升高，氧化镁微晶的烧结影响轻烧氧化镁“假象”微粒结构，进而影响其活性；800 ℃轻烧试样晶粒尺寸较小，结晶度较低，比孔容较大，且由于晶格调整使其平均孔径最大，大的孔径有利于溶液进入微粒内部，促进反应进行，因此其活性最高。

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GAO Yunqin (1972-), female, Master, Senior Engineer. E-mail: gaoyunqin@xauat.edu.cn

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高云琴（1972—），女，硕士，高级工程师。

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