Article(id=1319222703052145440, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222668956643677, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220922, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1666713600000, receivedDateStr=2022-10-26, revisedDate=1667404800000, revisedDateStr=2022-11-03, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456802380, onlineDateStr=2026-10-20, pubDate=1684512000000, pubDateStr=2023-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456802380, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456802380, creator=13701087609, updateTime=1792456802380, updator=13701087609, issue=Issue{id=1319222668956643677, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='5', pageStart='1091', pageEnd='1372', issueExtLink='null', onlineDate='null', pubDate='1684512000000', pubDateStr='2023-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456794251, creator='13701087609', updateTime=1792456976356, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223432827490920, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222668956643677, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223432827490921, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222668956643677, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1293, endPage=1301, ext={EN=ArticleExt(id=1319222703421244193, articleId=1319222703052145440, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis and Mechanism of Shrinkage-Reducing Polycarboxylate Superplasticizer, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

To provide a theoretical reference for reducing the shrinkage and cracking of concrete and promoting the development and application of the shrinkage-reducing polycarboxylate superplasticizer, a shrinkage-reducing polycarboxylate superplasticizer (SR-PCE) with dispersion and shrinkage reducing properties was synthesized via free radical polymerization with isopentenyl polyoxyethylene ether (IPEG), acrylic acid (AA), butyl acrylate (BA) and other monomers. The molecular structure of SR-PCE was characterized by gel permeation chromatography and Fourier transform infrared spectroscopy, and its shrinkage reduction mechanism was analyzed. The results show that the molecular structure of SR-PCE is a designed structure. The optimum shrinkage reducing performance of the synthesized PCE can be obtained at a molar ratio of IPEG∶AA∶BA of 1∶5∶4. The mechanism of SR-PCE with the optimum shrinkage reducing performance mainly is since SR-PCE can further reduce the surface tension of the solution rather than ordinary PCE, SR-PCE can reduce the evaporation rate of the pore solution of cement paste and improve the pore water retention.

, authors=Haosheng GE^{1, 2}, Zhenping SUN^{1, 2}, Haijing YANG^{1, 2}, Kunpeng ZHENG³, Ting ZHANG^{1, 2}, Yong CAO⁴, authorsList=Haosheng GE, Zhenping SUN, Haijing YANG, Kunpeng ZHENG, Ting ZHANG, Yong CAO, authorCompany=null, correspAuthors=Zhenping SUN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222703760982818, articleId=1319222703052145440, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=减缩型聚羧酸系减水剂的制备及机理, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

为了减少混凝土的收缩开裂、促进减缩型聚羧酸系减水剂的发展和应用，采用水溶液自由基聚合法，将异戊烯基聚氧乙烯醚（IPEG）、丙烯酸（AA）和丙烯酸丁酯（BA）等不饱和单体共聚合成了一种兼具分散性能和减缩性能的减缩型聚羧酸系减水剂（SR-PCE）。利用凝胶渗透色谱法和Fourier红外光谱法对SR-PCE的分子结构进行了表征，并对其减缩机理进行了分析。结果表明：所制备的SR-PCE的分子结构符合预先的设计；在保证优良分散性能的前提下，当SR-PCE分子结构中IPEG、AA和BA三者的摩尔比为1∶5∶4时，减缩性能最佳。SR-PCE发挥优良减缩作用的机理主要在于2个方面：首先，相比普通型聚羧酸系减水剂，SR-PCE可以进一步降低水溶液的表面张力；其次，SR-PCE可以减少水泥石孔溶液中水的蒸发速率，提高浆体对孔隙水的保持能力。

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GE Haosheng (1994-), male, Doctoral candidate. E-mail: 1044703776@qq.com

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GE Haosheng (1994-), male, Doctoral candidate. E-mail: 1044703776@qq.com

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葛好升（1994—），男，博士研究生。

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葛好升（1994—），男，博士研究生。

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