Article(id=1319222614032240685, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220837, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1664899200000, receivedDateStr=2022-10-05, revisedDate=1669392000000, revisedDateStr=2022-11-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456781156, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456781156, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456781156, creator=13701087609, updateTime=1792456781156, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=706, endPage=720, ext={EN=ArticleExt(id=1319222614254538798, articleId=1319222614032240685, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Reaction Mechanism and High-Temperature Oxidation Behavior of Reactively Sintered ZrB₂-SiC-Zr₂Al₄C₅ Composite Ceramics, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

ZrB₂-based composite ceramics have great potential for applications at ultra-high temperatures, but the low toughness and poor oxidation resistance of them limit their practical applications. In this work, the Zr, B₄C, Al, C and Si raw powders were used to prepare ZrB₂-SiC-Zr₂Al₄C₅ composite ceramics by reactive spark plasma sintering. The reaction processes and mechanism were studied. The effects of Zr₂Al₄C₅ content and oxidation temperature on high-temperature oxidation behavior of multiphase ceramics were investigated for revealing the anti-oxidation mechanism. The results indicated that the B₄C reacted with Zr to form ZrB₂ at 900 ℃, and then the SiC formed at 1 100 ℃. At 1 400 ℃, the Zr₂Al₄C₅ formed from the reaction of Zr₃Al₃C₅, ZrC and Al₄C₃ which formed at the early initial reaction stage. And the Zr₂Al₄C₅ transformed into Zr₃Al₄C₆ with further increasing temperature. The main phases of the composite ceramics after oxidation are ZrO₂, ZrSiO₄, aluminosilicate and SiO₂ glass. With increasing Zr₂Al₄C₅ content, the surface of the oxide layer of the composite ceramics became uneven, loose and porous, while obvious long strip grains and inhomogeneous distribution of glassy phases were also observed. This study not only provides a new experimental reference for in-depth understanding of the high-temperature oxidation behavior of ZrB₂-SiC based multiphase ceramics, but also provides new experimental and theoretical support for developing high-performance ZrB₂-SiC based high-temperature composite ceramics.

, authors=Qilong GUO^{1, 2}, Liang HUA¹, Ronghao LIU¹, Hao YING¹, Leilei LI^{1, 2}, Jing WANG^{1, 2}, authorsList=Qilong GUO, Liang HUA, Ronghao LIU, Hao YING, Leilei LI, Jing WANG, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222614472642607, articleId=1319222614032240685, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=ZrB₂-SiC-Zr₂Al₄C₅复相陶瓷烧结反应机理与高温氧化行为, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

ZrB₂基复相陶瓷在超高温领域有着重大应用潜力，但其韧性低、抗氧化性差限制了其实际应用。以Zr、B₄C、Al、C和Si粉为原料，采用反应放电等离子体烧结制备出ZrB₂-SiC-Zr₂Al₄C₅复相陶瓷，研究了反应过程和反应机理，探究了Zr₂Al₄C₅含量和氧化温度对复相陶瓷高温氧化行为的影响，揭示了其抗氧化机制。结果表明：900 ℃时，B₄C和Zr反应开始生成ZrB₂；1100 ℃开始生成SiC；1400 ℃时反应初期形成的Zr₃Al₃C₅与ZrC及Al₄C₃生成了Zr₂Al₄C₅；但随着温度继续升高Zr₂Al₄C₅则会转化为Zr₃Al₄C₆。复相陶瓷氧化后主要物相为ZrO₂、ZrSiO₄和铝硅酸盐以及SiO₂玻璃相；随着Zr₂Al₄C₅含量的增加，氧化层表面呈现出凹凸不平、疏松多孔，存在明显的长条状晶粒和不均匀分布的玻璃相。本工作为深化对ZrB₂-SiC基复相陶瓷的高温氧化行为的理解提供了实验依据，为开发高性能ZrB₂-SiC基高温复相陶瓷提供了实验与理论支持。

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Guo Qilong (1986-), male, Ph.D., Associate Professor. E-mail: guoqilong8@126.com

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Guo Qilong (1986-), male, Ph.D., Associate Professor. E-mail: guoqilong8@126.com

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郭启龙（1986—），男，博士，副教授。

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郭启龙（1986—），男，博士，副教授。

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