Article(id=1319222611599541103, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220822, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1664467200000, receivedDateStr=2022-09-30, revisedDate=1667318400000, revisedDateStr=2022-11-02, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456780576, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456780576, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456780576, creator=13701087609, updateTime=1792456780576, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=658, endPage=668, ext={EN=ArticleExt(id=1319222611826033520, articleId=1319222611599541103, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Spinel-Coated Aggregates on Thermal Shock Resistance and Cement Clinker Corrosion Resistance of Magnesia Spinel Refractories, columnId=1321891096775472081, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advances in Basic Research on Refractories Related—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Cement rotary kilns using refractories require excellent refractoriness, thermal shock stability and corrosion resistance due to the cyclic rotation and feeding-discharging of cement clinker. In this paper, a kind of magnesia-alumina spinel refractory containing coating structured aggregates were prepared by wrapping spinel fines on the surface of magnesia aggregates. The fracture behavior and corrosion resistance of prepared refractories were characterized by three-point bending test combined with digital image correlation, acoustic emission technique, and static slag resistance method. The results indicate that by changing the distribution of spinel to make coating structure aggregates, the alumina content is effectively reduced while a more uniform and extensive distribution of spinel phase is achieved. Compared with the merchant magnesia-alumina spinel refractory (10% Al2O3) with pre-synthetic spinel aggregates, the magnesia-alumina spinel refractory (5% Al2O3) with spinel coating aggregates has the improved mechanical strength and corrosion resistance, and maintains the thermal shock resistance.

, authors=Fangdi ZHU, Yajie DAI, Wen YAN, Yibiao XU, Dan WANG, Chao WANG, authorsList=Fangdi ZHU, Yajie DAI, Wen YAN, Yibiao XU, Dan WANG, Chao WANG, authorCompany=null, correspAuthors=Yajie DAI, authorNote=

ZHU Fangdi (1997-), male, Master candidate. E-mail:

, correspAuthorsNote=
DAI Yajie (1987-), female, Ph.D., Associate Professor. E-mail:
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由于周期性水泥熟料回转以及进出料,水泥回转窑用耐火材料需要兼顾优异的耐火度、热震稳定性和耐侵蚀性。本研究通过将尖晶石细粉包裹于镁砂骨料表面,制备出含包覆结构骨料的方镁石-镁铝尖晶石耐火材料,并采用三点弯曲测试结合数字图像相关以及声发射技术表征其断裂行为,以及采用静态抗渣法表征其抗侵蚀性能。结果表明:通过改变尖晶石分布,形成包覆结构复合骨料,降低了氧化铝含量,尖晶石相达到更为均匀且广泛的分散。与氧化铝含量(质量分数)为10%的市售预合成尖晶石骨料耐火材料相比,采用尖晶石包覆骨料的方镁石-尖晶石耐火材料(Al2O3含量为5%)在保证材料抗热震性能的同时,提升了力学强度、热震稳定性能以及抗侵蚀能力。

, authors=朱方迪, 戴亚洁, 鄢文, 徐义彪, 汪丹, 汪超, authorsList=朱方迪, 戴亚洁, 鄢文, 徐义彪, 汪丹, 汪超, authorCompany=null, correspAuthors=戴亚洁, authorNote=

朱方迪(1997—),男,硕士研究生。

, correspAuthorsNote=
戴亚洁(1987—),女,博士,副教授。
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朱方迪(1997—),男,硕士研究生。

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尖晶石包覆骨料对镁铝质耐火材料抗热震性和抗水泥熟料侵蚀的影响
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朱方迪 , 戴亚洁 , 鄢文 , 徐义彪 , 汪丹 , 汪超
硅酸盐学报 | 耐火材料相关基础研究进展专题—研究论文 2023,51(3): 658-668
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硅酸盐学报 |耐火材料相关基础研究进展专题—研究论文 2023 , 51 (3) : 658 -668
尖晶石包覆骨料对镁铝质耐火材料抗热震性和抗水泥熟料侵蚀的影响
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朱方迪 , 戴亚洁 , 鄢文, 徐义彪, 汪丹, 汪超
作者信息
  • 武汉科技大学,省部共建耐火材料与冶金国家重点实验室,高温材料与炉衬技术国家地方联合工程研究中心,武汉 430081
通讯作者:
戴亚洁(1987—),女,博士,副教授。
作者简介:

朱方迪(1997—),男,硕士研究生。

Effect of Spinel-Coated Aggregates on Thermal Shock Resistance and Cement Clinker Corrosion Resistance of Magnesia Spinel Refractories
Fangdi ZHU , Yajie DAI , Wen YAN, Yibiao XU, Dan WANG, Chao WANG
Affiliations
  • Wuhan University of Science and Technology, The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, National-provincial Joint Engineering Research Center of High Temperature Materials and Lining Technology, Wuhan 430081, China
  • Corresponding Author:
    DAI Yajie (1987-), female, Ph.D., Associate Professor. E-mail:

    ZHU Fangdi (1997-), male, Master candidate. E-mail:

出版时间: 2023-03-20 doi: 10.14062/j.issn.0454-5648.20220822
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由于周期性水泥熟料回转以及进出料,水泥回转窑用耐火材料需要兼顾优异的耐火度、热震稳定性和耐侵蚀性。本研究通过将尖晶石细粉包裹于镁砂骨料表面,制备出含包覆结构骨料的方镁石-镁铝尖晶石耐火材料,并采用三点弯曲测试结合数字图像相关以及声发射技术表征其断裂行为,以及采用静态抗渣法表征其抗侵蚀性能。结果表明:通过改变尖晶石分布,形成包覆结构复合骨料,降低了氧化铝含量,尖晶石相达到更为均匀且广泛的分散。与氧化铝含量(质量分数)为10%的市售预合成尖晶石骨料耐火材料相比,采用尖晶石包覆骨料的方镁石-尖晶石耐火材料(Al2O3含量为5%)在保证材料抗热震性能的同时,提升了力学强度、热震稳定性能以及抗侵蚀能力。

方镁石-尖晶石耐火材料  /  包覆结构骨料  /  热震稳定性能  /  抗侵蚀/渗透性能  /  无损探伤技术

Cement rotary kilns using refractories require excellent refractoriness, thermal shock stability and corrosion resistance due to the cyclic rotation and feeding-discharging of cement clinker. In this paper, a kind of magnesia-alumina spinel refractory containing coating structured aggregates were prepared by wrapping spinel fines on the surface of magnesia aggregates. The fracture behavior and corrosion resistance of prepared refractories were characterized by three-point bending test combined with digital image correlation, acoustic emission technique, and static slag resistance method. The results indicate that by changing the distribution of spinel to make coating structure aggregates, the alumina content is effectively reduced while a more uniform and extensive distribution of spinel phase is achieved. Compared with the merchant magnesia-alumina spinel refractory (10% Al2O3) with pre-synthetic spinel aggregates, the magnesia-alumina spinel refractory (5% Al2O3) with spinel coating aggregates has the improved mechanical strength and corrosion resistance, and maintains the thermal shock resistance.

magnesia-alumina spinel refractories  /  coating structured aggregates  /  thermal shock stability  /  corrosion/penetration resistance  /  nondestructive testing methods
朱方迪, 戴亚洁, 鄢文, 徐义彪, 汪丹, 汪超. 尖晶石包覆骨料对镁铝质耐火材料抗热震性和抗水泥熟料侵蚀的影响. 硅酸盐学报, 2023 , 51 (3) : 658 -668 . DOI: 10.14062/j.issn.0454-5648.20220822
Fangdi ZHU, Yajie DAI, Wen YAN, Yibiao XU, Dan WANG, Chao WANG. Effect of Spinel-Coated Aggregates on Thermal Shock Resistance and Cement Clinker Corrosion Resistance of Magnesia Spinel Refractories[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (3) : 658 -668 . DOI: 10.14062/j.issn.0454-5648.20220822
  • 国家自然科学基金青年项目(51902228)
  • 国家自然科学基金联合基金(U21A2058; U1908227)
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2023年第51卷第3期
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doi: 10.14062/j.issn.0454-5648.20220822
  • 接收时间:2022-09-30
  • 首发时间:2026-10-20
  • 出版时间:2023-03-20
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  • 收稿日期:2022-09-30
  • 修回日期:2022-11-02
基金
国家自然科学基金青年项目(51902228)
国家自然科学基金联合基金(U21A2058; U1908227)
作者信息
    武汉科技大学,省部共建耐火材料与冶金国家重点实验室,高温材料与炉衬技术国家地方联合工程研究中心,武汉 430081

通讯作者:

戴亚洁(1987—),女,博士,副教授。
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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