Article(id=1319222606910313457, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220858, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1665417600000, receivedDateStr=2022-10-11, revisedDate=1669737600000, revisedDateStr=2022-11-30, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456779457, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456779457, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456779457, creator=13701087609, updateTime=1792456779457, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=649, endPage=657, ext={EN=ArticleExt(id=1319222607145194482, articleId=1319222606910313457, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Magnesium Silicate Hydrate on Properties of Low-Microsilica Bonded Magnesia-Based Castables, columnId=1321891096775472081, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advances in Basic Research on Refractories Related—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Magnesium silicate hydrate (MgO-SiO₂-H₂O M-S-H) is a main bonding phase for microsilica bonded magnesium-castables used for tundish. Its content determines the mechanical properties after demolding. In this paper, M-S-H was synthesized with Na₂SiO₃·9H₂O and MgCl₂·6H₂O as raw materials. The effect of M-S-H at different calcination parameters was investigated by X-ray diffraction, scanning electron microscopy, specific surface area measurement, nuclear magnetic resonance, and thermogravimetry-differential scanning calorimetry. Moreover, the synthesized M-S-H with microsilica powder (1%) was introduced into the magnesia-based castables to evaluate their influences on the properties. The results show that M-S-H has a memory effect when the calcination temperature is below 400 ℃. Increasing the calcination time can facilitate the insertion of interlayer hydroxyl groups in M-S-H gels and contribute to the formation of a lamellar structure with a higher structure stability. A certain amount of pre-synthesized M-S-H and a small amount of silica powder can assure the castable with a good workability and a sufficient early bonding strength. The reduced silica can suppress the formation of large sized defects due to the volume shrinkage of matrix, in the interface of aggregates and matrix, thus improving the mechanical properties of castables. This work provides a support for the development of magnesia-based castables with a low silica content.

, authors=Yawei LI^{1, 2}, Ning LIAO², Wenjing LIU², Sisi ZHANG², Yibiao XU², Shengnian TIE¹, Xin LIU¹, Yueying LI¹, authorsList=Yawei LI, Ning LIAO, Wenjing LIU, Sisi ZHANG, Yibiao XU, Shengnian TIE, Xin LIU, Yueying LI, authorCompany=null, correspAuthors=Ning LIAO, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222607409435635, articleId=1319222606910313457, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=基于水合硅酸镁结构记忆特性制备低硅镁质浇注料, columnId=1321891096976798674, journalTitle=硅酸盐学报, columnName=耐火材料相关基础研究进展专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

水合硅酸镁是炼钢连铸过程中间包用镁质浇注料的重要结合相，其含量多少决定着浇注料的强度大小。本工作以Na₂SiO₃·9H₂O和MgCl₂·6H₂O为原料，采用水热法合成水合硅酸镁（MgO-SiO₂-H₂O, M-S-H），研究了焙烧温度和焙烧次数对水合硅酸镁的“结构记忆”特性；随后将预合成M-S-H复合硅微粉制备镁质浇注料，研究其对镁质浇注料性能的影响。结果表明：当焙烧温度低于400 ℃时，水合硅酸镁具有“结构记忆”特性，焙烧次数增加有利于M-S-H凝胶中层间羟基的插入，促进其层状结构晶粒的长大和结构稳定性的提高；在镁质浇注料制备过程中引入一定量的预合成水合硅酸镁和少量的硅微粉，使浇注料具有很好的施工性能和足够的早期结合强度；同时减少了高温热处理后浇注料缺陷形成，提高了材料力学性能，为开发低硅微粉镁质浇注料提供支撑。

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LI Yawei (1966-), male, Ph.D., Professor. E-mail: liyawei@wust.edu.cn

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LI Yawei (1966-), male, Ph.D., Professor. E-mail: liyawei@wust.edu.cn

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李亚伟（1966—），男，博士，教授。

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