Article(id=1319222570856067785, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20221010, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1669132800000, receivedDateStr=2022-11-23, revisedDate=1671292800000, revisedDateStr=2022-12-18, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456770861, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456770861, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456770861, creator=13701087609, updateTime=1792456770861, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=579, endPage=588, ext={EN=ArticleExt(id=1319222571053200074, articleId=1319222570856067785, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Structural Evolution of Cr₂AlB₂ Powder and Its Effect on Properties in Al₂O₃-C Refractories at High Temperature, columnId=1321891096775472081, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advances in Basic Research on Refractories Related—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Al₂O₃-C refractories are important for the continuous casting process. It is essential for safe and effective steel making processes to enhance the strength and oxidation resistance of Al₂O₃-C refractories. A compound MAB phase Cr₂AlB₂ has attracted recent attention due to its high fracture toughness, high damage tolerance and excellent oxidation resistance. In this work, a ternary layered compound Cr₂AlB₂ was introduced into the Al₂O₃-C refractories. The structural evolution of Cr₂AlB₂ in Al₂O₃-C refractories after treated at different temperatures and its effect on the comprehensive properties of Al₂O₃-C refractories were analyzed by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The results show that a gradual decomposition of Cr₂AlB₂ in Al₂O₃-C refractories generates a core-shell structure of CrB and Al₂O₃ covered with Al₂O₃, and catalyses the formation of carbon nanotubes and carbon fibers on the surface of the core-shell structure after thermal treatment at 800-1 200 ℃. Cr₃C₂ covered by BN structure is formed inside the core-shell structure after thermal treatment at 1 200-1 600 ℃. As a result, the densification of Al₂O₃-C refractories is facilitated, and the cold modulus of rupture and oxidation resistance is enhanced. The cold modulus of rupture after coking at 1 400-1 600 ℃ is increased by approximately 9%, and the oxide index after treated in air at 1 400 ℃ is reduced from 44% to 31%.

, authors=Yang ZHANG, Yawei LI, Ning LIAO, Gengfu LIU, Zixu JI, authorsList=Yang ZHANG, Yawei LI, Ning LIAO, Gengfu LIU, Zixu JI, authorCompany=null, correspAuthors=Yawei LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222571321635531, articleId=1319222570856067785, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=高温下Cr₂AlB₂粉末在铝碳耐火材料中的结构演变及其对性能的影响, columnId=1321891096976798674, journalTitle=硅酸盐学报, columnName=耐火材料相关基础研究进展专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

铝碳耐火材料是连铸滑动水口用关键材料，提高其强度和抗氧化性等服役性能，对于保障炼钢过程安全高效生产具有重要的意义。近年来，一种新型的MAB型层状化合物Cr₂AlB₂受到广泛关注，其具有高断裂韧性、高损伤容限和优异的抗氧化性。本工作在铝碳耐火材料中引入合成的Cr₂AlB₂，借助X射线衍射仪、场发射扫描电子显微镜、透射电子显微镜等测试手段，研究了高温下Cr₂AlB₂在铝碳材料中的结构演变及其对材料性能影响。结果表明：Cr₂AlB₂在800~1200 ℃热处理后逐步分解生成Al₂O₃包覆CrB的核壳结构，并在核壳结构表面催化生成碳纳米管、碳纤维；在1200~1600 ℃热处理后，核壳结构内部进一步演变，生成了Cr₃C₂和BN。因此，Cr₂AlB₂在铝碳耐火材料中发生的上述结构演变，促进了材料的致密化程度，提高了材料常温抗折强度以及抗氧化性。当Cr₂AlB₂引入量为1%时，材料性能最佳，经1400、1600 ℃热处理后的铝碳材料常温抗折强度提升约9%，经1400 ℃空气中处理后氧化指数从44%降低至31%。

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ZHANG Yang (1999-), male, Master candidate. E-mail: yangzhang9924@foxmail.com

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ZHANG Yang (1999-), male, Master candidate. E-mail: yangzhang9924@foxmail.com

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章阳（1999—），男，硕士研究生。

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章阳（1999—），男，硕士研究生。

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