Article(id=1319222290030637204, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220646, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1659888000000, receivedDateStr=2022-08-08, revisedDate=1662566400000, revisedDateStr=2022-09-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456703908, onlineDateStr=2026-10-20, pubDate=1674144000000, pubDateStr=2023-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456703908, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456703908, creator=13701087609, updateTime=1792456703908, updator=13701087609, issue=Issue{id=1319222240177144549, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='1', pageStart='1', pageEnd='282', issueExtLink='null', onlineDate='null', pubDate='1674144000000', pubDateStr='2023-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456692021, creator='13701087609', updateTime=1792456863865, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319222960989262349, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319222960989262350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=163, endPage=170, ext={EN=ArticleExt(id=1319222290227769493, articleId=1319222290030637204, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Mesoporous Petal-like MgAl₂O₄, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

In the field of catalyst support and adsorption, mesoporous petal-like MgAl₂O₄ has attracted much attention because of their large surface area, abundant and accessible catalytic sites and not easy to aggregate. Mesoporous petal-like MgAl₂O₄ was prepared by a molten salt assisted non-hydrolytic sol-gel method with aluminum wire as aluminum source, magnesium powder as magnesium source, absolute ethyl alcohol as a solvent and Na₂MoO₄ as a molten salt, respectively. The effects of heat treatment temperature and soaking time on the phase composition and morphology of petal-like MgAl₂O₄ were investigated by X-ray diffraction and field emission scanning electron microscopy. The microstructure of the petal-like MgAl₂O₄ was determined by transmission electron microscopy (TEM), and the specific surface area and pore volume were measured by N₂ adsorption-desorption analysis. The results show that heat treatment temperature and soaking time both have an influence on the morphology. MgAl₂O₄ prepared has a petal-like morphology with a length of 140-160 nm when the heat treatment temperature and time are 900 ℃ and 8 h. The specific surface area of the prepared MgAl₂O₄ is 76 m²/g. Based on the results by TEM and N₂ adsorption-desorption analysis, the petal-like MgAl₂O₄ exhibits a mesoporous structure. This work paves a promising approach to prepare mesoporous petal-like MgAl₂O₄.

, authors=Qian WU¹, Guo FENG¹, Sanhai WANG², Feng JIANG², Lifeng MIAO¹, Weihui JIANG^{1, 2}, authorsList=Qian WU, Guo FENG, Sanhai WANG, Feng JIANG, Lifeng MIAO, Weihui JIANG, authorCompany=null, correspAuthors=Weihui JIANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222290500399254, articleId=1319222290030637204, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=多孔片状镁铝尖晶石的制备, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

在催化剂载体和吸附等领域，具有介孔结构的片状镁铝尖晶石因比表面积大、活性位点丰富、不易团聚等特性，受到越来越多的关注。以铝丝为铝源、镁粉为镁源、无水乙醇为溶剂，Na₂MoO₄为熔盐，采用熔盐辅助非水解溶胶-凝胶法制备多孔片状镁铝尖晶石。借助X射线衍射仪、场发射扫描电子显微镜等测试手段研究了热处理温度及保温时间对镁铝尖晶石合成与形貌的影响，运用透射电子显微镜（TEM）观察片状晶体的微观结构，采用氮气吸附脱附测试对样品的比表面积和孔径进行了表征。结果表明：热处理温度和保温时间均对镁铝尖晶石形貌有较大影响。优选热处理温度为900 ℃，保温时间为8 h，可制备出具有介孔结构的片状镁铝尖晶石，片的长度为140~160 nm。所制得样品的比表面积为76 m²/g。TEM和氮气吸附脱附曲线测试结果表明，样品存在明显的介孔结构。为制备多孔片状镁铝尖晶石提供了一种新思路。

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WU Qian (1987-), female, Doctoral candidate. E-mail: wuqian@jci.edu.cn

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WU Qian (1987-), female, Doctoral candidate. E-mail: wuqian@jci.edu.cn

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吴倩（1987—），女，博士研究生。

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吴倩（1987—），女，博士研究生。

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