Article(id=1319222264806097822, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220519, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1656259200000, receivedDateStr=2022-06-27, revisedDate=1658246400000, revisedDateStr=2022-07-20, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456697894, onlineDateStr=2026-10-20, pubDate=1674144000000, pubDateStr=2023-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456697894, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456697894, creator=13701087609, updateTime=1792456697894, updator=13701087609, issue=Issue{id=1319222240177144549, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='1', pageStart='1', pageEnd='282', issueExtLink='null', onlineDate='null', pubDate='1674144000000', pubDateStr='2023-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456692021, creator='13701087609', updateTime=1792456863865, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319222960989262349, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319222960989262350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222240177144549, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=171, endPage=177, ext={EN=ArticleExt(id=1319222265045173151, articleId=1319222264806097822, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Oriented Arrangement Silver Halide Nanorods in Glass, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The formation and directional arrangement of silver halide nanorods in glass and their influences on the polarization properties were investigated. The results show that silver halide particles are easier to precipitate in a sodium boron rich phase. The optimum heat treatment condition for the crystallization is at 615 ℃ for holding time of 12 h. The formation and orientation of silver halide nanorods in glass is a winning combination of glass stretching temperature, stress and speed. The average diameter of AgCl nanorods in glass is 98 nm, the average length is 558 nm, the average aspect ratio of the nanorods is 1∶5.6, and the nanorods are oriented along the stretching direction of glass when the stretching temperature is 570 ℃, the stress is 735 N, and the speed is 120 mm/min. According to the polarizing property of glass after high-pressure reduction, the more AgCl nanorods in the unit area of the stretched glass surface is, the higher the extinction ratio of the reduced glass will be.

, authors=Jinyang FENG, Yuna SUN, Donghua WU, Kun LEI, Xiujian ZHAO, authorsList=Jinyang FENG, Yuna SUN, Donghua WU, Kun LEI, Xiujian ZHAO, authorCompany=null, correspAuthors=Xiujian ZHAO, authorNote=

FENG Jinyang (1969-), male, Ph. D., Associate Professor. E-mail:

, correspAuthorsNote=
ZHAO Xiujian (1959-), male, Ph. D., Professor. E-mail:
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围绕含AgCl钠硼硅酸盐玻璃的熔融制备、析晶热处理、高温拉伸及高压还原工艺,对于玻璃中卤化银纳米棒的形成、定向排布以及对于偏光性能的影响规律进行了研究,发现卤化银晶粒更易于在富钠硼相中析出,较佳的热处理制度是析晶温度615 ℃、保温时间12 h。玻璃中卤化银纳米棒的形成及定向是玻璃拉伸温度、拉伸应力与拉伸速度三者的有机结合。在拉伸温度570 ℃、拉力735 N、拉伸速度120 mm/min条件下,玻璃样品中AgCl纳米棒的平均直径98 nm、平均长度558 nm、纳米棒的平均长径比1.0∶5.6,并沿玻璃拉伸方向定向排布。通过高压还原后玻璃的偏光性能研究,拉伸后玻璃表层单位面积内AgCl纳米棒的数量越多,还原处理后玻璃的消光比越高。

, authors=冯晋阳, 孙玉娜, 伍冬华, 雷堃, 赵修建, authorsList=冯晋阳, 孙玉娜, 伍冬华, 雷堃, 赵修建, authorCompany=null, correspAuthors=赵修建, authorNote=

冯晋阳(1969—),男,博士,副研究员。

, correspAuthorsNote=
赵修建(1959—),男,博士,教授。
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冯晋阳(1969—),男,博士,副研究员。

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冯晋阳(1969—),男,博士,副研究员。

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玻璃中卤化银纳米棒定向排布制备
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冯晋阳 , 孙玉娜 , 伍冬华 , 雷堃 , 赵修建
硅酸盐学报 | 研究论文 2023,51(1): 171-177
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硅酸盐学报 |研究论文 2023 , 51 (1) : 171 -177
玻璃中卤化银纳米棒定向排布制备
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冯晋阳 , 孙玉娜, 伍冬华, 雷堃, 赵修建
作者信息
  • 武汉理工大学,硅酸盐建筑材料国家重点实验室,武汉 430070
通讯作者:
赵修建(1959—),男,博士,教授。
作者简介:

冯晋阳(1969—),男,博士,副研究员。

Preparation of Oriented Arrangement Silver Halide Nanorods in Glass
Jinyang FENG , Yuna SUN, Donghua WU, Kun LEI, Xiujian ZHAO
Affiliations
  • State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070, China
  • Corresponding Author:
    ZHAO Xiujian (1959-), male, Ph. D., Professor. E-mail:

    FENG Jinyang (1969-), male, Ph. D., Associate Professor. E-mail:

出版时间: 2023-01-20 doi: 10.14062/j.issn.0454-5648.20220519
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围绕含AgCl钠硼硅酸盐玻璃的熔融制备、析晶热处理、高温拉伸及高压还原工艺,对于玻璃中卤化银纳米棒的形成、定向排布以及对于偏光性能的影响规律进行了研究,发现卤化银晶粒更易于在富钠硼相中析出,较佳的热处理制度是析晶温度615 ℃、保温时间12 h。玻璃中卤化银纳米棒的形成及定向是玻璃拉伸温度、拉伸应力与拉伸速度三者的有机结合。在拉伸温度570 ℃、拉力735 N、拉伸速度120 mm/min条件下,玻璃样品中AgCl纳米棒的平均直径98 nm、平均长度558 nm、纳米棒的平均长径比1.0∶5.6,并沿玻璃拉伸方向定向排布。通过高压还原后玻璃的偏光性能研究,拉伸后玻璃表层单位面积内AgCl纳米棒的数量越多,还原处理后玻璃的消光比越高。

玻璃  /  定向排布  /  卤化银  /  纳米棒

The formation and directional arrangement of silver halide nanorods in glass and their influences on the polarization properties were investigated. The results show that silver halide particles are easier to precipitate in a sodium boron rich phase. The optimum heat treatment condition for the crystallization is at 615 ℃ for holding time of 12 h. The formation and orientation of silver halide nanorods in glass is a winning combination of glass stretching temperature, stress and speed. The average diameter of AgCl nanorods in glass is 98 nm, the average length is 558 nm, the average aspect ratio of the nanorods is 1∶5.6, and the nanorods are oriented along the stretching direction of glass when the stretching temperature is 570 ℃, the stress is 735 N, and the speed is 120 mm/min. According to the polarizing property of glass after high-pressure reduction, the more AgCl nanorods in the unit area of the stretched glass surface is, the higher the extinction ratio of the reduced glass will be.

glass  /  orientation arrangement  /  silver halide  /  nanorod
冯晋阳, 孙玉娜, 伍冬华, 雷堃, 赵修建. 玻璃中卤化银纳米棒定向排布制备. 硅酸盐学报, 2023 , 51 (1) : 171 -177 . DOI: 10.14062/j.issn.0454-5648.20220519
Jinyang FENG, Yuna SUN, Donghua WU, Kun LEI, Xiujian ZHAO. Preparation of Oriented Arrangement Silver Halide Nanorods in Glass[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (1) : 171 -177 . DOI: 10.14062/j.issn.0454-5648.20220519
  • 湖北省先进材料领域重点研发计划(2020BAB061)
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2023年第51卷第1期
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doi: 10.14062/j.issn.0454-5648.20220519
  • 接收时间:2022-06-27
  • 首发时间:2026-10-20
  • 出版时间:2023-01-20
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  • 收稿日期:2022-06-27
  • 修回日期:2022-07-20
基金
湖北省先进材料领域重点研发计划(2020BAB061)
作者信息
    武汉理工大学,硅酸盐建筑材料国家重点实验室,武汉 430070

通讯作者:

赵修建(1959—),男,博士,教授。
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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