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Electrolysis of water to produce hydrogen is a promising green method to achieve sustainable energy supply. A NiCuP foam nickel hydrogen precipitation electrocatalyst was prepared by one-step hydrothermal method. The results show that the electrocatalyst has a good hydrogen reaction activity at 12 h at the nickel-copper ratio of 8∶1 and the hydrothermal temperature of 140 ℃. The effect of modifier on the catalytic activity was also investigated. It is indicated that the addition of the modifier NaCl can provide a better ion interaction environment, thus significantly improving the catalytic performance. At a current density of 10 mA/cm², the overpotential is 108 mV with a Tafel slope of 113 mV/dec (the overpotential change is 113 mV for every 10-fold change in current). The calculations show that the atomic d-p orbital interaction of Ni₂P-Cu₃P induces an enhancement of the electronic activity at the catalyst interface, thus reducing the activation barrier. Moreover, the addition of NaCl promotes the dissociation of H₂O molecules into H ions, thus enhancing the catalytic activity of hydrogen evolution reaction. This work provides a research basis for the research and development of transition metal electrocatalysts.

, authors=Shizhi DONG^{1, 2}, Jiaqi HE¹, Zhuang MA¹, Xudong HU¹, Jinpeng YIN¹, Hongyu HU¹, Zhiyu LIU¹, Xing ZHANG¹, authorsList=Shizhi DONG, Jiaqi HE, Zhuang MA, Xudong HU, Jinpeng YIN, Hongyu HU, Zhiyu LIU, Xing ZHANG, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222263103214481, articleId=1319222260574049161, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=一步水热法合成镍铜复合磷化物及其电催化析氢性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

电解水制氢是一种很有前途的、可以实现可持续能源供应的绿色方法。通过一步水热法，制备出性能优异的NiCuP/泡沫镍析氢电催化剂。通过调控反应条件，发现当镍铜摩尔比8∶1，水热温度140 ℃，保温时间12 h时，催化剂具有良好的析氢反应活性。此外，探究了不同的改性剂对催化活性的影响。发现改性剂NaCl的加入能提供更好的离子交互环境从而显著提升催化性能：当电流密度为10 mA/cm²时，过电位达到108 mV，Tafel斜率为113 mV/dec（电流每变化10倍，过电位变化为113 mV）。计算表明，Ni₂P-Cu₃P的原子d-p轨道相互作用诱发催化剂界面电子活性提升，显著降低了活化势垒，并且NaCl的加入对H₂O分子解离成活性H离子起到促进作用，从而提升析氢反应的催化活性。这为过渡金属电催化剂的研发提供了研究基础。

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DONG Shizhi (1981-), female, Ph.D., Associate Professor. E-mail: xiaodong8125@163.com

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DONG Shizhi (1981-), female, Ph.D., Associate Professor. E-mail: xiaodong8125@163.com

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