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Article(id=1318979413585285835, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318979383570837667, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230558, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1690646400000, receivedDateStr=2023-07-30, revisedDate=1694534400000, revisedDateStr=2023-09-13, acceptedDate=null, acceptedDateStr=null, onlineDate=1792398797651, onlineDateStr=2026-10-19, pubDate=1700409600000, pubDateStr=2023-11-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792398797651, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792398797651, creator=13701087609, updateTime=1792398797651, updator=13701087609, issue=Issue{id=1318979383570837667, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='11', pageStart='2739', pageEnd='3038', issueExtLink='null', onlineDate='null', pubDate='1700409600000', pubDateStr='2023-11-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792398790495, creator='13701087609', updateTime=1792399377667, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981846411629158, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318979383570837667, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981846411629159, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318979383570837667, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2857, endPage=2867, ext={EN=ArticleExt(id=1318979413824361165, articleId=1318979413585285835, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Modified Polyacrylate Emulsion and Durability Evaluation of Polymer Cement-Based Coating, columnId=1321891504432460086, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advanced Marine Materials—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Hydrophobic modification of cement-based coating is beneficial to improving its protective effect, but it leads to poor dispersion of coating, weakening of physical properties and durability of coating. In this paper, a highly stable/hydrophobic modified polyacrylate emulsion was prepared by using hydroxy-containing polydimethylsiloxane (PDMS) as a second oil phase, and a high durability polymer cement-based protective coating was further constructed. The modified emulsions with good stability and hydrophobicity can be obtained by matching the molecular weight and dosage of PDMS and emulsifying the shear rate. Little stratification occurs after 30 d, the contact angle of latex film is increased by 24.9%, and the water absorption is decreased by 28.94%. The prepared polymer cement-based coating has superior mechanical properties, hydrophobicity, UV aging resistance, seawater and alkali immersion resistance, and the chloride ion permeability coefficient is only 0.193×10-6 mm2/s. In addition, the modification mechanism of emulsion and the durability enhancement mechanism of coating were also analyzed.

, authors=Shuo LU1, 2, Dongbing JIANG1, 2, Qiqi LI1, 2, Pengkun HOU1, 2, Hui RONG3, Piqi ZHAO1, 2, authorsList=Shuo LU, Dongbing JIANG, Qiqi LI, Pengkun HOU, Hui RONG, Piqi ZHAO, authorCompany=null, correspAuthors=Piqi ZHAO, authorNote=

LU Shuo (1998-), male, Master candidate. E-mail:

, correspAuthorsNote=
ZHAO Piqi (1987-), male, Ph.D., Professor. E-mail:
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水泥基涂层疏水化改性处理是提高其防护效果的有效途径，然而有机硅烷类疏水性材料存在分散性差、弱化涂层物理性能及耐久性的问题。以含羟基聚二甲基硅氧烷为第二油相（PDMS），采用一步法高速剪切乳化工艺实现了高稳定/疏水型改性聚丙烯酸酯乳液的制备，并进一步构建了高耐久聚合物水泥基防护涂层。研究结果表明：相匹配的PDMS分子量、掺量、剪切速率可获得兼具良好稳定性和疏水性的改性乳液，乳液30 d未见分层现象、乳胶膜接触角提高24.9%、吸水率降低28.94%；制备的聚合物水泥基涂层展现了优异的力学性能、疏水性、耐紫外老化、耐海水和碱溶液浸泡性能，氯离子渗透系数仅为0.193×10-6 mm2/s；分析了乳液的改性机理与涂层耐久性增强机制。

, authors=卢烁1, 2, 姜东兵1, 2, 李琦琦1, 2, 侯鹏坤1, 2, 荣辉3, 赵丕琪1, 2, authorsList=卢烁, 姜东兵, 李琦琦, 侯鹏坤, 荣辉, 赵丕琪, authorCompany=null, correspAuthors=赵丕琪, authorNote=

卢烁（1998—），男，硕士研究生。

, correspAuthorsNote=
赵丕琪（1987—），男，博士，教授。
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LU Shuo (1998-), male, Master candidate. E-mail:

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LU Shuo (1998-), male, Master candidate. E-mail:

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卢烁（1998—），男，硕士研究生。

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卢烁（1998—），男，硕士研究生。

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改性聚丙烯酸酯乳液的制备及聚合物水泥基涂层耐久性评价
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卢烁 1, 2 , 姜东兵 1, 2 , 李琦琦 1, 2 , 侯鹏坤 1, 2 , 荣辉 3 , 赵丕琪 1, 2
硅酸盐学报 | 先进海洋材料专题—研究论文 2023,51(11): 2857-2867
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硅酸盐学报 |先进海洋材料专题—研究论文 2023 , 51 (11) : 2857 -2867
改性聚丙烯酸酯乳液的制备及聚合物水泥基涂层耐久性评价
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卢烁1, 2 , 姜东兵1, 2, 李琦琦1, 2, 侯鹏坤1, 2, 荣辉3, 赵丕琪1, 2
作者信息
  • 1．济南大学，山东省建筑材料制备与测试技术重点实验室，济南 250022
  • 2．济南大学材料科学与工程学院，济南 250022
  • 3．天津城建大学材料科学与工程学院，天津 300192
通讯作者:
赵丕琪（1987—），男，博士，教授。
作者简介:

卢烁（1998—），男，硕士研究生。

Preparation of Modified Polyacrylate Emulsion and Durability Evaluation of Polymer Cement-Based Coating
Shuo LU1, 2 , Dongbing JIANG1, 2, Qiqi LI1, 2, Pengkun HOU1, 2, Hui RONG3, Piqi ZHAO1, 2
Affiliations
  • 1.Shandong Provincial Key Lab of Preparation and Measurement of Building Materials, University of Jinan, Jinan 250022, China
  • 2.School of Materials Science and Engineering, University of Jinan, Jinan 250022, China
  • 3.School of Materials Science and Engineering, Tianjin Chengjian University, Tianjin 300192, China
    • Corresponding Author:
    ZHAO Piqi (1987-), male, Ph.D., Professor. E-mail:

    LU Shuo (1998-), male, Master candidate. E-mail:

出版时间: 2023-11-20 doi: 10.14062/j.issn.0454-5648.20230558
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水泥基涂层疏水化改性处理是提高其防护效果的有效途径，然而有机硅烷类疏水性材料存在分散性差、弱化涂层物理性能及耐久性的问题。以含羟基聚二甲基硅氧烷为第二油相（PDMS），采用一步法高速剪切乳化工艺实现了高稳定/疏水型改性聚丙烯酸酯乳液的制备，并进一步构建了高耐久聚合物水泥基防护涂层。研究结果表明：相匹配的PDMS分子量、掺量、剪切速率可获得兼具良好稳定性和疏水性的改性乳液，乳液30 d未见分层现象、乳胶膜接触角提高24.9%、吸水率降低28.94%；制备的聚合物水泥基涂层展现了优异的力学性能、疏水性、耐紫外老化、耐海水和碱溶液浸泡性能，氯离子渗透系数仅为0.193×10-6 mm2/s；分析了乳液的改性机理与涂层耐久性增强机制。

聚丙烯酸酯  /  聚二甲基硅氧烷  /  水泥基涂层  /  耐久性  /  海工混凝土防护

Hydrophobic modification of cement-based coating is beneficial to improving its protective effect, but it leads to poor dispersion of coating, weakening of physical properties and durability of coating. In this paper, a highly stable/hydrophobic modified polyacrylate emulsion was prepared by using hydroxy-containing polydimethylsiloxane (PDMS) as a second oil phase, and a high durability polymer cement-based protective coating was further constructed. The modified emulsions with good stability and hydrophobicity can be obtained by matching the molecular weight and dosage of PDMS and emulsifying the shear rate. Little stratification occurs after 30 d, the contact angle of latex film is increased by 24.9%, and the water absorption is decreased by 28.94%. The prepared polymer cement-based coating has superior mechanical properties, hydrophobicity, UV aging resistance, seawater and alkali immersion resistance, and the chloride ion permeability coefficient is only 0.193×10-6 mm2/s. In addition, the modification mechanism of emulsion and the durability enhancement mechanism of coating were also analyzed.

polyacrylate  /  polydimethylsiloxane  /  cement-based coating  /  durability  /  marine concrete protection
卢烁, 姜东兵, 李琦琦, 侯鹏坤, 荣辉, 赵丕琪. 改性聚丙烯酸酯乳液的制备及聚合物水泥基涂层耐久性评价. 硅酸盐学报, 2023 , 51 (11) : 2857 -2867 . DOI: 10.14062/j.issn.0454-5648.20230558
Shuo LU, Dongbing JIANG, Qiqi LI, Pengkun HOU, Hui RONG, Piqi ZHAO. Preparation of Modified Polyacrylate Emulsion and Durability Evaluation of Polymer Cement-Based Coating[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (11) : 2857 -2867 . DOI: 10.14062/j.issn.0454-5648.20230558
基金
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  • 国家自然科学基金(52172021)
  • 国家重点研发计划(2021YFB 3802002)
  • 山东省优秀青年科学基金(ZR2023YQ041)
  • 山东省自然科学基金(ZR2021ME123)
  • 泰山学者计划
  • 山东省高校青年科研人员科技创新支持计划(2019KJA017)
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2023年第51卷第11期
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doi: 10.14062/j.issn.0454-5648.20230558
  • 接收时间：2023-07-30
  • 首发时间：2026-10-19
  • 出版时间：2023-11-20
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  • 收稿日期：2023-07-30
  • 修回日期：2023-09-13
基金
国家自然科学基金(52172021)
国家重点研发计划(2021YFB 3802002)
山东省优秀青年科学基金(ZR2023YQ041)
山东省自然科学基金(ZR2021ME123)
泰山学者计划
山东省高校青年科研人员科技创新支持计划(2019KJA017)
作者信息
    1．济南大学，山东省建筑材料制备与测试技术重点实验室，济南 250022
    2．济南大学材料科学与工程学院，济南 250022
    3．天津城建大学材料科学与工程学院，天津 300192

通讯作者:

赵丕琪（1987—），男，博士，教授。
参考文献
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20230558
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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