Article(id=1318978582894985991, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318978537852359595, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230293, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1683129600000, receivedDateStr=2023-05-04, revisedDate=1684252800000, revisedDateStr=2023-05-17, acceptedDate=null, acceptedDateStr=null, onlineDate=1792398599598, onlineDateStr=2026-10-19, pubDate=1697731200000, pubDateStr=2023-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792398599598, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792398599598, creator=13701087609, updateTime=1792398599598, updator=13701087609, issue=Issue{id=1318978537852359595, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='10', pageStart='2517', pageEnd='2738', issueExtLink='null', onlineDate='null', pubDate='1697731200000', pubDateStr='2023-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792398588860, creator='13701087609', updateTime=1792399337892, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981679578993157, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318978537852359595, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981679578993158, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318978537852359595, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2653, endPage=2661, ext={EN=ArticleExt(id=1318978583125672712, articleId=1318978582894985991, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Performance of Al₂O₃/Glass-Ceramic Composite Sealing Materials for Intermediate Temperature Solid Oxide Fuel Cell, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

To provide direction and guidance for the microstructure design and development of sealing materials for high-performance intermediate-temperature solid oxide fuel cell, a Al₂O₃/BaO-CaO-B₂O₃-Al₂O₃-SiO₂ glass-ceramic (BCBAS)-based composite sealing material with superior mechanical properties and a high thermal conductivity was prepared via tape casting. According to the analysis by scanning electron microscopy and X-ray diffraction, the lamellar Al₂O₃ is regularly distributed in the BCBAS glass-ceramic matrix. The main crystallization phase of BCBAS glass transforms from Ca_0.1Ba_0.9SiO₃ into Ba_1.55Ca_0.45SiO₄ and BaAl₂Si₂O₈, and further into BaAl₂Si₂O₈ and BaAl₂O₄ phases when the lamellar Al₂O₃ content increases from 0 to 25% (in mass fraction). The thermal conductivity of biomimetic sealants increases from 0.892 W/(m·K) to 1.255 W/(m·K), and the bending strength and Vickers hardness with higher than 10 of the Weibull modulus β increase from 96 MPa to 140 MPa and 444 HV to 677 HV as the lamellar Al₂O₃ content increases from 0 to 25% (in mass fraction), indicating the mechanical properties and thermal conductivity of the sealant. The sealing tensile strength of the biomimetic sealant with the mass fraction of lamellar Al₂O₃≤20% maintains above 4 MPa. The composite with 20% Al₂O₃-80% BCBAS glass exhibits the superior comprehensive properties (i.e., thermal conductivity of 1.203 W/(m·K), bending toughness of 136 MPa, Vickers hardness of 677 and sealing strength at 4.22 MPa), thus being a potential candidate for application of intermediate- temperature solid oxide fuel cell.

, authors=Yunxiang SI^{1, 2}, Shangke PAN¹, Haishen REN², Huixin LIN², authorsList=Yunxiang SI, Shangke PAN, Haishen REN, Huixin LIN, authorCompany=null, correspAuthors=Haishen REN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1318978583389913865, articleId=1318978582894985991, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=用于中温固体氧化物燃料电池的Al₂O₃/微晶玻璃复合密封材料的制备与性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

通过流延法制备了一种新型的Al₂O₃/BaO-CaO-B₂O₃-Al₂O₃-SiO₂微晶玻璃（BCBAS）系复合密封材料，其具有突出的机械性能和较高的导热性能。结果表明，片状Al₂O₃可有规律定向分布在BCBAS玻璃基体中。随着片状Al₂O₃质量分数从0增加到25%，BCBAS玻璃的主要结晶相从Ca_0.1Ba_0.9SiO₃转变为Ba_1.55Ca_0.45SiO₄和BaAl₂Si₂O₈，并进一步转变为BaAl₂Si₂O₈和BaAl₂O₄相。同时复合密封材料的导热系数从0.892 W/（m·K）增加到1.255 W/（m·K），弯曲强度和Vickers硬度分别从96 MPa增加到140 MPa，444 HV增加到677 HV。当片状Al₂O₃的质量分数不大于20%时，密封材料与连接件之间的抗拉强度保持在4 MPa以上。20% Al₂O₃~80% BCBAS微晶玻璃的复合密封材料表现出优异的综合性能：导热系数为1.203 W/（m·K）、弯曲强度为136 MPa、Vickers硬度为677 HV、密封件的抗拉强度为4.22 MPa，在抗热震性能上体现出较大的优势，使其成为中温固体氧化物燃料电池密封应用的潜在候选材料。

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²Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China, bio={"content":"

SI Yunxiang (1995-), male, Master candidate. E-mail: 2011086135@nbu.edu.cn

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SI Yunxiang (1995-), male, Master candidate. E-mail: 2011086135@nbu.edu.cn

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司运祥（1995—），男，硕士研究生。

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司运祥（1995—），男，硕士研究生。

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