Article(id=1318977218278174981, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230083, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1676908800000, receivedDateStr=2023-02-21, revisedDate=1680969600000, revisedDateStr=2023-04-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1792398274249, onlineDateStr=2026-10-19, pubDate=1694102400000, pubDateStr=2023-09-08, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792398274249, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792398274249, creator=13701087609, updateTime=1792398274249, updator=13701087609, issue=Issue{id=1318977205884014990, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='12', pageStart='3039', pageEnd='3250', issueExtLink='null', onlineDate='null', pubDate='1703001600000', pubDateStr='2023-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792398271294, creator='13701087609', updateTime=1792399409679, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981980671295626, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981980671295627, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3083, endPage=3094, ext={EN=ArticleExt(id=1318977218496278790, articleId=1318977218278174981, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Electrochemical Properties of BaZr_0.76-xY_0.2Pr_xNi_0.04O_3-δ Proton Conductors, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Y-doped BaZrO₃ proton conductor has been extensively studied due to its outstanding chemical stability. However, the high sintering temperature has limited its practical application. To enhance the sintering activity of BaZrO₃, we co-doped Y-BaZrO₃ with Pr³⁺ and Ni²⁺, and investigated its microscopic morphology and electrochemical properties. The introduction of Ni forms a solid solution with the sample, while Pr³⁺ doping increases the grain size, a critical factor for the densification process. XPS, Raman and EPR results reveal that a small amount of Pr³⁺ doping significantly raises the concentration of oxygen vacancies in the materials. This increase promotes proton incorporation by accelerating the dissociation and adsorption of water, thereby facilitating the proton conduction. However, it's important to note that excessive Pr³⁺ doping leads to a high concentration of oxygen vacancies, which triggers a defect association reaction. Consequently, this results in a slight decrease in conductivity at low temperatures. On the other hand, as the temperature increases, the hydrogen permeability of the membrane increases also rises. Moreover, the hydrogen permeability of BaZr_0.66Y_0.2Pr_0.1Ni_0.04O_3-δ is found to be higher than that of BaZr_0.71Y_0.2Pr_0.05Ni_0.04O_3-δ, with the former reaching 2.60×10^-8 mol·cm^-2·s^-1 at 1 173 K. Notably, these membranes exhibit remarkable in CO₂-containing atmosphere indicating excellent resistance to CO₂.

, authors=Jing WANG, Chunli YANG, Hao ZHANG, Qingtao SHEN, Weiji CAO, Jun LI, Wei YAO, Lei WANG, authorsList=Jing WANG, Chunli YANG, Hao ZHANG, Qingtao SHEN, Weiji CAO, Jun LI, Wei YAO, Lei WANG, authorCompany=null, correspAuthors=Chunli YANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1318977218798268679, articleId=1318977218278174981, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=BaZr_0.76-xY_0.2Pr_xNi_0.04O_3-δ质子导体的电化学性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

Y掺杂的BaZrO₃因其优异的化学稳定性而被广泛研究。然而，较高的烧结温度限制了其应用。为改善BaZrO₃的烧结活性，对Y-BaZrO₃采用Pr³⁺和Ni²⁺进行共掺杂，并对其微观形貌及电化学性能进行研究。Ni与材料形成固溶体，Pr³⁺的掺杂增大了晶粒尺寸，这对致密化过程极为重要。XPS、Raman和EPR结果表明，少量Pr³⁺掺杂可以增加材料的氧空位含量，并通过加速水的解离和吸附促进质子进入，从而促进质子传导。然而，过量Pr³⁺掺杂导致的高浓度氧空位会产生缺陷缔合反应，使低温下的电导率略有下降。随着温度的升高，氢分离膜的氢渗透性也增加。此外，BaZr_0.66Y_0.2Pr_0.1Ni_0.04O_3-δ的氢渗透性高于BaZr_0.71Y_0.2Pr_0.05Ni_0.04O_3-δ，在1 173 K时，氢渗透性达到2.60×10^-8 mol·cm^-2·s^-1。

, authors=王靖, 杨春利, 张浩, 申清涛, 曹伟际, 李俊, 姚伟, 王雷, authorsList=王靖, 杨春利, 张浩, 申清涛, 曹伟际, 李俊, 姚伟, 王雷, authorCompany=null, correspAuthors=杨春利, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=hVhkpoAKqyCiWK+gzRLzFw==, magXml=nf5Y1ttMc3Ir97GiggzGBw==, pdfUrl=null, pdf=mTTzGgTHxDnhJ4kfb6J+CQ==, pdfFileSize=997504, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=n+zhX0wAP6cxYhBJaPyBBw==, mapNumber=null, fund=null)}, authors=[Author(id=1318977219075092748, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1318977218278174981, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=958797695@qq.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1318977219158978830, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1318977218278174981, authorId=1318977219075092748, language=EN, stringName=Jing WANG, firstName=Jing, middleName=null, lastName=WANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=College of Materials Science and Engineering, Xi'an University of Architecture and Technology, Xi'an 710055, China, bio={"content":"

WANG Jing (1998-), male, Master. E-mail: 958797695@qq.com

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WANG Jing (1998-), male, Master. E-mail: 958797695@qq.com

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王靖（1998—），男，硕士研究生。

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王靖（1998—），男，硕士研究生。

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