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Article(id=1318974538155667567, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230018, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1673452800000, receivedDateStr=2023-01-12, revisedDate=1676131200000, revisedDateStr=2023-02-12, acceptedDate=null, acceptedDateStr=null, onlineDate=1792397635257, onlineDateStr=2026-10-19, pubDate=1685289600000, pubDateStr=2023-05-29, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792397635257, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792397635257, creator=13701087609, updateTime=1792397635257, updator=13701087609, issue=Issue{id=1318974513019207979, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='7', pageStart='1649', pageEnd='1882', issueExtLink='null', onlineDate='null', pubDate='1689782400000', pubDateStr='2023-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792397629265, creator='13701087609', updateTime=1792399256269, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981337223119779, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981337223119780, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1783, endPage=1791, ext={EN=ArticleExt(id=1318974538352799856, articleId=1318974538155667567, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Influence of Saline Sulfuric Acid Treatment on Vermiculite Process and Its Mechanism, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The study of weathering alteration of phyllosilicate minerals is of great significance for understanding the chemical cycle of the earth surface, soil formation and environmental changes. A phlogopite from Xinjiang, China was used as a raw material to control the oxidation environment, pH value, ion species and concentration of sulfuric acid solution in the process of phlogopite vermiculization. The phase, composition release law, spectroscopic properties and thermal properties were characterized by X-ray diffraction, inductive coupled plasma emission spectroscopy, Fourier transform infrared spectroscopy, and thermogravimetry-differential scanning calorimetry, respectively. The results show that the degree of vermiculite increases with the increase of Mg2+ ions concentration in the solution, but the less conversion effect exists at a certain H2O2 content in the solution. The conversion effect can be enhanced after the use of sulfuric acid to adjust the solution pH value, because the acidic environment can improve the oxidation capacity of hydrogen peroxide and the increase of SO42- ions concentration. The more jarosite substances are formed, thus accelerating the process of vermiculization.

, authors=Shaokun HUANG1, 2, Liming LUO2, 3, Hongjuan SUN1, 2, Tongjiang PENG2, Shize CHEN1, 2, authorsList=Shaokun HUANG, Liming LUO, Hongjuan SUN, Tongjiang PENG, Shize CHEN, authorCompany=null, correspAuthors=Liming LUO, authorNote=

HUANG Shaokun (1997-), male, Master candidate. E-mail:

, correspAuthorsNote=
LUO Liming (1986-), male, Ph.D., Associate Professor. E-mail:
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层状硅酸盐矿物的风化蚀变研究对于了解地球表层化学循环、土壤的形成及环境变化等具有重要意义。本工作基于金云母在氧化环境下易转化形成金云母-蛭石或蛭石的特性，以新疆尉犁金云母为原料，通过改变硫酸溶液的氧化环境、pH值、溶液阳离子浓度等，调控金云母的蛭石化过程；利用X射线衍射、电感耦合等离子发射光谱、红外光谱、热重等分析手段，研究了硫酸溶液pH值、阳离子浓度等对金云母蛭石化过程中组分释出的规律，产物的物相、谱学特性和热学性能的影响。结果表明：在溶液中H2O2质量分数不变的情况下，随着溶液中Mg2+浓度的增加，金云母的蛭石化程度会逐渐增强，但转化效果有限，使用硫酸调节溶液pH值后，转化效果会进一步加强，这是由于酸性环境会提高双氧水的氧化能力，同时SO42-浓度的增加，会生成更多的黄钾铁矾，从而加速金云母的蛭石化。

, authors=黄少坤1, 2, 罗利明2, 3, 孙红娟1, 2, 彭同江2, 陈仕泽1, 2, authorsList=黄少坤, 罗利明, 孙红娟, 彭同江, 陈仕泽, authorCompany=null, correspAuthors=罗利明, authorNote=

黄少坤（1997—），男，硕士研究生。

, correspAuthorsNote=
罗利明（1986—），男，博士，副教授。
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HUANG Shaokun (1997-), male, Master candidate. E-mail:

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黄少坤（1997—），男，硕士研究生。

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含盐硫酸溶液对金云母蛭石化过程的影响及作用机制
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黄少坤 1, 2 , 罗利明 2, 3 , 孙红娟 1, 2 , 彭同江 2 , 陈仕泽 1, 2
硅酸盐学报 | 研究论文 2023,51(7): 1783-1791
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硅酸盐学报 |研究论文 2023 , 51 (7) : 1783 -1791
含盐硫酸溶液对金云母蛭石化过程的影响及作用机制
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HUANG Shaokun (1997-), male, Master candidate. E-mail:

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黄少坤（1997—），男，硕士研究生。

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黄少坤1, 2 , 罗利明2, 3 , 孙红娟1, 2, 彭同江2, 陈仕泽1, 2
作者信息
  • 1．西南科技大学环境与资源学院，四川 绵阳 621010
  • 2．西南科技大学矿物材料及应用研究所，四川 绵阳 621010
  • 3．西南科技大学，核废物与环境安全国防重点学科实验室，四川 绵阳 621010
通讯作者:
罗利明（1986—），男，博士，副教授。
作者简介:

黄少坤（1997—），男，硕士研究生。

Influence of Saline Sulfuric Acid Treatment on Vermiculite Process and Its Mechanism
Shaokun HUANG1, 2 , Liming LUO2, 3 , Hongjuan SUN1, 2, Tongjiang PENG2, Shize CHEN1, 2
Affiliations
  • 1.School of Environment and Resources, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
  • 2.Institute of Mineral Materials and Application, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
  • 3.Fundamental Science on Nuclear Wastes and Environmental Safety Laboratory, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
    • Corresponding Author:
    LUO Liming (1986-), male, Ph.D., Associate Professor. E-mail:

    HUANG Shaokun (1997-), male, Master candidate. E-mail:

出版时间: 2023-05-29 doi: 10.14062/j.issn.0454-5648.20230018
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层状硅酸盐矿物的风化蚀变研究对于了解地球表层化学循环、土壤的形成及环境变化等具有重要意义。本工作基于金云母在氧化环境下易转化形成金云母-蛭石或蛭石的特性，以新疆尉犁金云母为原料，通过改变硫酸溶液的氧化环境、pH值、溶液阳离子浓度等，调控金云母的蛭石化过程；利用X射线衍射、电感耦合等离子发射光谱、红外光谱、热重等分析手段，研究了硫酸溶液pH值、阳离子浓度等对金云母蛭石化过程中组分释出的规律，产物的物相、谱学特性和热学性能的影响。结果表明：在溶液中H2O2质量分数不变的情况下，随着溶液中Mg2+浓度的增加，金云母的蛭石化程度会逐渐增强，但转化效果有限，使用硫酸调节溶液pH值后，转化效果会进一步加强，这是由于酸性环境会提高双氧水的氧化能力，同时SO42-浓度的增加，会生成更多的黄钾铁矾，从而加速金云母的蛭石化。

金云母  /  蛭石化  /  氧化电势  /  组分释出

The study of weathering alteration of phyllosilicate minerals is of great significance for understanding the chemical cycle of the earth surface, soil formation and environmental changes. A phlogopite from Xinjiang, China was used as a raw material to control the oxidation environment, pH value, ion species and concentration of sulfuric acid solution in the process of phlogopite vermiculization. The phase, composition release law, spectroscopic properties and thermal properties were characterized by X-ray diffraction, inductive coupled plasma emission spectroscopy, Fourier transform infrared spectroscopy, and thermogravimetry-differential scanning calorimetry, respectively. The results show that the degree of vermiculite increases with the increase of Mg2+ ions concentration in the solution, but the less conversion effect exists at a certain H2O2 content in the solution. The conversion effect can be enhanced after the use of sulfuric acid to adjust the solution pH value, because the acidic environment can improve the oxidation capacity of hydrogen peroxide and the increase of SO42- ions concentration. The more jarosite substances are formed, thus accelerating the process of vermiculization.

phlogopite  /  vermiculization  /  oxidation electric potential  /  release of components
黄少坤, 罗利明, 孙红娟, 彭同江, 陈仕泽. 含盐硫酸溶液对金云母蛭石化过程的影响及作用机制. 硅酸盐学报, 2023 , 51 (7) : 1783 -1791 . DOI: 10.14062/j.issn.0454-5648.20230018
Shaokun HUANG, Liming LUO, Hongjuan SUN, Tongjiang PENG, Shize CHEN. Influence of Saline Sulfuric Acid Treatment on Vermiculite Process and Its Mechanism[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (7) : 1783 -1791 . DOI: 10.14062/j.issn.0454-5648.20230018
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  • 国家自然科学基金项目(42002039; 42072048; 41972042)
  • 四川省科技厅项目(21ZHSF0157)
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2023年第51卷第7期
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doi: 10.14062/j.issn.0454-5648.20230018
  • 接收时间：2023-01-12
  • 首发时间：2026-10-19
  • 出版时间：2023-05-29
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  • 收稿日期：2023-01-12
  • 修回日期：2023-02-12
基金
国家自然科学基金项目(42002039; 42072048; 41972042)
四川省科技厅项目(21ZHSF0157)
作者信息
    1．西南科技大学环境与资源学院，四川 绵阳 621010
    2．西南科技大学矿物材料及应用研究所，四川 绵阳 621010
    3．西南科技大学，核废物与环境安全国防重点学科实验室，四川 绵阳 621010

通讯作者:

罗利明（1986—），男，博士，副教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20230018
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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