Article(id=1318974532518527409, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230063, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1676131200000, receivedDateStr=2023-02-12, revisedDate=1677686400000, revisedDateStr=2023-03-02, acceptedDate=null, acceptedDateStr=null, onlineDate=1792397633913, onlineDateStr=2026-10-19, pubDate=1686240000000, pubDateStr=2023-06-09, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792397633913, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792397633913, creator=13701087609, updateTime=1792397633913, updator=13701087609, issue=Issue{id=1318974513019207979, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='7', pageStart='1649', pageEnd='1882', issueExtLink='null', onlineDate='null', pubDate='1689782400000', pubDateStr='2023-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792397629265, creator='13701087609', updateTime=1792399256269, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981337223119779, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981337223119780, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974513019207979, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1746, endPage=1755, ext={EN=ArticleExt(id=1318974533399331250, articleId=1318974532518527409, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Microstructure Regulation Through W⁶⁺ Doping to Boost Cycling Stability of LiNi_0.9Co_0.1O₂ Ni-Rich Cathode Materials, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The applications such as electric vehicles require a high energy density in lithium-ion batteries. LiNi_0.9Co_0.1O₂ has attracted much attention, which has a potential to be next-generation cathode material due to its high specific capacity and reasonable cost. However, some related issues such as Li/Ni mixing, microcracks and surface side reactions caused by H2-H3 phase transformation result in a poor cycling stability for LiNi_0.9Co_0.1O₂. In this paper, the microstructures of LiNi_0.9Co_0.1O₂ by W⁶⁺ doping were regulated by an effective method to adjust the surface energy of the primary particles and transform the disordered and irregular-shape primary particles into the well-ordered radially-aligned elongated shape particles. This microstructure feature can suppress the stress accumulation and the formation of micro-cracks in LiNi_0.9Co_0.1O₂, and provide abundant diffusion channels for Li⁺, thus improving the cycling stability and rate performance of LiNi_0.9Co_0.1O₂ cathode materials. The discharge capacities of 1% (in mole fraction) W-doped LiNi_0.9Co_0.1O₂ are 231.2 mA·h/g at 0.1 C and 213.3 mA·h/g at 0.5 C, respectively, with a high capacity retention of 93% after 150 cycles. This microstructure regulation strategy provides an effective approach for improving the cycling stability of LiNi_0.9Co_0.1O₂ Ni-rich cathode materials.

, authors=Afei LI¹, Chengzhi HU¹, Can WANG¹, Shicheng CAO¹, Weijian TANG¹, Zhibao LIU², Kai CHEN², Changping WANG², Zhangxian CHEN¹, authorsList=Afei LI, Chengzhi HU, Can WANG, Shicheng CAO, Weijian TANG, Zhibao LIU, Kai CHEN, Changping WANG, Zhangxian CHEN, authorCompany=null, correspAuthors=Zhangxian CHEN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1318974533944590771, articleId=1318974532518527409, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=W⁶⁺掺杂调控微结构增强LiNi_0.9Co_0.1O₂高镍正极材料的循环稳定性, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

电动汽车等应用领域对锂离子电池能量密度的需求日益增长，LiNi_0.9Co_0.1O₂因其高比容量和价格适中等优势受到了广泛的关注，有潜力成为下一代锂离子电池正极材料。然而，锂镍混排、H2-H3相变引起的微裂纹和表面副反应等问题导致LiNi_0.9Co_0.1O₂的充放电循环稳定性较差。通过掺杂W⁶⁺对LiNi_0.9Co_0.1O₂的微结构进行了有效调控，并调节一次晶粒的表面能使其由无序堆积的不规则形状转变为径向有序排列的细长条状。该微结构特征可以抑制LiNi_0.9Co_0.1O₂的应力累积和微裂纹的形成，同时为Li⁺提供了丰富的扩散通道，有效提高了LiNi_0.9Co_0.1O₂正极材料的循环稳定性和倍率性能。当W⁶⁺掺杂量为1%（摩尔分数）时，LiNi_0.9Co_0.1O₂改性样品在0.1 C倍率下的放电比容量高达231.2 mA·h/g，在0.5 C倍率下放电比容量为213.3 mA·h/g，循环150次后容量保持率达93%。该微结构调控策略为提高LiNi_0.9Co_0.1O₂高镍正极材料的循环稳定性提供了一种思路。

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LI Afei (1995-), male, Master candidate. E-mail: liaf1129@163.com

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李阿飞（1995—），男，硕士研究生。

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李阿飞（1995—），男，硕士研究生。

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