Article(id=1320095768510312675, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320095743872971684, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20250565, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1752854400000, receivedDateStr=2025-07-19, revisedDate=1758643200000, revisedDateStr=2025-09-24, acceptedDate=null, acceptedDateStr=null, onlineDate=1792664957405, onlineDateStr=2026-10-22, pubDate=1778601600000, pubDateStr=2026-05-13, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792664957405, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792664957405, creator=13701087609, updateTime=1792664957405, updator=13701087609, issue=Issue{id=1320095743872971684, tenantId=1146029695717560320, journalId=1263187385517883426, year='2026', volume='54', issue='6', pageStart='1881', pageEnd='2170', issueExtLink='null', onlineDate='null', pubDate='1781884800000', pubDateStr='2026-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792664951531, creator='13701087609', updateTime=1792738533970, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1320404371276411812, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320095743872971684, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1320404371276411813, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1320095743872971684, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2057, endPage=2071, ext={EN=ArticleExt(id=1320095768703250660, articleId=1320095768510312675, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Ca-Mg-Al-Si Corrosion Resistance Behavior and Mechanism of Plasma Sprayed (Eu
0.2Gd
0.2Er
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0.2)
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2O
7 Thermal Barrier Coatings, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=
Introduction Thermal barrier coatings (TBCs) are crucial for protecting aero-engine components against high-temperature and corrosive environments. Conventional yttria-stabilized zirconia (YSZ) coatings undergo phase transformation and degradation at high temperatures of > 1250 ℃, while accelerating their failure process particularly under Ca-Mg-Al-Si (CMAS) attack. The emergence of high-entropy ceramics can give an effective pathway for the development of advanced thermal barrier coating materials. Some studies demonstrate that the incorporation of multiple rare-earth elements endows high-entropy rare-earth zirconates with a lower thermal conductivity, a better phase stability, and a superior corrosion resistance, compared to YSZ. However, the existing research predominantly focuses on rare-earth zirconate materials or process optimization of conventional YSZ coatings, while studies on the atmospheric plasma spraying (APS) preparation process of high-entropy rare-earth zirconate coatings as well as their CMAS erosion behavior and dynamic reaction mechanisms remain insufficient. This study was to thus investigate the CMAS erosion behavior of atmospheric plasma-sprayed high-entropy rare-earth zirconate (Eu0.2Gd0.2Er0.2Tm0.2Yb0.2)2Zr2O7 thermal barrier coatings. In addition, the regulatory mechanism of high-entropy design on the CMAS erosion resistance of the coatings was also revealed via systematically analyzing the microstructural evolution, phase transformation, and chemical reaction kinetics under high-temperature CMAS environments.
Methods High-entropy (Eu0.2Gd0.2Er0.2Tm0.2Yb0.2)2Zr2O7 (EGETYZ) powder was synthesized via solid-state reaction and subsequent spray granulation to produce spherical particles suitable for APS. Coatings were applied on nickel-based alloy substrates with varying spraying distances (i.e., 80, 100 mm and 120 mm) to optimize the microstructure. The CMAS corrosion tests were conducted at different temperatures (i.e., 1300, 1400 ℃ and 1500 ℃) with a synthetic CMAS composition (33CaO-9MgO-13AlO1.5-45SiO2). The phase composition was analyzed by X-ray diffraction (XRD), the surface roughness was determined by laser confocal microscopy (LCM), and the microstructure/elemental distribution was characterized by scanning electron microscopy with energy-dispersive spectroscopy (SEM-EDS).
Results and discussion The results show that the high-entropy zirconate coating exhibits a defect-fluorite structure with a minimal surface roughness (2.72 μm) and a low porosity (10.10%) at an 80 mm spraying distance. At 1300 ℃, the CMAS corrosion forms a dense reaction layer of apatite and fluorite, effectively limiting a penetration (i.e., 19.7 μm after 5 h). At 1400 ℃, a three-layer reaction structure emerges, with an increased penetration (i.e., 95.2 μm). At 1500 ℃, a penetration deepeneds significantly (i.e., 321.1 μm), with sparse apatite and prevalent gehlenite and transitional phases. Higher temperatures reduce the CMAS viscosity (by up to 77.57%), accelerating infiltration along coating defects. The dense reaction layer at lower temperatures is a key to corrosion resistance, while a rapid CMAS penetration at higher temperatures hinders its formation.
Conclusions The EGETYZ coating exhibited the superior resistance to the CMAS corrosion. The corrosion temperature directly affected the viscosity change of CMAS, thereby exerting a significant influence on the corrosion behavior and reaction products. At 1300 ℃, the reaction layer was mainly composed of fluorite and apatite, forming a dense structure that effectively inhibited the CMAS infiltration. At 1400 ℃, the EGETYZ at the bottom of the reaction layer was not completely melted. The elements Al/Mg enriched in the gaps, in synergy with elements Ca/Si/RE, form a rare-earth gehlenite solid solution, resulting in a three-layer structure of the reaction layer (i.e., pure fluorite at the top, fluorite and apatite in the middle, and gehlenite-containing phase at the bottom). At 1500 ℃, only a minimal amount of apatite phase appeared, the degree of EGETYZ melting was relatively low, and it was not completely transformed into the fluorite phase, with the gehlenite phase distributing more extensively. To enhance the CMAS corrosion resistance of high-entropy rare-earth zirconate thermal barrier coatings, the key could lie in promoting the reaction with the CMAS to form a continuous and dense reaction layer. All the formed reaction products could effectively consume the CMAS components.
, authors=Shihua ZHANG, Kunying DING, Jianhai YU, Tao ZHANG, Jintao LU, Jiaxi YUAN, authorsList=Shihua ZHANG, Kunying DING, Jianhai YU, Tao ZHANG, Jintao LU, Jiaxi YUAN, authorCompany=null, correspAuthors=Kunying DING, authorNote=
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0.2Gd
0.2Er
0.2Tm
0.2Yb
0.2)
2Zr
2O
7热障涂层的钙镁铝硅酸盐侵蚀行为, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=
基于航空发动机对新型高性能热障涂层的需求，采用大气等离子喷涂的方式制备高熵稀土锆酸盐（Eu0.2Gd0.2Er0.2Tm0.2Yb0.2）2Zr2O7热障涂层，研究其在1300、1400 ℃和1500 ℃温度条件下钙镁铝硅酸盐（CMAS）对涂层的侵蚀行为，系统分析了高熵涂层的腐蚀反应机理。结果表明：温度显著影响CMAS在涂层中的侵蚀程度。在较低温度（1300 ℃条件下），CMAS与涂层间反应生成磷灰石和萤石，形成致密反应层，有效阻挡CMAS持续渗透。随着腐蚀温度升高（1400 ℃和1500 ℃），CMAS黏度降低，加速CMAS沿涂层缺陷渗透的速率，导致致密反应层无法快速形成。分析混合反应产物表明，不同温度条件下反应产物均能有效消耗CMAS成分，反应层的形成是阻挡CMAS持续侵蚀的关键。
, authors=张石华, 丁坤英, 于建海, 张涛, 陆锦涛, 袁嘉禧, authorsList=张石华, 丁坤英, 于建海, 张涛, 陆锦涛, 袁嘉禧, authorCompany=null, correspAuthors=丁坤英, authorNote=
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丁坤英（1981—），男，博士，教授。
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ZHANG Shihua (2000-), male, Master candidate. E-mail: shzhang2000@qq.com
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张石华（2000—），男，硕士研究生。
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张石华（2000—），男，硕士研究生。
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