Article(id=1318977223953068347, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230489, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1689004800000, receivedDateStr=2023-07-11, revisedDate=1690560000000, revisedDateStr=2023-07-29, acceptedDate=null, acceptedDateStr=null, onlineDate=1792398275602, onlineDateStr=2026-10-19, pubDate=1694448000000, pubDateStr=2023-09-12, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792398275602, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792398275602, creator=13701087609, updateTime=1792398275602, updator=13701087609, issue=Issue{id=1318977205884014990, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='12', pageStart='3039', pageEnd='3250', issueExtLink='null', onlineDate='null', pubDate='1703001600000', pubDateStr='2023-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792398271294, creator='13701087609', updateTime=1792399409679, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981980671295626, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981980671295627, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3121, endPage=3132, ext={EN=ArticleExt(id=1318977224187949372, articleId=1318977223953068347, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Properties of Al-Pillared Montmorillonite/Carbon Nanocomposites, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Al-pillared montmorillonite/carbon nanocomposites were prepared by a hydrothermal method using Al-pillared montmorillonite as a template and chitosan as a carbon source, and then hot-pressed to obtain Al-pillared montmorillonite-based ceramic/carbon composites. The effect of carbon content on the densities, mechanics, electrical conductivity and wave absorption properties of the composites was investigated by X-ray diffraction, scanning electron microscopy, universal material tests and vector network analysis. The results show that the Al-pillared montmorillonite/carbon is transformed into mullite/carbon ceramic material by hot-press sintering, and the carbon is further graphitized in the hot pressing. The introduction of carbon enhances the electrical conductivity and toughness of the composites, while a large amount of interfacial polarization is formed inside the material, which enhances the dielectric loss of the composites and transforms the ceramic material from a wave-transparent body to an electromagnetic wave absorbing material. The internal microcracks of the composites increase and the flexural strength gradually decreases with the further increase of carbon mass fraction in aluminum column-supported montmorillonite. The fracture toughness of the composite material is the maximum value when the mass ratio of montmorillonite to chitosan is 32 at 1 300 ℃, 20 MPa and 120 min of holding time, which is 11.41% greater than that of ceramics without carbon addition. The maximum electrical conductivity of the composite material is 17.53 S·m^-1 when the mass ratio of montmorillonite to chitosan is 4. According to the simulation calculations through wave absorption performance tests, the minimum R_L value of the obtained material reaches -44.93 dB when the coating thickness is 1.4 mm. The minimum R_L value is -36.28 dB and the effective absorption bandwidth is 5.0 GHz when the coating thickness is 1.6 mm.

, authors=Xueping WU^{1, 2}, Qing HE¹, Jiarui YU¹, Taohou YU¹, Xianlong ZHANG¹, authorsList=Xueping WU, Qing HE, Jiarui YU, Taohou YU, Xianlong ZHANG, authorCompany=null, correspAuthors=Xianlong ZHANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1318977224439607613, articleId=1318977223953068347, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=铝柱撑蒙脱石基陶瓷/碳复合材料的制备及其性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以铝柱撑蒙脱石为模板、壳聚糖为碳源，采用水热法制备铝柱撑蒙脱石/碳纳米复合材料，然后热压得到铝柱撑蒙脱石基陶瓷/碳复合材料。通过X射线衍射仪、扫描电子显微镜、万能材料试验机和矢量网络分析仪等研究了碳含量对复合材料的致密度、力学、导电性能和吸波性能的影响。结果表明：铝柱撑蒙脱石/碳经热压烧结转变为莫来石/碳陶瓷材料，碳在热压中进一步石墨化，碳的引入提高了复合材料的导电性和韧性，同时在材料内部形成了大量界面极化，增强了复合材料的介电损耗，使陶瓷材料由透波体转化为电磁波吸收材料。随着铝柱撑蒙脱石中碳质量分数的进一步增加，复合材料内部微裂纹增多，弯曲强度逐渐降低。在1 300 ℃、20 MPa、保温120 min的条件下进行热压烧结，蒙脱石与壳聚糖质量比为32∶1时，复合材料的断裂韧性最高，比不添加碳的陶瓷提高了11.41%；当蒙脱石与壳聚糖质量比为4∶1时，复合材料的电导率最高，达到17.53 S·m^-1。吸波性能测试模拟计算结果表明：所得材料在涂层厚度为1.4 mm时，最小反射损耗R_L值达到-44.93 dB；当涂层厚度为1.6 mm时，最小R_L值为-36.28 dB，有效吸收带宽为5.0 GHz。

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WU Xueping (1978-), female, Ph.D., Professor. E-mail: xuepingw@ustc.edu.cn

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WU Xueping (1978-), female, Ph.D., Professor. E-mail: xuepingw@ustc.edu.cn

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吴雪平（1978—），女，博士，教授。

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