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Article(id=1318977234220729241, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230432, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1687622400000, receivedDateStr=2023-06-25, revisedDate=1688918400000, revisedDateStr=2023-07-10, acceptedDate=null, acceptedDateStr=null, onlineDate=1792398278049, onlineDateStr=2026-10-19, pubDate=1694448000000, pubDateStr=2023-09-12, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792398278049, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792398278049, creator=13701087609, updateTime=1792398278049, updator=13701087609, issue=Issue{id=1318977205884014990, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='12', pageStart='3039', pageEnd='3250', issueExtLink='null', onlineDate='null', pubDate='1703001600000', pubDateStr='2023-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792398271294, creator='13701087609', updateTime=1792399409679, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981980671295626, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981980671295627, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318977205884014990, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3196, endPage=3203, ext={EN=ArticleExt(id=1318977236141720474, articleId=1318977234220729241, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Corrosion Resistance of Fused-Cast AZCS Refractory by Borosilicate Melt, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The Al2O3-ZrO2-Cr2O3-SiO2 (AZCS) material as a new type of fused-cast refractory has better corrosion resistance than other fused refractories under high-temperature and high-corrosion resistance conditions. To investigate the erosion resistance behavior of the material to the borosilicate glass melt, the AZCS material was subjected to an erosion test at 1 500 ℃, by using borosilicate glass waste-forms containing B2O3 of 12% (in mass fraction). The samples before and after erosion were analyzed by chemical analysis, X-ray diffraction, scanning electron microscopy and energy disperse spectroscopy. The results show that AZCS material can be divided into the metamorphic layer, transitional layer and central layer based on the degree of corrosion. The central layer changes little, there are still a large amount of aluminum-chromium solid solution and baddeleyite, and only a small amount of newly formed magnesia-alumina spinel. MgO infiltrating the material reacts with the solid solution to form the MA spinel in situ and partially replaces the aluminum-chromium solid solution in the original position. In the transitional layer, the maximum amount of MA spinel is formed, and the Al-Cr solid solution dissolves and disappears. Therefore, the phases in this layer are MA spinel and baddeleyite. In the metamorphic layer, there is basically only undissolved Cr2O3 phase with a loose Cr2O3 structure and a worm-like morphology. Aluminum-chromium solid solution, baddeleyite and MA spinel dissolve and disappear.

, authors=Han WEI1, 2, Limin MAO1, 2, Juntao WANG1, 2, Haishan CHEN1, 2, Haiyun YANG2, Jiwang LIU2, Xiaobin QING2, Zhanghuai ZHOU2, Qiang LIU2, Shixun SU2, Huan LI1, 2, authorsList=Han WEI, Limin MAO, Juntao WANG, Haishan CHEN, Haiyun YANG, Jiwang LIU, Xiaobin QING, Zhanghuai ZHOU, Qiang LIU, Shixun SU, Huan LI, authorCompany=null, correspAuthors=Limin MAO, authorNote=

WEI Han (1988-), male, Senior Engineer. E-mail:

, correspAuthorsNote=
MAO Limin (1965-), male, Professor. E-mail:
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Al2O3-ZrO2-Cr2O3-SiO2（AZCS）材料是一种新型熔铸耐火材料，该材料在高温、高侵蚀性条件下的抗侵蚀性能优于其他类型的电熔耐火材料。为了研究该材料对硼硅酸盐玻璃熔体的抗侵蚀行为，利用含B2O3质量分数约12%的硼硅酸盐玻璃固化体对AZCS材料在1 500 ℃条件下进行侵蚀试验。结果表明：AZCS材料在侵蚀后，按照侵蚀程度可划分为变质层、过渡层、中心层。中心层变化很小，该层仍存在大量的铝-铬固溶体和斜锆石相，只有少量新形成的镁铝尖晶石相；渗入材料的MgO与固溶体反应，在原位形成镁铝尖晶石，并部分取代原有位置上的铝-铬固溶体。在过渡层中镁铝尖晶石形成的量达到最大，铝-铬固溶体溶解消失，该层存在的相为镁铝尖晶石相与斜锆石相；在变质层中基本只存在未被溶解的Cr2O3相，Cr2O3结构松散，呈蠕虫状形貌，铝-铬固溶体、斜锆石及镁铝尖晶石均溶解消失。

, authors=魏瀚1, 2, 毛利民1, 2, 王俊涛1, 2, 陈海山1, 2, 杨海云2, 刘继旺2, 卿晓斌2, 周章怀2, 刘强2, 苏士勋2, 李欢1, 2, authorsList=魏瀚, 毛利民, 王俊涛, 陈海山, 杨海云, 刘继旺, 卿晓斌, 周章怀, 刘强, 苏士勋, 李欢, authorCompany=null, correspAuthors=毛利民, authorNote=

魏瀚（1988—），男，高级工程师。

, correspAuthorsNote=
毛利民（1965—），男，教授。
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WEI Han (1988-), male, Senior Engineer. E-mail:

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WEI Han (1988-), male, Senior Engineer. E-mail:

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魏瀚（1988—），男，高级工程师。

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魏瀚（1988—），男，高级工程师。

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熔铸锆铬刚玉耐火材料抗硼硅酸盐熔体的侵蚀行为
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魏瀚 1, 2 , 毛利民 1, 2 , 王俊涛 1, 2 , 陈海山 1, 2 , 杨海云 2 , 刘继旺 2 , 卿晓斌 2 , 周章怀 2 , 刘强 2 , 苏士勋 2 , 李欢 1, 2
硅酸盐学报 | 研究论文 2023,51(12): 3196-3203
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硅酸盐学报 |研究论文 2023 , 51 (12) : 3196 -3203
熔铸锆铬刚玉耐火材料抗硼硅酸盐熔体的侵蚀行为
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魏瀚1, 2 , 毛利民1, 2 , 王俊涛1, 2, 陈海山1, 2, 杨海云2, 刘继旺2, 卿晓斌2, 周章怀2, 刘强2, 苏士勋2, 李欢1, 2
作者信息
  • 1．中国建筑材料科学研究总院，北京 100024
  • 2．瑞泰科技股份有限公司，北京 100024
通讯作者:
毛利民（1965—），男，教授。
作者简介:

魏瀚（1988—），男，高级工程师。

Corrosion Resistance of Fused-Cast AZCS Refractory by Borosilicate Melt
Han WEI1, 2 , Limin MAO1, 2 , Juntao WANG1, 2, Haishan CHEN1, 2, Haiyun YANG2, Jiwang LIU2, Xiaobin QING2, Zhanghuai ZHOU2, Qiang LIU2, Shixun SU2, Huan LI1, 2
Affiliations
  • 1.China Building Materials Academy Co., Ltd., Beijing 100024, China
  • 2.Ruitai Materials Technology Co., Ltd., Beijing 100024, China
    • Corresponding Author:
    MAO Limin (1965-), male, Professor. E-mail:

    WEI Han (1988-), male, Senior Engineer. E-mail:

出版时间: 2023-09-12 doi: 10.14062/j.issn.0454-5648.20230432
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Al2O3-ZrO2-Cr2O3-SiO2（AZCS）材料是一种新型熔铸耐火材料，该材料在高温、高侵蚀性条件下的抗侵蚀性能优于其他类型的电熔耐火材料。为了研究该材料对硼硅酸盐玻璃熔体的抗侵蚀行为，利用含B2O3质量分数约12%的硼硅酸盐玻璃固化体对AZCS材料在1 500 ℃条件下进行侵蚀试验。结果表明：AZCS材料在侵蚀后，按照侵蚀程度可划分为变质层、过渡层、中心层。中心层变化很小，该层仍存在大量的铝-铬固溶体和斜锆石相，只有少量新形成的镁铝尖晶石相；渗入材料的MgO与固溶体反应，在原位形成镁铝尖晶石，并部分取代原有位置上的铝-铬固溶体。在过渡层中镁铝尖晶石形成的量达到最大，铝-铬固溶体溶解消失，该层存在的相为镁铝尖晶石相与斜锆石相；在变质层中基本只存在未被溶解的Cr2O3相，Cr2O3结构松散，呈蠕虫状形貌，铝-铬固溶体、斜锆石及镁铝尖晶石均溶解消失。

熔铸  /  锆铬刚玉材料  /  硼硅酸盐玻璃熔体  /  抗侵蚀

The Al2O3-ZrO2-Cr2O3-SiO2 (AZCS) material as a new type of fused-cast refractory has better corrosion resistance than other fused refractories under high-temperature and high-corrosion resistance conditions. To investigate the erosion resistance behavior of the material to the borosilicate glass melt, the AZCS material was subjected to an erosion test at 1 500 ℃, by using borosilicate glass waste-forms containing B2O3 of 12% (in mass fraction). The samples before and after erosion were analyzed by chemical analysis, X-ray diffraction, scanning electron microscopy and energy disperse spectroscopy. The results show that AZCS material can be divided into the metamorphic layer, transitional layer and central layer based on the degree of corrosion. The central layer changes little, there are still a large amount of aluminum-chromium solid solution and baddeleyite, and only a small amount of newly formed magnesia-alumina spinel. MgO infiltrating the material reacts with the solid solution to form the MA spinel in situ and partially replaces the aluminum-chromium solid solution in the original position. In the transitional layer, the maximum amount of MA spinel is formed, and the Al-Cr solid solution dissolves and disappears. Therefore, the phases in this layer are MA spinel and baddeleyite. In the metamorphic layer, there is basically only undissolved Cr2O3 phase with a loose Cr2O3 structure and a worm-like morphology. Aluminum-chromium solid solution, baddeleyite and MA spinel dissolve and disappear.

fused-cast  /  zirconium-chromium corundum refractory  /  borosilicate glass melt  /  corrosion resistance
魏瀚, 毛利民, 王俊涛, 陈海山, 杨海云, 刘继旺, 卿晓斌, 周章怀, 刘强, 苏士勋, 李欢. 熔铸锆铬刚玉耐火材料抗硼硅酸盐熔体的侵蚀行为. 硅酸盐学报, 2023 , 51 (12) : 3196 -3203 . DOI: 10.14062/j.issn.0454-5648.20230432
Han WEI, Limin MAO, Juntao WANG, Haishan CHEN, Haiyun YANG, Jiwang LIU, Xiaobin QING, Zhanghuai ZHOU, Qiang LIU, Shixun SU, Huan LI. Corrosion Resistance of Fused-Cast AZCS Refractory by Borosilicate Melt[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (12) : 3196 -3203 . DOI: 10.14062/j.issn.0454-5648.20230432
基金
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  • 中国建材集团攻关专项资助项目—高放核废液玻璃固化关键技术及工程化应用(2021HX0809)
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2023年第51卷第12期
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doi: 10.14062/j.issn.0454-5648.20230432
  • 接收时间：2023-06-25
  • 首发时间：2026-10-19
  • 出版时间：2023-09-12
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  • 收稿日期：2023-06-25
  • 修回日期：2023-07-10
基金
中国建材集团攻关专项资助项目—高放核废液玻璃固化关键技术及工程化应用(2021HX0809)
作者信息
    1．中国建筑材料科学研究总院，北京 100024
    2．瑞泰科技股份有限公司，北京 100024

通讯作者:

毛利民（1965—），男，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20230432
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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