Article(id=1318974610364805747, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20230151, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1678723200000, receivedDateStr=2023-03-14, revisedDate=1681142400000, revisedDateStr=2023-04-11, acceptedDate=null, acceptedDateStr=null, onlineDate=1792397652473, onlineDateStr=2026-10-19, pubDate=1683216000000, pubDateStr=2023-05-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792397652473, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792397652473, creator=13701087609, updateTime=1792397652473, updator=13701087609, issue=Issue{id=1318974603884606018, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='8', pageStart='1883', pageEnd='2118', issueExtLink='null', onlineDate='null', pubDate='1692460800000', pubDateStr='2023-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792397650929, creator='13701087609', updateTime=1792399225992, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981210261541260, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981210261541261, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1979, endPage=1986, ext={EN=ArticleExt(id=1318974610570326644, articleId=1318974610364805747, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Influence of Calcium Silicate Hydrate Seeds Modified by Polycarboxylate Superplasticizer on Cement Hydration Process, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

To study the promotion process of cement hydration by polycarboxylate superplasticizers modified calcium silicate hydrate (C-S-H/PCE) and understand the mechanism of C-S-H/PCE seeds promotion of cement hydration. Acrylic acid-based polycarboxylate superplasticizer (PCE-1) and silane-based polycarboxylate superplasticizer (PCE-2) were used to surface modify the hydrothermal synthesized calcium silicate hydrate (C-S-H/Unmodified) seeds, resulting in the polycarboxylate superplasticizer modified C-S-H seeds (C-S-H/PCE-1 and C-S-H/PCE-2). Subsequently, these three C-S-H seeds were added to the cement paste. The compressive strength, phase composition, and heat release curve of cement paste and the surface tension of C-S-H seeds were tested. The results showed that the surface modification of PCE-1 and PCE-2 resulted in an increase in the surface contact angle of C-S-H seeds from 36.9° to 41.1° and 42.9°, resulting in lattice mismatch of the sedimentary phase (hydration product) on the surface of the substrate material (C-S-H seeds) and inhibiting the epitaxial growth of cement hydration products on the surface of C-S-H seeds. PCE modification reduced the promoting effect of C-S-H seeds on the hydration process of Portland cement. Moreover, the degree of reduction in the hydration promoting effect of C-S-H/PCE-2 on Portland cement is significantly greater than that of C-S-H/PCE-1 crystal nucleus. Tests of the adsorption equilibrium of PCE in the pore solution indicated that the C-S-H/PCE seeds did not directly introduce new crystal nucleation sites but exposed new C-S-H surfaces through the desorption of PCE on the surface of C-S-H/PCE seeds. The desorption degree of PCE on the surface of C-S-H/PCE seeds determined the promoting effect of C-S-H/PCE seeds on cement hydration.

, authors=Xuechuang WANG¹, Ziming WANG², Xiao LIU², Hongyao SUN³, Chunyang ZHENG¹, authorsList=Xuechuang WANG, Ziming WANG, Xiao LIU, Hongyao SUN, Chunyang ZHENG, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1318974610796819061, articleId=1318974610364805747, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=聚羧酸减水剂改性水化硅酸钙晶核对水泥水化进程的影响, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

为研究聚羧酸减水剂改性水化硅酸钙晶核（C-S-H/PCE）对水泥水化的促进过程，了解C-S-H/PCE对水泥水化的促进作用机理，采用丙烯酸类型的聚羧酸减水剂（PCE-1）和硅烷类型的聚羧酸减水剂（PCE-2）对水热合成的水化硅酸钙（C-S-H/Unmodified）晶核进行表面处理得到聚羧酸减水剂改性水化硅酸钙晶核C-S-H/PCE-1和C-S-H/PCE-2，随后将不同C-S-H晶核添加到水泥净浆中。对C-S-H晶核表面张力和水泥净浆抗压强度、物相组成、水化放热曲线进行了测试，结果表明：PCE-1和PCE-2表面改性导致C-S-H晶核表面接触角从36.9°增加到41.1°和42.9°，造成了沉积相（水化产物）在衬底材料（晶核）表面的晶格失配，抑制了水泥水化产物在C-S-H晶核表面外延生长，降低了C-S-H晶核对硅酸盐水泥水化进程的促进作用，且C-S-H/PCE-2晶核对硅酸盐水泥水化促进作用降低程度明显大于C-S-H/PCE-1晶核。对水泥净浆空隙溶液中PCE的吸附平衡过程测试表明，C-S-H/PCE晶核并非直接引入了新的结晶成核位点，而是通过表面PCE的解吸附暴露出新C-S-H表面，且PCE在C-S-H/PCE晶核表面解吸附过程决定了C-S-H/PCE晶核对水泥水化促进效果。

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WANG Xuechuan (1991-), male, Master, Engineer. E-mail: aritwxc@163.com

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