Article(id=1319222591940838075, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220859, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1665417600000, receivedDateStr=2022-10-11, revisedDate=1667318400000, revisedDateStr=2022-11-02, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456775889, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456775889, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456775889, creator=13701087609, updateTime=1792456775889, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=594, endPage=601, ext={EN=ArticleExt(id=1319222592226050748, articleId=1319222591940838075, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Reaction Mechanism of Mineralizers Ferrosilicon Nitride and Calcium Carbonate in Silica Bricks, columnId=1321891096775472081, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advances in Basic Research on Refractories Related—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Silica bricks only used the combined mineralizer of calcium hydroxide and iron scale in the early domestic production. It is feasible and necessary to explore novel mineralizers to improve the performance of silica bricks. In this paper, novel silica bricks were prepared with ferrosilicon nitride and calcium carbonate as mineralizers instead of calcium hydroxide and iron scale. The prepared silica bricks have good properties, and the content of tridymite with 2% ferrosilicon nitride and calcium carbonate added reaches 62% and 65%, respectively. The effects of ferrosilicon nitride and calcium carbonate on the formation of tridymite in silica bricks were investigated by X-ray diffraction and scanning electron microscopy. The results show that in the silica brick with ferrosilicon nitride as mineralizer, Si₃N₄ network formed by the intertwined columnar Si₃N₄ in the sea urchin-like structure ferrosilicon nitride protects Fe and Fe₃Si through its oxidation reaction, thereby achieving a higher FeO/Fe₂O₃ ratio and a lower liquid formation temperature in the FeO-Fe₂O₃-SiO₂ ternary phase. The FeO/Fe₂O₃ ratio in the liquid phase fluctuates at a high temperature, and then the constant change of the solubility of tridymite in the saturated liquid phase promotes the crystallization of tridymite due to the reducibility of Fe, Fe₃Si and Si₃N₄. When calcium carbonate is used as a mineralizer of silicon brick, the formation temperature of the liquid phase in the brick is increased to 1 436 ℃. Before that, the reactions in the bricks are mainly the decomposition of calcium carbonate and the transformation from β-quartz to α-quartz and to metastable α-cristobalite. The increase of the formation temperature of the liquid phase does not reduce the content of tridymite in the brick, and the content of glass phase in the brick is less than that in the brick with iron mineralizer.

, authors=Xiuhua ZHANG¹, Chenhong MA¹, Yu QIAN², Jing YANG², Yang SUN², Yong LI¹, authorsList=Xiuhua ZHANG, Chenhong MA, Yu QIAN, Jing YANG, Yang SUN, Yong LI, authorCompany=null, correspAuthors=Chenhong MA, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222592553206461, articleId=1319222591940838075, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=硅质耐火材料中矿化剂氮化硅铁和碳酸钙的作用机理, columnId=1321891096976798674, journalTitle=硅酸盐学报, columnName=耐火材料相关基础研究进展专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

硅砖使用石灰土加铁鳞的组合矿化剂是早期国内生产条件限制下的无奈选择，随着生产条件的提升，探寻新型矿化剂以实现硅砖性能的进一步突破是切实可行且十分必要的。本工作分别以氮化硅铁和碳酸钙替代传统石灰乳加铁鳞的复合矿化剂制备硅砖。制备的新型硅砖性能良好，添加2%（质量分数）氮化硅铁和碳酸钙的硅砖中鳞石英含量分别达到62%和65%。结果表明：以氮化硅铁作为矿化剂的硅砖内，海胆结构氮化硅铁中柱状Si₃N₄相互交织构成的Si₃N₄网络，通过自身的氧化反应对其中心位置的Fe和Fe₃Si起到了保护作用，于高温下实现了FeO-Fe₂O₃-SiO₂三元系中更高的FeO/Fe₂O₃摩尔比，并同时降低了液相的生成温度。借由氮化硅铁中Fe、Fe₃Si、Si₃N₄的还原性，FeO-Fe₂O₃-SiO₂三元液相形成后，其中的FeO/Fe₂O₃摩尔比呈现波动变化，进而通过改变饱和液相中鳞石英溶解度，促进液相中石英的溶解-析晶作用。以碳酸钙作为硅砖的矿化剂时，砖内液相的生成温度提升至1436 ℃，在此之前砖内发生的反应主要为碳酸钙的分解以及β-石英至α-石英至亚稳态α-方石英的转变。液相生成温度的提升并没有降低成品砖内的鳞石英含量，并且较添加铁质矿化剂硅砖其成品砖内玻璃相含量更少。

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ZHANG Xiuhua (1978-), famale, Doctorial candidate. E-mail: zhangxiuhuajj@163.com

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ZHANG Xiuhua (1978-), famale, Doctorial candidate. E-mail: zhangxiuhuajj@163.com

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张秀华（1978—）女，博士研究生。

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张秀华（1978—）女，博士研究生。

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