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Article(id=1318974638210793635, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220854, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1665331200000, receivedDateStr=2022-10-10, revisedDate=1666627200000, revisedDateStr=2022-10-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1792397659113, onlineDateStr=2026-10-19, pubDate=1683216000000, pubDateStr=2023-05-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792397659113, onlineIssueDateStr=2026-10-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792397659113, creator=13701087609, updateTime=1792397659113, updator=13701087609, issue=Issue{id=1318974603884606018, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='8', pageStart='1883', pageEnd='2118', issueExtLink='null', onlineDate='null', pubDate='1692460800000', pubDateStr='2023-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792397650929, creator='13701087609', updateTime=1792399225992, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1318981210261541260, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1318981210261541261, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1318974603884606018, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1987, endPage=1999, ext={EN=ArticleExt(id=1318974639980789926, articleId=1318974638210793635, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Leaching Behavior of Simulated High-Level Radioactive Borosilicate Glass, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The leaching behavior of R7T7 borosilicate glasses with different waste loading amounts was evaluated via hanging the static immersion method at different temperatures and two leaching systems (i.e., deionized water and simulated North Mountain groundwater) for 365 days. The changes of etched layer phases, morphology, and composition with leaching time were also analyzed by X-ray diffractometry, scanning electron microscopy-X-ray energy spectrometry, and inductively coupled plasma mass spectrometry. The results show that the glass starts to appear in heterogeneous phases when the loading amount of waste exceeds 20%, and its composition is mainly molybdenum-rich materials and noble metals. The results of leaching experiments reveal a positive correlation between the mass loss rate of the glass and the leaching temperature. In the initial leaching phase, the three elements Na, Si, and B were leached at a higher rate in deionized water rather than in simulated Beishan groundwater, while after equilibration the three elements were leached at comparable rates in both leaching agents. The surface of the glass has a variety of crystalline phases generated after 365 days of leaching, mainly in spherical, floral, and prismatic and honeycomb morphologies, consisting mainly of components such as Mg-Si-O and Si-Nd-Gd-O. Based on the analysis above, the leaching process of glass solid is controlled due to the ion diffusion mechanism and glass network dissolution mechanism. The results of these studies can provide the data to support the future safety evaluation of high-level radioactive glass waste in geological disposal processes.

, authors=Yanli WEN1, Chunyu LIU1, Peng LIN1, Xiajie LIU1, Meng ZHANG2, Zhanglian XU2, authorsList=Yanli WEN, Chunyu LIU, Peng LIN, Xiajie LIU, Meng ZHANG, Zhanglian XU, authorCompany=null, correspAuthors=Zhanglian XU, authorNote=

WEN Yanli (1988-), male, Ph.D. E-mail:

, correspAuthorsNote=
XU Zhanglian (1985-), male, Ph.D., Professor. E-mail:
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基于R7T7硼硅酸盐玻璃配方，采用挂片静态浸泡法评价了不同包容量的R7T7硼硅酸盐玻璃固化体在不同温度和2种浸泡剂（去离子水和北山模拟地下水）浸蚀长达365 d的浸出行为。同时，用X射线衍射仪，扫描电子显微镜-X射线能谱仪和电感耦合等离子体质谱仪等手段分析了蚀变层物相、形貌及成分随浸出时间的变化情况。结果表明：包容率超过20%时玻璃开始出现异相，均匀性变差，其成分主要为富钼物质和贵金属。其后的浸出实验中发现玻璃的质量损失率与浸出温度成正相关。在初始浸出阶段，各个温度下Na，Si和B 3种元素在去离子水比模拟北山地下水的浸出率高，而平衡后三者在2种浸出剂中的浸出率相当。玻璃固化体表面在浸泡365 d后有多种结晶相生成，主要呈球状，花状和棱状和蜂窝状形貌，主要由Mg-Si-O和Si-Nd-Gd-O等成分组成。玻璃固化体的浸出过程由离子扩散机制和玻璃固化体网络溶解机制共同控制。这些研究结果可为中国未来高放玻璃固化体在地质处置过程的安全评价提供数据支撑。

, authors=文焱立1, 刘春雨1, 林鹏1, 刘夏杰1, 张蒙2, 许章炼2, authorsList=文焱立, 刘春雨, 林鹏, 刘夏杰, 张蒙, 许章炼, authorCompany=null, correspAuthors=许章炼, authorNote=

文焱立（1988—），男，博士。

, correspAuthorsNote=
许章炼（1985—），男，博士，研究员。
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模拟高放硼硅酸盐玻璃固化体的浸出行为
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文焱立 1 , 刘春雨 1 , 林鹏 1 , 刘夏杰 1 , 张蒙 2 , 许章炼 2
硅酸盐学报 | 研究论文 2023,51(8): 1987-1999
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硅酸盐学报 |研究论文 2023 , 51 (8) : 1987 -1999
模拟高放硼硅酸盐玻璃固化体的浸出行为
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文焱立1 , 刘春雨1, 林鹏1, 刘夏杰1, 张蒙2, 许章炼2
作者信息
  • 1.中广核研究院有限公司，广东 深圳 518031
  • 2.西安交通大学能源与动力工程学院，西安 710049
通讯作者:
许章炼（1985—），男，博士，研究员。
作者简介:

文焱立（1988—），男，博士。

Leaching Behavior of Simulated High-Level Radioactive Borosilicate Glass
Yanli WEN1 , Chunyu LIU1, Peng LIN1, Xiajie LIU1, Meng ZHANG2, Zhanglian XU2
Affiliations
  • 1.China Nuclear Power Technology Research Institute Co. Ltd., Shenzhen 518031, Guangdong, China
  • 2.Xi'an Jiaotong University, School of Energy and Power Engineering, Xi'an 710049, China
    • Corresponding Author:
    XU Zhanglian (1985-), male, Ph.D., Professor. E-mail:

    WEN Yanli (1988-), male, Ph.D. E-mail:

出版时间: 2023-05-05 doi: 10.14062/j.issn.0454-5648.20220854
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基于R7T7硼硅酸盐玻璃配方，采用挂片静态浸泡法评价了不同包容量的R7T7硼硅酸盐玻璃固化体在不同温度和2种浸泡剂（去离子水和北山模拟地下水）浸蚀长达365 d的浸出行为。同时，用X射线衍射仪，扫描电子显微镜-X射线能谱仪和电感耦合等离子体质谱仪等手段分析了蚀变层物相、形貌及成分随浸出时间的变化情况。结果表明：包容率超过20%时玻璃开始出现异相，均匀性变差，其成分主要为富钼物质和贵金属。其后的浸出实验中发现玻璃的质量损失率与浸出温度成正相关。在初始浸出阶段，各个温度下Na，Si和B 3种元素在去离子水比模拟北山地下水的浸出率高，而平衡后三者在2种浸出剂中的浸出率相当。玻璃固化体表面在浸泡365 d后有多种结晶相生成，主要呈球状，花状和棱状和蜂窝状形貌，主要由Mg-Si-O和Si-Nd-Gd-O等成分组成。玻璃固化体的浸出过程由离子扩散机制和玻璃固化体网络溶解机制共同控制。这些研究结果可为中国未来高放玻璃固化体在地质处置过程的安全评价提供数据支撑。

硼硅酸盐玻璃  /  静态浸出  /  浸出行为  /  蚀变层  /  浸出机理

The leaching behavior of R7T7 borosilicate glasses with different waste loading amounts was evaluated via hanging the static immersion method at different temperatures and two leaching systems (i.e., deionized water and simulated North Mountain groundwater) for 365 days. The changes of etched layer phases, morphology, and composition with leaching time were also analyzed by X-ray diffractometry, scanning electron microscopy-X-ray energy spectrometry, and inductively coupled plasma mass spectrometry. The results show that the glass starts to appear in heterogeneous phases when the loading amount of waste exceeds 20%, and its composition is mainly molybdenum-rich materials and noble metals. The results of leaching experiments reveal a positive correlation between the mass loss rate of the glass and the leaching temperature. In the initial leaching phase, the three elements Na, Si, and B were leached at a higher rate in deionized water rather than in simulated Beishan groundwater, while after equilibration the three elements were leached at comparable rates in both leaching agents. The surface of the glass has a variety of crystalline phases generated after 365 days of leaching, mainly in spherical, floral, and prismatic and honeycomb morphologies, consisting mainly of components such as Mg-Si-O and Si-Nd-Gd-O. Based on the analysis above, the leaching process of glass solid is controlled due to the ion diffusion mechanism and glass network dissolution mechanism. The results of these studies can provide the data to support the future safety evaluation of high-level radioactive glass waste in geological disposal processes.

borosilicate glass  /  static leaching  /  leaching behavior  /  altered layer  /  leaching mechanism
文焱立, 刘春雨, 林鹏, 刘夏杰, 张蒙, 许章炼. 模拟高放硼硅酸盐玻璃固化体的浸出行为. 硅酸盐学报, 2023 , 51 (8) : 1987 -1999 . DOI: 10.14062/j.issn.0454-5648.20220854
Yanli WEN, Chunyu LIU, Peng LIN, Xiajie LIU, Meng ZHANG, Zhanglian XU. Leaching Behavior of Simulated High-Level Radioactive Borosilicate Glass[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (8) : 1987 -1999 . DOI: 10.14062/j.issn.0454-5648.20220854
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  • 国家自然科学基金(21906128)
  • 西安交通大学青年拔尖人才项目基金(7121181102)
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doi: 10.14062/j.issn.0454-5648.20220854
  • 接收时间：2022-10-10
  • 首发时间：2026-10-19
  • 出版时间：2023-05-05
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  • 收稿日期：2022-10-10
  • 修回日期：2022-10-25
基金
国家自然科学基金(21906128)
西安交通大学青年拔尖人才项目基金(7121181102)
作者信息
    1.中广核研究院有限公司，广东 深圳 518031
    2.西安交通大学能源与动力工程学院，西安 710049

通讯作者:

许章炼（1985—），男，博士，研究员。
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2种不同金属材料的力学参数
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
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