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Using blue-emitting UiO-66-NH₂ with red-emitting Eu-MOF as fluorescence groups, a ratio fluorescence probe (UiO-66-NH₂@Eu-MOF) was constructed and successfully applied to the determination of trace PO₄^3- ions in environmental water samples. A ratiometric fluorescent probe for the determination of trace PO₄^3- ions in environmental water samples was constructed via combining blue-emitting UiO-66-NH₂ with red-emitting Eu-MOF. As PO₄^3- ions concentration increases, the coupling of PO₄^3- ions with Zr⁴⁺ ions in UiO-66-NH₂ leads to a weakened ligand-metal charge transfer effect, effectively restoring the luminescence of UiO-66-NH₂. Also, an intense coordination of Eu³⁺ ions with PO₄^3- ions can hinder the ligand-metal energy transfer, destroy the "antenna" effect, and lead to the quenching of Eu-MOF fluorescence. Under optimal conditions, a ratio of the fluorescence intensity at 445 nm to the fluorescence intensity at 633 nm is linearly related to PO₄^3- ions concentration in the range of 1-12 μmol/L. The sensor constructed has a good selectivity and accuracy, thus providing an effective way for the rapid detection of PO₄^3- ions.

, authors=Jiahong ZHENG, Yan ZHOU, authorsList=Jiahong ZHENG, Yan ZHOU, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222601092805599, articleId=1319222600677569501, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=基于UiO-66-NH₂@Eu-MOFs比率荧光探针的构建及其对PO₄^3-检测, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以发射蓝色荧光的UiO-66-NH₂和发射红色荧光的Eu-MOFs为荧光基团，构建了比率荧光探针（UiO-66-NH₂@Eu-MOFs），成功应用于环境水样中的微量PO₄^3-的检测。将发射蓝色荧光UiO-66-NH₂与发射红色荧光Eu-MOF结合，构建了测定环境水样中的微量PO₄^3-的比率荧光探针。结果表明：当PO₄^3-存在时，由于配体-金属电荷转移（LMCT）效应的减弱，导致UiO-66-NH₂的荧光增强；另一方面，PO₄^3-和Eu³⁺的强配位作用将阻止配体-金属的能量转移（LMET），破坏了“天线”效应并导致Eu-MOF的荧光猝灭，在最优条件下，F₄₄₅/F₆₃₃与PO₄^3-在1~12 μmol/L浓度范围内呈现良好的线性关系，表明该传感器对检测PO₄^3-有较好的选择性和灵敏性，为PO₄^3-的快速检测提供了一种新思路。

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ZHENG Jiahong (1983-), female, Ph.D., Associate Professor. E-mail: jhzheng@chd.edu.cn

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ZHENG Jiahong (1983-), female, Ph.D., Associate Professor. E-mail: jhzheng@chd.edu.cn

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郑佳红（1983—），女，博士，副教授。

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郑佳红（1983—），女，博士，副教授。

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