Article(id=1319222576203809351, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220800, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1664294400000, receivedDateStr=2022-09-28, revisedDate=1666886400000, revisedDateStr=2022-10-28, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456772136, onlineDateStr=2026-10-20, pubDate=1679241600000, pubDateStr=2023-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456772136, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456772136, creator=13701087609, updateTime=1792456772136, updator=13701087609, issue=Issue{id=1319222570398888648, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='3', pageStart='561', pageEnd='830', issueExtLink='null', onlineDate='null', pubDate='1679241600000', pubDateStr='2023-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456770752, creator='13701087609', updateTime=1792456924637, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223215889699377, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223215889699378, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222570398888648, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=571, endPage=578, ext={EN=ArticleExt(id=1319222576421913160, articleId=1319222576203809351, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis of Porous Magnesia Based Composite Spinel (Mg (Fe, Al)₂O₄) Refractory Aggregates, columnId=1321891096775472081, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Advances in Basic Research on Refractories Related—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Porous aggregates are a key material for the lightweight refractory. Porous magnesia based composite spinel (Mg (Fe, Al)₂O₄) refractory aggregates were prepared by an in-situ decomposition synthesis method with calcined magnesite, Al(OH)₃ and iron oxide as raw materials. The influence of sintering temperature (i.e., 1 000-1 600 ℃) on the microstructures and strengths was investigated, and the synthesis mechanism of porous aggregates was analyzed. The results show that the pores in the samples are composed of the pores in the micron-sized particles and the pores among micron-sized particles as well as they have a few neck connections at the sintering temperatures of 1 000-1 300 ℃, and the pores in the micron-sized particles migrate to the gaps and the necks grow with a further increase of sintering temperature to 1 400-1 600 ℃, thus promoting the compressive strength of the samples. The formation of composite spinel (Mg (Fe, Al)₂O₄) in the samples involves that MgAl₂O₄ is formed on the surface of Al(OH)₃ pseudomorph and reacts with Fe³⁺ to form the composite spinel (Mg (Fe, Al)₂O₄) with a ring structure, and MgFe₂O₄ is formed in the position of MgO and reacts with Al³⁺ to form the composite spinel (Mg (Fe, Al)₂O₄) with the granular and strip structures. The porous magnesia based composite spinel (Mg (Fe, Al)₂O₄) refractory aggregates have the optimum performance (i.e., an apparent porosity of 24.4%, a median pore size of 25.89 μm, a thermal conductivity of 2.79 W/(m·K) at 1 000 ℃ and a compressive strength of 74.4 MPa) at the sintering temperature of 1 550 ℃. Meanwhile, compared with the existing sintered magnesia, the thermal conductivity of porous magnesia based composite spinel (Mg (Fe, Al)₂O₄) refractory aggregates synthesized can be reduced by 64.7%.

, authors=Qianlin CHEN¹, Wen YAN¹, Xiao WANG², authorsList=Qianlin CHEN, Wen YAN, Xiao WANG, authorCompany=null, correspAuthors=Wen YAN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222576648405577, articleId=1319222576203809351, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=多孔镁基镁铁铝复合尖晶石耐火骨料的合成机理, columnId=1321891096976798674, journalTitle=硅酸盐学报, columnName=耐火材料相关基础研究进展专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

多孔骨料是对耐火材料进行轻量化设计的关键。以轻烧菱镁矿、氢氧化铝和铁红为原料，采用原位分解合成法，成功制备了多孔镁基镁铁铝复合尖晶石耐火骨料，在分析烧成温度（1000~1600 ℃）对显微结构与强度影响的基础上，研究了多孔骨料的合成机理。研究表明：当烧成温度为1000~1300 ℃时，试样内气孔来自微颗粒内和微颗粒之间，基本没有颈部连接；当烧成温度升高到1400~1600 ℃时，微颗粒内气孔合并长大、迁出，颈部显著长大，强度提高；镁铁铝复合尖晶石的形成过程分为2步，一是在氢氧化铝假象表面生成MgAl₂O₄后，再与Fe³⁺反应生成环状镁铁铝复合尖晶石，二是在MgO位置生成MgFe₂O₄，再与Al³⁺反应生成粒状和条状镁铁铝复合尖晶石；当烧成温度为1550 ℃时，试样具有优异的综合性能，其显气孔率为24.4%，中位孔径为25.89 μm，导热系数为2.79 W/（m·K）（1000 ℃），耐压强度为74.4 MPa，与市售烧结镁砂相比，导热系数降低了64.7%。

, authors=陈茜琳¹, 鄢文¹, 王晓², authorsList=陈茜琳, 鄢文, 王晓, authorCompany=null, correspAuthors=鄢文, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=zK0DZ0++YZGVPEDnaOz45w==, magXml=0Gib9HwJFMaDNeg1HGkkmw==, pdfUrl=null, pdf=1lAFXndc3vRPmbsKk/uXVg==, pdfFileSize=1217901, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=KYlhOUPDLo0oDK67HC8lXQ==, mapNumber=null, fund=null)}, authors=[Author(id=1322521645504381638, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1319222576203809351, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=1435294394@qq.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322521645605044936, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1319222576203809351, authorId=1322521645504381638, language=EN, stringName=Qianlin CHEN, firstName=Qianlin, middleName=null, lastName=CHEN, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=¹, address=^1.Wuhan University of Science and Technology, The State Key Laboratory of Refractories and Metallurgy, Wuhan 430081, China, bio={"content":"

CHEN Qianlin (1998-), female, Doctorial candidate. E-mail: 1435294394@qq.com

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CHEN Qianlin (1998-), female, Doctorial candidate. E-mail: 1435294394@qq.com

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陈茜琳（1998—），女，博士研究生。

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陈茜琳（1998—），女，博士研究生。

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