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Article(id=1319222658483474872, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220724, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1662048000000, receivedDateStr=2022-09-02, revisedDate=1663516800000, revisedDateStr=2022-09-19, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456791753, onlineDateStr=2026-10-20, pubDate=1681920000000, pubDateStr=2023-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456791753, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456791753, creator=13701087609, updateTime=1792456791753, updator=13701087609, issue=Issue{id=1319222618356559896, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='4', pageStart='831', pageEnd='1090', issueExtLink='null', onlineDate='null', pubDate='1681920000000', pubDateStr='2023-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456782187, creator='13701087609', updateTime=1792456947953, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223313692472320, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223313692472321, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=982, endPage=990, ext={EN=ArticleExt(id=1319222659100037561, articleId=1319222658483474872, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Fly Ash-Based No-Sintered High-Strength Filter and Its Removal of Ni2+, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

It is important to utilize fly ash (FA) as a resource due to its increasing amount. In this paper, a no-sintered fly ash-based zeolitised ceramsite (FACZ) was prepared by a high-temperature steaming method with FA as a main raw material, silica fume (SF) as a reinforcing agent and additional silicon source to achieve the high-value utilization of fly ash. The pore structure, crystal structure, microscopic morphology and functional group characteristics of the samples at each stage were characterized by specific surface area and pore size analyzer (BET), X-ray diffractometer (XRD), scanning electron microscope (SEM) and Fourier transform infrared spectrometer (FTIR). The effects of alkali concentration, SF mass fraction, temperature and steaming time on FACZ were investigated. The results show that analcime with a good crystallinity can be synthesized in FACZ under the optimized conditions (i.e., 8 mol/L NaOH, 15% SF and steaming at 190 ℃ for 48 h). The specific surface area of FACZ can reach 14.4 m2/g and the strength is 27.25 MPa after steaming. The removal efficiency of FACZ can reach 99.9%, and the maximum removal amount is 31.934 mg/g under the optimal removal conditions. The removal mechanism is a combined action of silanol and zeolite ion exchange, in which the ion exchange is the main cause.

, authors=Qian WANG1, Yi QI2, Kun WANG3, Shangquan YANG3, Yang MIAO1, Feng GAO1, authorsList=Qian WANG, Yi QI, Kun WANG, Shangquan YANG, Yang MIAO, Feng GAO, authorCompany=null, correspAuthors=Yang MIAO, authorNote=

WANG Qian (1997-), female, Master candidate. E-mail:

, correspAuthorsNote=
MIAO Yang (1987-), male, Ph.D., Associate Professor. E-mail:
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随着粉煤灰堆存量逐年增加，其资源化利用迫在眉睫。以粉煤灰（FA）为主要原料，硅灰（SF）为增强剂和外加硅源采用高温蒸养法制备免烧粉煤灰基沸石化陶粒（FACZ），从而实现粉煤灰的高值化利用。采用比表面及孔径分析仪（BET）、X射线衍射仪（XRD）、扫描电子显微镜（SEM）、红外光谱仪（FTIR）等手段，表征了各阶段样品的孔结构、晶体结构、微观形貌及官能团特征，并探究了碱浓度、SF质量分数、温度、蒸养时间对FACZ的影响，以及pH值、Ni2+浓度、时间、FACZ投加量、温度对FACZ去除Ni2+的影响。XRD、SEM、FTIR均表明FACZ中合成了结晶度良好的方沸石，优化后的工艺为8 mol/L NaOH、15% SF、190 ℃蒸养48 h；优化后的FACZ的比表面积可达14.4 m2/g，强度可达27.25 MPa。在最佳条件下，FACZ对Ni2+去除效率可达99.9%，最大去除量为31.934 mg/g；去除机理为硅羟基和沸石离子交换联合作用，且离子交换为主要原因。

, authors=王倩1, 齐怡2, 王坤3, 杨尚权3, 苗洋1, 高峰1, authorsList=王倩, 齐怡, 王坤, 杨尚权, 苗洋, 高峰, authorCompany=null, correspAuthors=苗洋, authorNote=

王倩（1997—），女，硕士研究生。

, correspAuthorsNote=
苗洋（1987—），男，博士，副教授。
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WANG Qian (1997-), female, Master candidate. E-mail:

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王倩（1997—），女，硕士研究生。

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王倩（1997—），女，硕士研究生。

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粉煤灰基免烧高强滤料的制备及其对Ni2+的去除
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王倩 1 , 齐怡 2 , 王坤 3 , 杨尚权 3 , 苗洋 1 , 高峰 1
硅酸盐学报 | 研究论文 2023,51(4): 982-990
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硅酸盐学报 |研究论文 2023 , 51 (4) : 982 -990
粉煤灰基免烧高强滤料的制备及其对Ni2+的去除
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王倩1 , 齐怡2, 王坤3, 杨尚权3, 苗洋1 , 高峰1
作者信息
  • 1．太原理工大学材料科学与工程学院，太原 030024
  • 2．山西国控晋纺实业有限公司，太原 030002
  • 3．山西省玻璃陶瓷科学研究所有限公司，山西省多孔陶瓷材料技术创新中心，太原 030013
通讯作者:
苗洋（1987—），男，博士，副教授。
作者简介:

王倩（1997—），女，硕士研究生。

Preparation of Fly Ash-Based No-Sintered High-Strength Filter and Its Removal of Ni2+
Qian WANG1 , Yi QI2, Kun WANG3, Shangquan YANG3, Yang MIAO1 , Feng GAO1
Affiliations
  • 1.College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
  • 2.Shanxi State Control Jinfang Industry Co., Taiyuan 030002, China
  • 3.Shanxi Porous Ceramic Materials Technology Innovation Center, Shanxi Provincial Glass and Ceramic Scientific Research Institute Co., Taiyuan 030013, China
    • Corresponding Author:
    MIAO Yang (1987-), male, Ph.D., Associate Professor. E-mail:

    WANG Qian (1997-), female, Master candidate. E-mail:

出版时间: 2023-04-20 doi: 10.14062/j.issn.0454-5648.20220724
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随着粉煤灰堆存量逐年增加，其资源化利用迫在眉睫。以粉煤灰（FA）为主要原料，硅灰（SF）为增强剂和外加硅源采用高温蒸养法制备免烧粉煤灰基沸石化陶粒（FACZ），从而实现粉煤灰的高值化利用。采用比表面及孔径分析仪（BET）、X射线衍射仪（XRD）、扫描电子显微镜（SEM）、红外光谱仪（FTIR）等手段，表征了各阶段样品的孔结构、晶体结构、微观形貌及官能团特征，并探究了碱浓度、SF质量分数、温度、蒸养时间对FACZ的影响，以及pH值、Ni2+浓度、时间、FACZ投加量、温度对FACZ去除Ni2+的影响。XRD、SEM、FTIR均表明FACZ中合成了结晶度良好的方沸石，优化后的工艺为8 mol/L NaOH、15% SF、190 ℃蒸养48 h；优化后的FACZ的比表面积可达14.4 m2/g，强度可达27.25 MPa。在最佳条件下，FACZ对Ni2+去除效率可达99.9%，最大去除量为31.934 mg/g；去除机理为硅羟基和沸石离子交换联合作用，且离子交换为主要原因。

粉煤灰  /  免烧陶粒  /  硅灰  /  金属离子

It is important to utilize fly ash (FA) as a resource due to its increasing amount. In this paper, a no-sintered fly ash-based zeolitised ceramsite (FACZ) was prepared by a high-temperature steaming method with FA as a main raw material, silica fume (SF) as a reinforcing agent and additional silicon source to achieve the high-value utilization of fly ash. The pore structure, crystal structure, microscopic morphology and functional group characteristics of the samples at each stage were characterized by specific surface area and pore size analyzer (BET), X-ray diffractometer (XRD), scanning electron microscope (SEM) and Fourier transform infrared spectrometer (FTIR). The effects of alkali concentration, SF mass fraction, temperature and steaming time on FACZ were investigated. The results show that analcime with a good crystallinity can be synthesized in FACZ under the optimized conditions (i.e., 8 mol/L NaOH, 15% SF and steaming at 190 ℃ for 48 h). The specific surface area of FACZ can reach 14.4 m2/g and the strength is 27.25 MPa after steaming. The removal efficiency of FACZ can reach 99.9%, and the maximum removal amount is 31.934 mg/g under the optimal removal conditions. The removal mechanism is a combined action of silanol and zeolite ion exchange, in which the ion exchange is the main cause.

fly ash  /  no-sintered ceramsite  /  silica fume  /  metal ion
王倩, 齐怡, 王坤, 杨尚权, 苗洋, 高峰. 粉煤灰基免烧高强滤料的制备及其对Ni2+的去除. 硅酸盐学报, 2023 , 51 (4) : 982 -990 . DOI: 10.14062/j.issn.0454-5648.20220724
Qian WANG, Yi QI, Kun WANG, Shangquan YANG, Yang MIAO, Feng GAO. Preparation of Fly Ash-Based No-Sintered High-Strength Filter and Its Removal of Ni2+[J]. Journal of the Chinese Ceramic Society, 2023 , 51 (4) : 982 -990 . DOI: 10.14062/j.issn.0454-5648.20220724
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  • 山西省重点研发计划项目(201903D321064)
  • 山西省科技平台建设项目(202104010911002)
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doi: 10.14062/j.issn.0454-5648.20220724
  • 接收时间：2022-09-02
  • 首发时间：2026-10-20
  • 出版时间：2023-04-20
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  • 收稿日期：2022-09-02
  • 修回日期：2022-09-19
基金
山西省重点研发计划项目(201903D321064)
山西省科技平台建设项目(202104010911002)
作者信息
    1．太原理工大学材料科学与工程学院，太原 030024
    2．山西国控晋纺实业有限公司，太原 030002
    3．山西省玻璃陶瓷科学研究所有限公司，山西省多孔陶瓷材料技术创新中心，太原 030013

通讯作者:

苗洋（1987—），男，博士，副教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20220724
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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