Article(id=1319222650237468924, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220702, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1661702400000, receivedDateStr=2022-08-29, revisedDate=1664899200000, revisedDateStr=2022-10-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456789788, onlineDateStr=2026-10-20, pubDate=1681920000000, pubDateStr=2023-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456789788, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456789788, creator=13701087609, updateTime=1792456789788, updator=13701087609, issue=Issue{id=1319222618356559896, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='4', pageStart='831', pageEnd='1090', issueExtLink='null', onlineDate='null', pubDate='1681920000000', pubDateStr='2023-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456782187, creator='13701087609', updateTime=1792456947953, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223313692472320, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223313692472321, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=872, endPage=881, ext={EN=ArticleExt(id=1319222650422018301, articleId=1319222650237468924, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Rattling Effect in A Site and Microwave Dielectric Properties of Ca_3-xMg_xYb₂Ge₃O₁₂ (0≤x≤3) Garnets, columnId=1321891335796281568, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on 5G/6G Materials—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Microwave dielectric ceramics are the key basic materials of 5G/6G communication technology, and the materials with a high quality factor (Q×f), a low dielectric constant (ε_r) and a near-zero temperature coefficient of resonant frequency (τ_f) become a focus of research and development. In this paper, a series of garnet Ca_3-xMg_xYb₂Ge₃O₁₂ (0≤x≤3) ceramics were prepared by a solid-state reaction approach, and the influence of Mg²⁺ "rattling" effects in the A-site on the microwave dielectric properties was investigated. The ceramics with 0≤x≤2 exhibit a normal garnet structure, ε_r gradually increases from 10.3 to 11.8, whereas the Q×f gradually decreases from 98 000 GHz to 78 000 GHz, and τ_f is in the range from -40×10^-6 to -56×10^-6/℃. The ceramics with 2<x≤3 have an inverse garnet structure with Mg²⁺ in the A-site and ε_r quickly increases to 13.5, whereas the Q×f apparently decreases to 19, 800 GHz, and the τ_f value varies from the negative value to the positive value (+70.5×10^-6/℃), which are attributed to the rattling effect Mg²⁺ and the mismatch between Mg²⁺ and Yb³⁺ in the A-site. According to the extrapolated values of the far-infrared reflective spectrum in the microwave region, the intrinsic ε_r and Q×f values are in a reasonable agreement with the measured values.

, authors=Ying TANG^{1, 2}, Huaicheng XIANG^{1, 2}, Jie LI¹, Liang FANG¹, authorsList=Ying TANG, Huaicheng XIANG, Jie LI, Liang FANG, authorCompany=null, correspAuthors=Liang FANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222650619150590, articleId=1319222650237468924, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Ca_3-xMg_xYb₂Ge₃O₁₂ (0≤x≤3)石榴石的A位Rattling效应与微波介电性能, columnId=1321891335972442337, journalTitle=硅酸盐学报, columnName=5G/6G材料专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

微波介质陶瓷是5G/6G通讯技术的关键基础材料，具有高品质因数（Q×f）、低介电常数（ε_r）以及近零谐振频率温度系数（τ_f）的材料已逐渐成为研究与开发的重点。通过固相反应法制备了系列Ca_3-xMg_xYb₂Ge₃O₁₂（0≤x≤3）石榴石陶瓷。当0≤x≤2时，样品为正石榴石结构，相对介电常数ε_r逐渐从10.3增加至11.8，品质因数Q×f值逐渐从98000 GHz降低到78000 GHz，谐振频率温度系数τ_f在（-40~-56）×10^-6/℃之间波动。当2<x≤3时，Mg²⁺进入A位，ε_r迅速增大（~13.5），Q×f值显著降低（~19800 GHz），τ_f值则从负急剧转变为正（+70.5×10^-6/℃），可归之于A位Mg²⁺的Rattling效应以及Mg²⁺与Yb³⁺失配的缘故。根据远红外反射谱拟合外推了Ca_3-xMg_xYb₂Ge₃O₁₂（0≤x≤3）陶瓷微波频段的本征ε_r和Q×f值，与实际测量值相符合。

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TANG Ying (1988-), female, Ph.D., Associate Professor. E-mail: tangyinggl001@aliyun.com

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TANG Ying (1988-), female, Ph.D., Associate Professor. E-mail: tangyinggl001@aliyun.com

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唐莹（1988—），女，博士，副研究员。

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唐莹（1988—），女，博士，副研究员。

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