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Article(id=1319237216153485691, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220540, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1656950400000, receivedDateStr=2022-07-05, revisedDate=1659369600000, revisedDateStr=2022-08-02, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460262572, onlineDateStr=2026-10-20, pubDate=1671465600000, pubDateStr=2022-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460262572, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460262572, creator=13701087609, updateTime=1792460262572, updator=13701087609, issue=Issue{id=1319237171312177253, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='12', pageStart='3091', pageEnd='3336', issueExtLink='null', onlineDate='null', pubDate='1671465600000', pubDateStr='2022-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460251882, creator='13701087609', updateTime=1792460721974, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319239143067071226, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319239143067071227, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3314, endPage=3322, ext={EN=ArticleExt(id=1319237216388366716, articleId=1319237216153485691, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Interfacial Reaction Between BaZrO3/Al2O3 Composite Mould and Ti-46Al-8Nb Melt, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Ti-46Al-8Nb alloy was heated to 1 650 ℃ in a BaZrO3/Al2O3 composite mould at different time. The microstructure and the dissolution of mould after contacting the alloy melt at different time were analyzed by optical microscopy, scanning electron microscopy, X-ray diffraction and inductively coupled plasma emission spectroscopy, respectively. The interfacial reaction between the alloy melt and the mould was investigated. The results show that the dissolution reaction of the mould in the alloy melt results in the different thicknesses of the erosion layer on the inner wall of the mould (i.e., 1 510, 2 476 μm and 3 574 μm) after the alloy is held for 30, 60 min and 120 min, respectively. The erosion mechanism of the melt on the mould follows a dynamic model controlled by the diffusion dissolution. The dissolution of mould refractory results in the increase of the contents of O, Zr, Y, and Si elements in the alloy as the holding time increases, further leading to the increase of the microhardness of the alloy. After solidification, an adhesion layer is formed on the alloy surface. Meanwhile, BaAl2O4 and Y4Al2O9 phases are formed in the erosion layer. Two typical inclusions, i.e., (Ti, Zr)5(Si, Al)3 and Y4Al2O9, are formed in the alloy, and their contents increase with the increase of holding time.

, authors=Lu MAO1, Yuchen YANG1, Guangyao CHEN1, 2, Baohua DUAN1, Haitao LI1, Qisheng FENG1, Xionggang LU1, 2, 3, Chonghe LI1, 2, authorsList=Lu MAO, Yuchen YANG, Guangyao CHEN, Baohua DUAN, Haitao LI, Qisheng FENG, Xionggang LU, Chonghe LI, authorCompany=null, correspAuthors=Guangyao CHEN, Chonghe LI, authorNote=

MAO Lu (1995-), male, Master candidate. E-mail:

, correspAuthorsNote=
CHEN Guangyao (1987-), male, Ph.D., Lecturer; E-mail:
LI Chonghe (1962-), male, Ph.D., Professor.
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319237216686162301, articleId=1319237216153485691, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=BaZrO3/Al2O3复合模壳与Ti-46Al-8Nb熔体界面反应机理, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

将Ti-46Al-8Nb合金置于BaZrO3/Al2O3复合模壳中，在氩气气氛下，于1 650 ℃分别保温不同时间。通过使用光学显微镜、扫描电子显微镜、X射线衍射仪及电感耦合等离子体发射光谱仪等分析了复合模壳与合金熔体接触后的界面形貌及合金中耐火材料元素的溶解量，研究了模壳与熔体间界面反应。结果表明：分别保温30、60 min和120 min后，模壳面层受熔体侵蚀并持续发生溶解反应，侵蚀层厚度分别为1 510、2 476 μm和3 574 μm，侵蚀机理符合扩散型溶解机制控制的动力学模型。合金中O、Zr、Y和Si含量及显微硬度均随保温时间增加而增加。凝固后合金表面形成附着层并有新相形成，其物相为BaAl2O4和Y4Al2O9，合金基体生成（Ti,Zr）5（Si,Al）3和Y4Al2O9 2种夹杂物，其含量随保温时间增加而增加。

, authors=毛露1, 杨宇辰1, 陈光耀1, 2, 段保华1, 李海涛1, 冯齐胜1, 鲁雄刚1, 2, 3, 李重河1, 2, authorsList=毛露, 杨宇辰, 陈光耀, 段保华, 李海涛, 冯齐胜, 鲁雄刚, 李重河, authorCompany=null, correspAuthors=陈光耀, 李重河, authorNote=

毛露（1995—），男，硕士研究生。

, correspAuthorsNote=
陈光耀（1987—），男，博士，讲师。
李重河（1962—），男，博士，教授。
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MAO Lu (1995-), male, Master candidate. E-mail:

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MAO Lu (1995-), male, Master candidate. E-mail:

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毛露（1995—），男，硕士研究生。

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BaZrO3/Al2O3复合模壳与Ti-46Al-8Nb熔体界面反应机理
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毛露 1 , 杨宇辰 1 , 陈光耀 1, 2 , 段保华 1 , 李海涛 1 , 冯齐胜 1 , 鲁雄刚 1, 2, 3 , 李重河 1, 2
硅酸盐学报 | 研究论文 2022,50(12): 3314-3322
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硅酸盐学报 |研究论文 2022 , 50 (12) : 3314 -3322
BaZrO3/Al2O3复合模壳与Ti-46Al-8Nb熔体界面反应机理
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毛露1 , 杨宇辰1, 陈光耀1, 2 , 段保华1, 李海涛1, 冯齐胜1, 鲁雄刚1, 2, 3, 李重河1, 2
作者信息
  • 1．上海大学材料科学与工程学院，省部共建高品质特殊钢冶金与制备国家重点实验室，上海市钢铁冶金新技术开发应用重点实验室，上海 200072
  • 2．上海市特种铸造工程技术研究中心，上海 201605
  • 3．上海电机学院材料学院，上海 201306
通讯作者:
陈光耀（1987—），男，博士，讲师。
李重河（1962—），男，博士，教授。
作者简介:

毛露（1995—），男，硕士研究生。

Interfacial Reaction Between BaZrO3/Al2O3 Composite Mould and Ti-46Al-8Nb Melt
Lu MAO1 , Yuchen YANG1, Guangyao CHEN1, 2 , Baohua DUAN1, Haitao LI1, Qisheng FENG1, Xionggang LU1, 2, 3, Chonghe LI1, 2
Affiliations
  • 1.State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy, School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
  • 2.Shanghai Special Casting Engineering Technology Research Center, Shanghai 201605, China
  • 3.School of Materials Science and Engineering, Shanghai DianJi University, Shanghai 201306, China
    • Corresponding Author:
    CHEN Guangyao (1987-), male, Ph.D., Lecturer; E-mail:
    LI Chonghe (1962-), male, Ph.D., Professor.

    MAO Lu (1995-), male, Master candidate. E-mail:

出版时间: 2022-12-20 doi: 10.14062/j.issn.0454-5648.20220540
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将Ti-46Al-8Nb合金置于BaZrO3/Al2O3复合模壳中，在氩气气氛下，于1 650 ℃分别保温不同时间。通过使用光学显微镜、扫描电子显微镜、X射线衍射仪及电感耦合等离子体发射光谱仪等分析了复合模壳与合金熔体接触后的界面形貌及合金中耐火材料元素的溶解量，研究了模壳与熔体间界面反应。结果表明：分别保温30、60 min和120 min后，模壳面层受熔体侵蚀并持续发生溶解反应，侵蚀层厚度分别为1 510、2 476 μm和3 574 μm，侵蚀机理符合扩散型溶解机制控制的动力学模型。合金中O、Zr、Y和Si含量及显微硬度均随保温时间增加而增加。凝固后合金表面形成附着层并有新相形成，其物相为BaAl2O4和Y4Al2O9，合金基体生成（Ti,Zr）5（Si,Al）3和Y4Al2O9 2种夹杂物，其含量随保温时间增加而增加。

钛铝合金  /  锆酸钡/氧化铝复合模壳  /  反应机制  /  夹杂物

Ti-46Al-8Nb alloy was heated to 1 650 ℃ in a BaZrO3/Al2O3 composite mould at different time. The microstructure and the dissolution of mould after contacting the alloy melt at different time were analyzed by optical microscopy, scanning electron microscopy, X-ray diffraction and inductively coupled plasma emission spectroscopy, respectively. The interfacial reaction between the alloy melt and the mould was investigated. The results show that the dissolution reaction of the mould in the alloy melt results in the different thicknesses of the erosion layer on the inner wall of the mould (i.e., 1 510, 2 476 μm and 3 574 μm) after the alloy is held for 30, 60 min and 120 min, respectively. The erosion mechanism of the melt on the mould follows a dynamic model controlled by the diffusion dissolution. The dissolution of mould refractory results in the increase of the contents of O, Zr, Y, and Si elements in the alloy as the holding time increases, further leading to the increase of the microhardness of the alloy. After solidification, an adhesion layer is formed on the alloy surface. Meanwhile, BaAl2O4 and Y4Al2O9 phases are formed in the erosion layer. Two typical inclusions, i.e., (Ti, Zr)5(Si, Al)3 and Y4Al2O9, are formed in the alloy, and their contents increase with the increase of holding time.

titanium aluminum alloy  /  barium zirconate/alumina composite mould  /  interaction mechanism  /  inclusion
毛露, 杨宇辰, 陈光耀, 段保华, 李海涛, 冯齐胜, 鲁雄刚, 李重河. BaZrO3/Al2O3复合模壳与Ti-46Al-8Nb熔体界面反应机理. 硅酸盐学报, 2022 , 50 (12) : 3314 -3322 . DOI: 10.14062/j.issn.0454-5648.20220540
Lu MAO, Yuchen YANG, Guangyao CHEN, Baohua DUAN, Haitao LI, Qisheng FENG, Xionggang LU, Chonghe LI. Interfacial Reaction Between BaZrO3/Al2O3 Composite Mould and Ti-46Al-8Nb Melt[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (12) : 3314 -3322 . DOI: 10.14062/j.issn.0454-5648.20220540
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  • 国家自然科学基金面上项目(52104305)
  • 上海市2021年度“科技创新行动计划”科技支撑碳达峰碳中和专项(21DZ1208900)
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doi: 10.14062/j.issn.0454-5648.20220540
  • 接收时间：2022-07-05
  • 首发时间：2026-10-20
  • 出版时间：2022-12-20
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  • 收稿日期：2022-07-05
  • 修回日期：2022-08-02
基金
国家自然科学基金面上项目(52104305)
上海市2021年度“科技创新行动计划”科技支撑碳达峰碳中和专项(21DZ1208900)
作者信息
    1．上海大学材料科学与工程学院，省部共建高品质特殊钢冶金与制备国家重点实验室，上海市钢铁冶金新技术开发应用重点实验室，上海 200072
    2．上海市特种铸造工程技术研究中心，上海 201605
    3．上海电机学院材料学院，上海 201306

通讯作者:

陈光耀（1987—），男，博士，讲师。
李重河（1962—），男，博士，教授。
参考文献
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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