Article(id=1319222652955377957, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220518, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1656345600000, receivedDateStr=2022-06-28, revisedDate=1664121600000, revisedDateStr=2022-09-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1792456790435, onlineDateStr=2026-10-20, pubDate=1681920000000, pubDateStr=2023-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792456790435, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792456790435, creator=13701087609, updateTime=1792456790435, updator=13701087609, issue=Issue{id=1319222618356559896, tenantId=1146029695717560320, journalId=1263187385517883426, year='2023', volume='51', issue='4', pageStart='831', pageEnd='1090', issueExtLink='null', onlineDate='null', pubDate='1681920000000', pubDateStr='2023-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792456782187, creator='13701087609', updateTime=1792456947953, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319223313692472320, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319223313692472321, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319222618356559896, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=851, endPage=858, ext={EN=ArticleExt(id=1319222653169287462, articleId=1319222652955377957, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of CaTiO₃ Addition on Properties of MgNb₂O₆ Microwave Dielectric Ceramics, columnId=1321891335796281568, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on 5G/6G Materials—Research Articles, runingTitle=null, highlight=null, articleAbstract=

To meet the requirements of high-frequency wireless communication, microwave dielectric ceramics of (1-x)MgNb₂O₆-xCaTiO₃ (x=0, 0.02, 0.04, 0.08, 0.12, and 0.16) with a near-zero temperature coefficient were prepared by a solid-state method. The effect of CaTiO₃ addition on the microstructure and dielectric properties of MgNb₂O₆ was investigated, and the formation and sintering behavior of each phase were analyzed. The results show that a proper addition of CaTiO₃ can promote the sintering of MgNb₂O₆ and reduce its sintering temperature. Based on the X-ray diffraction analysis, CaTiO₃ can react with MgNb₂O₆ to form CaNb₂O₆, Ti₈O₁₅, and Ti₂Nb₁₀O₂₉ at a high temperature. Increasing the proportion of CaTiO₃ reduces the quality factor Q×f, but increases the dielectric constant ε_r and frequency temperature coefficient τ_f. When the addition amount (x) of CaTiO₃ is 0.16, the sample has the optimum microwave dielectric properties after sintering at 1 250 ℃ for 4 h (i.e., ε_r=21.6, Q×f =86 601 GHz, and _{τf =} -₇.3×10^-6/℃).

, authors=Jiajun HUANG^{1, 2, 3}, Yueming LI^{1, 2, 3}, Yi SUN^{1, 2, 3}, Kai LI^{1, 2, 3}, Zhumei WANG^{1, 2, 3}, authorsList=Jiajun HUANG, Yueming LI, Yi SUN, Kai LI, Zhumei WANG, authorCompany=null, correspAuthors=Yueming LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319222653433528615, articleId=1319222652955377957, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=CaTiO₃添加对MgNb₂O₆微波介质陶瓷性能的影响, columnId=1321891335972442337, journalTitle=硅酸盐学报, columnName=5G/6G材料专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

为了更好的满足无线通讯高频化的要求，采用固相法制备了温度系数近零的（1-x）MgNb₂O₆-xCaTiO₃（x=0，0.02，0.04，0.08，0.12，0.16）微波介质陶瓷。研究了CaTiO₃的加入量对MgNb₂O₆微观结构和介电性能的影响，探究各物相的形成和烧结行为。结果表明：适当的CaTiO₃加入量能够促进MgNb₂O₆的烧结，降低了烧结温度。通过X射线衍射分析，CaTiO₃与MgNb₂O₆在高温时会反应生成CaNb₂O₆和Ti₈O₁₅、Ti₂Nb₁₀O₂₉。增加CaTiO₃的加入量，会降低陶瓷的品质因数Q×f，但同时会提高其介电常数ε_r和频率温度系数τ_f。当CaTiO₃的添加量x=0.16时，样品在1250 ℃烧结4 h后具有最佳的微波介电性能：ε_r=21.6，Q×f=86601 GHz，τ_f=-7.3×10^-6/℃。

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HUANG Jiajun (1996-), male, Master candidate. E-mail: 2457912385@qq.com

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HUANG Jiajun (1996-), male, Master candidate. E-mail: 2457912385@qq.com

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