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Article(id=1319237213301354947, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220415, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1652976000000, receivedDateStr=2022-05-20, revisedDate=1656432000000, revisedDateStr=2022-06-29, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460261892, onlineDateStr=2026-10-20, pubDate=1671465600000, pubDateStr=2022-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460261892, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460261892, creator=13701087609, updateTime=1792460261892, updator=13701087609, issue=Issue{id=1319237171312177253, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='12', pageStart='3091', pageEnd='3336', issueExtLink='null', onlineDate='null', pubDate='1671465600000', pubDateStr='2022-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460251882, creator='13701087609', updateTime=1792460721974, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319239143067071226, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319239143067071227, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319237171312177253, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=3260, endPage=3269, ext={EN=ArticleExt(id=1319237213603344836, articleId=1319237213301354947, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=In-situ Fabrication of Sm0.20NixCe0.80-xO2-δ Anode Materials for High-Performance Intermediate Temperatures Solid Oxide Fuel Cell, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

In-situ exsolution of metal nanoparticles affords a high content and uniform distribution of metal nanocatalysts without complex synthetic processes. To implement this strategy in practical electrodes for solid oxide fuel cells (SOFC), a series of Ni doped Sm0.20NixCe0.80-xO2-δ (SNDC) anode materials were fabricated by the Pechini method. The in-situ exsolved Ni nanoparticles are uniformly distributed on the surface of the SNDC substrate after reduction. The maximum cell performance is achieved with SNDC15 as the anode of electrolyte supported single cell, and the maximum power density of the single cell is 1.26 W/cm2 and 1.48 W/cm2 when fed with hydrogen and methanol at 700 ℃, respectively. Moreover, a strong interaction between Ni nanoparticles and the oxide support effectively inhibits the growth of carbon deposition. The single cell with methanol fuel exhibits a stable power output at 700 ℃ for 10 h.

, authors=Tian GAN1, 2, Jie MEI1, Yongdan LI2, 3, authorsList=Tian GAN, Jie MEI, Yongdan LI, authorCompany=null, correspAuthors=null, authorNote=

GAN Tian (1992-), female, Ph.D., Lecturer. E-mail:

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金属纳米颗粒的原位析出提供了高含量和均匀分布的金属纳米催化剂，并且无需复杂的合成过程。为在固体氧化物燃料电池（SOFC）的实际电极中实施这一策略，本工作用Pechini法制备了一系列不同含量Ni掺杂的Sm0.20NixCe0.80-xO2-δ（SNDC）阳极材料，并通过还原处理形成具有Ni纳米颗粒出溶的SOFC阳极材料。采用SNDC15为阳极时，电解质支撑的单电池输出性能最高，在700 ℃以氢气和甲醇为燃料时单电池最大功率密度分别为1.26 W/cm2和1.48 W/cm2。此外，小尺寸的Ni颗粒与氧化物载体之间有强相互作用，有效抑制了积碳的生长。单电池在700 ℃甲醇为燃料时能稳定运行10 h以上。

, authors=甘甜1, 2, 梅杰1, 李永丹2, 3, authorsList=甘甜, 梅杰, 李永丹, authorCompany=null, correspAuthors=null, authorNote=

甘甜（1992—），女，博士，讲师。

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GAN Tian (1992-), female, Ph.D., Lecturer. E-mail:

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甘甜（1992—），女，博士，讲师。

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甘甜（1992—），女，博士，讲师。

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原位析出制备高性能中温固体氧化物燃料电池阳极材料Sm0.20NixCe0.80-xO2-δ
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甘甜 1, 2 , 梅杰 1 , 李永丹 2, 3
硅酸盐学报 | 研究论文 2022,50(12): 3260-3269
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硅酸盐学报 |研究论文 2022 , 50 (12) : 3260 -3269
原位析出制备高性能中温固体氧化物燃料电池阳极材料Sm0.20NixCe0.80-xO2-δ
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甘甜1, 2 , 梅杰1, 李永丹2, 3
作者信息
  • 1．苏州科技大学化学与生命科学学院，江苏 苏州 215009
  • 2．天津大学化工学院，天津 300072
  • 3．芬兰阿尔托大学化工学院，芬兰 赫尔辛基 00076
作者简介:

甘甜（1992—），女，博士，讲师。

In-situ Fabrication of Sm0.20NixCe0.80-xO2-δ Anode Materials for High-Performance Intermediate Temperatures Solid Oxide Fuel Cell
Tian GAN1, 2 , Jie MEI1, Yongdan LI2, 3
Affiliations
  • 1.School of Chemistry and Life Sciences, Suzhou University of Science and Technology, Suzhou 215009, Jiangsu, China
  • 2.School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China
  • 3.School of Chemical Engineering, Aalto University, Kemistintie 1 Espoo P.O. Box 16100, FI-00076, Aalto, Finland

    • GAN Tian (1992-), female, Ph.D., Lecturer. E-mail:

出版时间: 2022-12-20 doi: 10.14062/j.issn.0454-5648.20220415
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摘要
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金属纳米颗粒的原位析出提供了高含量和均匀分布的金属纳米催化剂，并且无需复杂的合成过程。为在固体氧化物燃料电池（SOFC）的实际电极中实施这一策略，本工作用Pechini法制备了一系列不同含量Ni掺杂的Sm0.20NixCe0.80-xO2-δ（SNDC）阳极材料，并通过还原处理形成具有Ni纳米颗粒出溶的SOFC阳极材料。采用SNDC15为阳极时，电解质支撑的单电池输出性能最高，在700 ℃以氢气和甲醇为燃料时单电池最大功率密度分别为1.26 W/cm2和1.48 W/cm2。此外，小尺寸的Ni颗粒与氧化物载体之间有强相互作用，有效抑制了积碳的生长。单电池在700 ℃甲醇为燃料时能稳定运行10 h以上。

固体氧化物燃料电池  /  阳极  /  原位析出  /  掺杂氧化铈  /  甲醇燃料

In-situ exsolution of metal nanoparticles affords a high content and uniform distribution of metal nanocatalysts without complex synthetic processes. To implement this strategy in practical electrodes for solid oxide fuel cells (SOFC), a series of Ni doped Sm0.20NixCe0.80-xO2-δ (SNDC) anode materials were fabricated by the Pechini method. The in-situ exsolved Ni nanoparticles are uniformly distributed on the surface of the SNDC substrate after reduction. The maximum cell performance is achieved with SNDC15 as the anode of electrolyte supported single cell, and the maximum power density of the single cell is 1.26 W/cm2 and 1.48 W/cm2 when fed with hydrogen and methanol at 700 ℃, respectively. Moreover, a strong interaction between Ni nanoparticles and the oxide support effectively inhibits the growth of carbon deposition. The single cell with methanol fuel exhibits a stable power output at 700 ℃ for 10 h.

solid oxide fuel cells  /  anode  /  in situ exsolution  /  doped-ceria  /  methanol fuel
甘甜, 梅杰, 李永丹. 原位析出制备高性能中温固体氧化物燃料电池阳极材料Sm0.20NixCe0.80-xO2-δ. 硅酸盐学报, 2022 , 50 (12) : 3260 -3269 . DOI: 10.14062/j.issn.0454-5648.20220415
Tian GAN, Jie MEI, Yongdan LI. In-situ Fabrication of Sm0.20NixCe0.80-xO2-δ Anode Materials for High-Performance Intermediate Temperatures Solid Oxide Fuel Cell[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (12) : 3260 -3269 . DOI: 10.14062/j.issn.0454-5648.20220415
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doi: 10.14062/j.issn.0454-5648.20220415
  • 接收时间：2022-05-20
  • 首发时间：2026-10-20
  • 出版时间：2022-12-20
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  • 收稿日期：2022-05-20
  • 修回日期：2022-06-29
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苏州科技大学科研启动经费(332114509)
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    1．苏州科技大学化学与生命科学学院，江苏 苏州 215009
    2．天津大学化工学院，天津 300072
    3．芬兰阿尔托大学化工学院，芬兰 赫尔辛基 00076
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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