Article(id=1319236714472784053, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20220398, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1652371200000, receivedDateStr=2022-05-13, revisedDate=1654963200000, revisedDateStr=2022-06-12, acceptedDate=null, acceptedDateStr=null, onlineDate=1792460142963, onlineDateStr=2026-10-20, pubDate=1666195200000, pubDateStr=2022-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792460142963, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792460142963, creator=13701087609, updateTime=1792460142963, updator=13701087609, issue=Issue{id=1319236705027207343, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='10', pageStart='2579', pageEnd='2808', issueExtLink='null', onlineDate='null', pubDate='1666195200000', pubDateStr='2022-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792460140711, creator='13701087609', updateTime=1792460672919, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319238937323884737, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319238937323884738, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319236705027207343, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2676, endPage=2683, ext={EN=ArticleExt(id=1319236714724442294, articleId=1319236714472784053, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Fe/SiO₂ Ratio on Slag Structure and Separation Characteristic of Slag and Low Nickel Matte, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

To investigate the problems of high loss of nickel metal in slag for nickel flash smelting, the mechanism of Fe/SiO₂ ratio(mass ratio of Fe element to silica, hereinafter referred to as Fe/SiO₂ ratio) on the separation characteristics of matte and slag was analyzed based on the bridge oxygen structure, FeO activity and valence change law of Fe in molten slag. The results show that the activity of FeO and the contents of Fe²⁺ and Fe³⁺ in nickel slag increase with increasing the addition of Fe/SiO₂ ratio from 1.1 to 1.5. The increased Fe²⁺, Fe³⁺ and O^2- promote the dissociation of complex silicate ion groups. The contents of Q₁ and Q₂ in silicate are reduced from 32.54% and 50.25% to 23.84% and 38.81%, respectively, while the content of Q₀ is increased from 17.21% to 37.33%. The main structure of nickel slag is gradually transformed from a complex silicate structure to a Fe³⁺ connected SiO₄^4- tetrahedron structure. The mass distribution ratio of Ni in matte and slag reaches the maximum value when m(Fe)/m(SiO₂) = 1.2, which is greater than that of the original smelting slag under the same condition.

, authors=Guohua WANG¹, Yaru CUI¹, Ruimeng SHI¹, Chaofei LV^{2, 3}, Xiaoming LI¹, Junxue ZHAO¹, Shufeng Yang⁴, authorsList=Guohua WANG, Yaru CUI, Ruimeng SHI, Chaofei LV, Xiaoming LI, Junxue ZHAO, Shufeng Yang, authorCompany=null, correspAuthors=Yaru CUI, Ruimeng SHI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319236714967711927, articleId=1319236714472784053, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Fe/SiO₂比对渣结构及渣-锍分离特性的影响, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

针对硫化镍闪速熔炼过程存在的渣中镍金属损失高等难题，从熔渣桥氧结构、FeO活度及Fe的变价机制等角度分析了Fe/SiO₂比（Fe元素和SiO₂的质量比，后文简称Fe/SiO₂比）对渣-锍分离效果的作用机理。结果表明：随着渣中Fe/SiO₂比由1.1增加到1.5，FeO活度增加，增多的Fe²⁺、Fe³⁺和O^2-促进了复杂硅酸盐离子基团离解，硅酸盐结构中只有一个桥氧的Q₁和包含2个桥氧的Q₂的百分含量分别由32.54%和50.25%降低到23.84%和38.81%，而不含桥氧的Q₀的含量由17.21%增加到37.33%，镍渣的主体结构逐渐由复杂硅酸盐结构转化为由Fe³⁺连接SiO₄^4-四面体的结构，Ni在锍和渣中的质量分配比在m（Fe）/m（SiO₂）=1.2达到最大，且远高于同等条件下Ni在锍与企业原渣中对比实验结果。

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WANG Guohua (1993-), male, Doctoral candidate. E-mail: wgh@xauat.edu.cn

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WANG Guohua (1993-), male, Doctoral candidate. E-mail: wgh@xauat.edu.cn

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王国华（1993—），男，冶金环保及资源综合利用，博士研究生。

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王国华（1993—），男，冶金环保及资源综合利用，博士研究生。

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