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The microstructure of magnesium silicate hydrates pastes in different Mg/Si molar ratios was investigated by X-ray diffraction, Fourier transform infrared spectroscopy, solid-state nuclear magnetic resonance and thermogravimetric analysis, respectively. The results reveal that the formed magnesium silicate hydrates (M-S-H) is a main structure of layered tetrahedra with some chain tetrahedra and branching chain tetrahedra. The layered tetrahedra is dominated by Q³_a at a higher Mg/Si molar ratio, and the layered tetrahedra is Q³_b at a lower Mg/Si molar ratio. The contents of Q¹, Q² and Q³, especially Q² in the system of MgO-SiO₂-H₂O, all increase as the Mg/Si molar ratio increases. Also, the content of magnesium hydroxide (MH) increases, the content of unreacted Q⁴ silica decreases rapidly, the degree of hydration reaction increases, the degree of gel order and the degree of gel polymerization decrease. At a long age, the decomposition rate of MH increases, and the complexity of the gel structure increases, and the prolonged hydration time is conducive to the formation of diversified layered silicon-oxygen tetrahedral structures and the occurrence of M-S-H polymerization. The water structures of M-S-H are free, confined and structural water. The hydroxyl group is bonded with Mg²⁺ ions or combined with adsorbed water. Chain tetrahedra and branching chain tetrahedra are linked to hydroxyl groups, but Q³ silicate sites are not directly linked to hydroxyl groups. The molar ratio of Mg and Si or structural water and Si in a gel is a fixed value.

, authors=Jianmin XIAO, Yaru HU, authorsList=Jianmin XIAO, Yaru HU, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319236454534984162, articleId=1319236453956170208, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=长龄期下水化硅酸镁凝胶微观结构, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

利用X射线衍射分析、Fourier变换红外光谱、固体核磁共振和热重分析技术对长龄期下不同Mg/Si摩尔比的水化硅酸镁试样进行微观结构研究，旨在为深入表征水化硅酸镁凝胶（M-S-H）提供一定技术支撑和理论基础。结果表明：M-S-H主体为层状硅氧四面体结构，包含部分端链和支链硅氧四面体，富镁条件下M-S-H层状结构以Q³_a为主，贫镁条件下以Q³_b为主。随着Mg/Si摩尔比增大，MgO-SiO₂-H₂O体系中M-S-H凝胶Q¹、Q²、Q³含量均增多，其中Q²增幅最大，Mg（OH）₂（MH）含量增大，未反应的Q⁴_silica含量迅速降低，水化反应程度提高，凝胶有序度下降，凝胶聚合度降低。长龄期条件MH解离速度增大，凝胶结构复杂度增大；延长龄期有利于层状硅氧四面体结构多样化的形成，有助于M-S-H聚合反应的发生。M-S-H凝胶中水分子以自由水、结合水和结构水形式存在，结构水中，羟基与Mg²⁺键合或与吸附水结合，端链硅氧四面体和支链硅氧四面体与羟基直接相连，层状硅氧四面体未直接与羟基键合，凝胶中Mg与Si以及结构水与Si的摩尔比为固定值。

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XIAO Jianmin (1988-), female, Engineer, Master. E-mail: xiaomin0622@126.com

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XIAO Jianmin (1988-), female, Engineer, Master. E-mail: xiaomin0622@126.com

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肖建敏（1988—），女，工程师，硕士。

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肖建敏（1988—），女，工程师，硕士。

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