Article(id=1319986577925849302, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20211150, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1640534400000, receivedDateStr=2021-12-27, revisedDate=1642694400000, revisedDateStr=2022-01-21, acceptedDate=null, acceptedDateStr=null, onlineDate=1792638924341, onlineDateStr=2026-10-22, pubDate=1655654400000, pubDateStr=2022-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792638924341, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792638924341, creator=13701087609, updateTime=1792638924341, updator=13701087609, issue=Issue{id=1319986532933555119, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='6', pageStart='1455', pageEnd='1774', issueExtLink='null', onlineDate='null', pubDate='1655654400000', pubDateStr='2022-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792638913615, creator='13701087609', updateTime=1792639299444, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988151507075566, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988151507075567, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1504, endPage=1511, ext={EN=ArticleExt(id=1319986579175751895, articleId=1319986577925849302, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis, Microstructure and Wear Resistance of High-Entropy (Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3)C Ceramics, columnId=1321892005832151399, journalTitle=Journal of the Chinese Ceramic Society, columnName=Advanced High Entropy Ceramics—Research Articles, runingTitle=null, highlight=null, articleAbstract=

Transition metal carbide ceramics are typical representatives of ultra-high temperature ceramics with extremely high melting point and hardness. However, the toughness and wear resistance need to be improved. Based on the high-entropy theory, a multi-carbides solid solution, i.e., high-entropy carbides, has a higher melting point, a good toughness and superior friction/wear characteristics. In this paper, (Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3)C high-entropy ceramics were prepared via spark plasma sintering (SPS) at 1 600-2 100 ℃, and the densification behavior, phase composition, microstructure, mechanical properties and wear resistance were investigated. The results show that (Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3)C high-entropy ceramics with a single-phase face-centered cubic structure can be obtained by sintering at 1 700 ℃. The relative density of the high-entropy ceramics is greater than 98% at ≥1 900 ℃. The grain size increases and the elemental distribution becomes uniform as the sintering temperature increases from 1 700 ℃ to 2 100 ℃. The grain boundary sliding and oxide impurities (TiO₂) aggregation occur at grain boundaries. The dislocations appear in grains. The optimal mechanical properties of the high-entropy ceramics prepared by sintering at 2 100 ℃ can be obtained, i.e., the Vickers hardness of 20 GPa, elastic modulus of 431 GPa and fracture toughness of 4.46 MPa·m^1/2, respectively, and the average specific wear rate is 5×10^-7 mm³/(N·m), showing a superior wear resistance.

, authors=Hao CHEN¹, Zihao WU¹, Shubo ZHANG¹, Meiling LIU^{1, 2}, Wanxiu HAI^{1, 2}, Yuhong CHEN^{1, 2}, Wenzhou SUN^{1, 2}, authorsList=Hao CHEN, Zihao WU, Shubo ZHANG, Meiling LIU, Wanxiu HAI, Yuhong CHEN, Wenzhou SUN, authorCompany=null, correspAuthors=Wanxiu HAI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986581700722905, articleId=1319986577925849302, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=(Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3)C高熵陶瓷的制备、微观结构与抗磨损性能, columnId=1321892006461297000, journalTitle=硅酸盐学报, columnName=新型高熵陶瓷材料专题—研究论文, runingTitle=null, highlight=null, articleAbstract=

过渡金属碳化物陶瓷是超高温陶瓷的典型代表，具有极高的熔点和硬度，而韧性和耐磨性有待提高。近年来，在高熵理论指导下合成的多元碳化物固溶体—高熵碳化物陶瓷具有更高的熔点和良好的韧性。本工作采用放电等离子烧结（SPS）制备了具有优异耐磨性能的（Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3）C高熵陶瓷。研究了1600~2100 ℃烧结的（Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3）C高熵陶瓷的致密化行为、物相、微观形貌、力学和耐磨性能。结果表明，烧结温度为1700 ℃时，可得到面心立方结构的（Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3）C高熵陶瓷。1900 ℃以上时，高熵陶瓷相对密度大于98%。烧结温度由1700 ℃升高至2100 ℃，晶粒长大，元素扩散趋于均匀。晶粒间存在晶界滑动和氧化物杂质（TiO₂）聚集，晶粒内部存在位错。2100 ℃烧结得到的高熵陶瓷的力学性能最优，Vickers硬度、弹性模量和断裂韧性分别增加到20 GPa、431 GPa和4.46 MPa·m^1/2，同时具有优异的耐磨性，2100 ℃条件下烧结的（Ti_1/6V_1/6Nb_1/6Ta_1/6Mo_1/3）C高熵陶瓷的平均比磨损率可低至5×10^-7 mm³/（N·m）。

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CHEN Hao (1995-), male, Master candidate. E-mail: 1192343680@qq.com

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CHEN Hao (1995-), male, Master candidate. E-mail: 1192343680@qq.com

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陈浩（1995—），男，硕士研究生。

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陈浩（1995—），男，硕士研究生。

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